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Antimony pentafluoride CAS NO.7783-70-2 Application:Antimony pentafluoride CAS NO.7783-70-2
Antimony pentafluoride CAS NO.7783-70-2Appearance:off-white fine crystalline powder Storage:Dry and ventilated Package:Standard or as customer's require Application:intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for sm
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inquiryProduct Name: ANTIMONY PENTAFLUORIDE Synonyms: Antimony fluoride (SbF5);Antimony(V) pentafluoride;antimony(v)pentafluoride;ant
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Antimony pentafluoride CAS NO.7783-70-2 Application:Antimony pentafluoride CAS NO.7783-70-2
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antimony
trifluoroamine oxide
antimony pentafluoride
Conditions | Yield |
---|---|
In neat (no solvent) cylinder fiited with dry powdered element, NF3O condensed into cylinder at -196°C, mixt. heated at 210°C for 24h; not isolated, monitored by NMR, IR; | 90% |
((pentafluorosulfanyl)imino)difluorosulfane
antimonypentachloride
A
SF5N=SCl2
B
((pentafluorosulfanyl)imino)chlorofluorosulfane
C
antimony pentafluoride
Conditions | Yield |
---|---|
sulfane was condesed on SbCl5 at -196°C, heated at 100°C to initiate the reaction; fractionation through a series of traps at -6, -45, -78, -112 and -196°C in vac., a -45°C trap contained the product; | A 35% B n/a C n/a |
H2F(1+)*SbClF5(1-)=H2FSbClF5
antimony pentafluoride
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: HCl, HF; decomposition above -50°C;; |
Conditions | Yield |
---|---|
In neat (no solvent) powdered metal treated with XeF2 (air-tight autoclave, 200-300°C); |
Conditions | Yield |
---|---|
burning antimony filings in F2 atmosphere; without isolation of intermediates the end product liq. SbF5; | |
in a stream of HF-free F2; distn. in vac.; | |
In not given |
Conditions | Yield |
---|---|
HF free of water;; | |
HF free of water;; | |
at 100℃; for 3h; Autoclave; Inert atmosphere; |
Conditions | Yield |
---|---|
In hydrogen fluoride | |
In hydrogen fluoride HF (liquid); |
antimony pentafluoride
Conditions | Yield |
---|---|
With hydrogen fluoride by addn. antimonic acid into HF soln.; evapn. in vac.; cannot be crystallized; | |
With calcium fluoride; sulfuric acid by distn.; | 0% |
With hydrogen fluoride anhydrous antimonic acid with concd. HF soln.; | 0% |
Conditions | Yield |
---|---|
by glowing antimonic acid with dry HgF2; | 0% |
by glowing antimonic acid with dry HgF2; | 0% |
antimony pentafluoride
Conditions | Yield |
---|---|
With diethyl ether In dichloromethane Kinetics; byproducts: Et2O, CH3CH2F; vac. line; 298 - 343 K; | |
With 1,3-dioxolan In dichloromethane Kinetics; byproducts: Et2O, CH3CH2F; vac. line; 298 - 343 K; |
Conditions | Yield |
---|---|
With hydrogen fluoride | |
With hydrogen fluoride byproducts: HCl; with anhydrous HF excess; temp. programming is given; SbF5 in liq. form; | |
With HF byproducts: HCl; with anhydrous HF, at room temp., in dry conditions; HF excess; SbF5 in liq. form; | |
With HF byproducts: HCl; with anhydrous HF excess; temp. programming is given; SbF5 in liq. form; | |
With HF |
antimony pentafluoride
Conditions | Yield |
---|---|
byproducts: HF; at 80 °C; |
antimony pentafluoride
Conditions | Yield |
---|---|
at >240 °C; | |
at >240 °C; |
Dichlorodifluoromethane
A
antimony tetrachloride fluoride
B
antimony dichloride trifluoride
C
SbF4Cl
D
SbCl3F2
E
antimony pentafluoride
Conditions | Yield |
---|---|
In neat (no solvent) reaction at 600°C;; |
Conditions | Yield |
---|---|
In neat (no solvent) heating of antimony powder and OF2; inflammation;; | |
In neat (no solvent) heating of antimony powder and OF2; inflammation;; |
perfluoro(2,4-dimethyl-3-oxa-2,4-diazapentane)
tris(trifluoromethyl)stibane
A
Perfluoro-2-azapropen
B
tris(trifluoromethyl)hydroxylamine
C
antimony pentafluoride
Conditions | Yield |
---|---|
warming from -60°C to room temp. within 10 h; | A >99 B >99 C >99 |
warming from -60°C to room temp. within 10 h; | A >99 B >99 C >99 |
Conditions | Yield |
---|---|
In neat (no solvent) dry air atmosphere; melting and thermal decompn. above 600-650°C; TGA; |
Conditions | Yield |
---|---|
In neat (no solvent) dry air atmosphere; melting and thermal decompn. above 600-650°C; TGA; |
Conditions | Yield |
---|---|
In neat (no solvent) dry air atmosphere; melting and thermal decompn. above 600-650°C; TGA; |
Conditions | Yield |
---|---|
In neat (no solvent) dry air atmosphere; melting and thermal decompn. above 600-650°C; TGA; |
antimony(V) chloride
hydrogen fluoride
A
hydrogenchloride
B
antimony pentafluoride
Conditions | Yield |
---|---|
In hydrogen fluoride solving of SbCl5 in liq. HF;; | |
In hydrogen fluoride solving of SbCl5 in liq. HF;; |
plutonium hexafluoride
antimony(III) fluoride
A
PuF4
B
antimony pentafluoride
Conditions | Yield |
---|---|
below room temp.; powder XRD; |
iridium hexafluoride
antimony(III) fluoride
A
iridium pentafluoride
B
antimony pentafluoride
Conditions | Yield |
---|---|
In neat (no solvent) IrF6 condensed onto excess of SbF3 at -196°C, allowed to warm slowly to room temp.; volatiles species removed, fractionated; IR; |
chromium pentafluoride
KrF(1+)*SbF6(1-) = [KrF][SbF6]
A
hexafluoro-chromium(VI)
C
antimony pentafluoride
D
fluorine
Conditions | Yield |
---|---|
34°C; | A 0% B n/a C n/a D n/a |
Conditions | Yield |
---|---|
partial decompn. in wet air; | |
partial decompn. in wet air; |
fluoro(trifluoromethylsulfenyl)phosphonium SbF6
antimony pentafluoride
Conditions | Yield |
---|---|
In liquid sulphur dioxide byproducts: HF, (CF3SP)99; |
ruthenium(VI) fluoride
antimony(III) fluoride
A
ruthenium(V) fluoride
B
antimony pentafluoride
Conditions | Yield |
---|---|
RuF6 was condensed onto SbF3 at -196°C; was allowed to warm slowly to room temperature; volatiles were removed; IR; |
antimonypentachloride
B
antimony(III) chloride
C
antimony pentafluoride
Conditions | Yield |
---|---|
With HF byproducts: HCl, Cl2; with anhydrous HF; distn. (8h) at 90 °C (distn. of HCl and HF), and up to 125 °C (distn. of SbCl5, SbCl3 and SbF5); distn. at 390 °C; |
A
antimony pentafluoride
B
phosphorus pentafluoride
Conditions | Yield |
---|---|
in soln.; 194 K; 30 min; | A >99 B >99 |
NF2O(1+)*SbF6(1-) = (NF2O)(SbF6)
A
trifluoroamine oxide
B
antimony pentafluoride
antimony pentafluoride
Conditions | Yield |
---|---|
In liquid sulphur dioxide under Ar; recrystn. (SO2), elem. anal.; | 100% |
Ph3GeCo(CO)4
antimony pentafluoride
triphenylgermanium fluoride
Conditions | Yield |
---|---|
With pyrographite In diethyl ether under N2 a soln. of Co-complex in ether was added dropwise with stirring to a suspension of SbF5/C in ether at room temp., stood for 6 d; monitored by IR, filtered, pumped off, dissolved in pentane, filtered, cocnd., cooled to -20°C; | 100% |
indium(I) tetrafluoroborate
hydrogen fluoride
antimony pentafluoride
indium(I) hexafluoroantimonate
Conditions | Yield |
---|---|
In hydrogen fluoride HF (liquid); equimol., HF condenced onto reagent at 77 K, alowed to warm to room temp., left for 1 d; volatiles removed (vac.); elem. anal.; | 100% |
(2,3,7,8,12,13,17,18-octaethylporphyrinato)zinc(II)
antimony pentafluoride
Conditions | Yield |
---|---|
In dichloromethane at -78 - 20℃; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
Stage #1: hydrogen fluoride; antimony pentafluoride at -196 - 20℃; Sealed tube; Stage #2: acetonitrile at -196 - 20℃; for 0.5h; Sealed tube; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
Stage #1: hydrogen fluoride; antimony pentafluoride at -196 - 20℃; Sealed tube; Stage #2: acetonitrile at -196 - 20℃; for 0.5h; Sealed tube; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
at -196 - -64℃; for 0.166667h; Sealed tube; | 100% |
Conditions | Yield |
---|---|
at -196 - -64℃; for 0.166667h; Sealed tube; | 100% |
Conditions | Yield |
---|---|
at -196 - -64℃; for 0.166667h; Sealed tube; | 100% |
Conditions | Yield |
---|---|
In sulfur dioxide condensation of SbF5 in SO2 into a soln. of Ti-compd. in SO2 at -50°C, warming to room temp. with stirring, then stirring at room temp. for 30 min; cooling to 10-15°C and condensation of SO2, formation of a solid, elem. anal.; | 99.8% |
cis-difluorodiazene
antimony pentafluoride
N2F(1+)*SbF6(1-)=[N2F][SbF6]
Conditions | Yield |
---|---|
In hydrogen fluoride HF (liquid); (vac.); condensing HF onto SbF5 at -196°C, warming to room temp.,addn. of N2F2 at -196°C, warming to room temp., stirring for 10 min; pumping off at -64°C for 2 h; | 99.7% |
cis-osmium tetrafluoride dioxide
antimony pentafluoride
B
[OsO2F3](1+)*[SbF6](1-)=[OsO2F3][SbF6]
Conditions | Yield |
---|---|
In hydrogen fluoride HF (liquid); SbF5 added to OsO2F4, HF condensed at -196°C, warmed to room temp.; pptd. at -78°C, pumped for 5 h at 0°C; | A 99.4% B 0% |
In neat (no solvent) warmed to room temp.; pumped at 0°C for 6 d; | A 107 % B 0% |
bis(pentafluoroethyl)selenium difluoride
antimony pentafluoride
Conditions | Yield |
---|---|
20°C, 1.5 h; | 99% |
carbon monoxide
antimony pentafluoride
Conditions | Yield |
---|---|
mild conditions, low CO pressure; | 99% |
krypton difluoride
antimony pentafluoride
KrF(1+)*SbF6(1-) = [KrF][SbF6]
Conditions | Yield |
---|---|
In hydrogen fluoride dry HF was distd. in 1 equiv of SbF5, homogenized at ambient temp., 1.06 equiv of KrF2 was transferred under vac. at -196°C, warmed to room temp., cooled, warmup was repeated three cycles; volatiles pumped off at -22°C; | 99% |
Conditions | Yield |
---|---|
In further solvent(s) byproducts: COF2; absence of air and moisture; stirring AuCl3 in SbF5 under 0.6 atm CO (60-70°C, 5 d); evapn. (vac., 55°C); | 99% |
carbon monoxide
antimony pentafluoride
Conditions | Yield |
---|---|
mild conditions, low CO pressure; | 99% |
carbon monoxide
antimony pentafluoride
Conditions | Yield |
---|---|
mild conditions, low CO pressure; | 99% |
fluoroformyl chloride
antimony pentafluoride
(COClF)SbF5
Conditions | Yield |
---|---|
In neat (no solvent) Teflon ampoule inside stainless-steel vac. line; excess COClF, mixing at-196°C, stirring at -78°C for 1 h; pumping at -110°C; | 99% |
Conditions | Yield |
---|---|
In neat (no solvent) Teflon ampoule inside stainless-steel vac. line; excess COF2, mixing at -196°C, stirring at -78°C for 1 h; pumping at -126°C; | 99% |
carbon monoxide
antimony pentafluoride
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: CO2, S2O5F2, Sb2F9(SO3F); liquid SbF5, ca. 1 atm CO, 60-90°C, 2-4 d; | 99% |
With HF byproducts: CO2, S2O5F2, Sb2F9(SO3F); to the reactor charged with Os(SO3F)3 were added SbF5 and HF using a stainless steel vac. line, at -195°C CO was admitted to the reactor,heated to 50-60°C for 1-2 days without stirring; volatiles were removed in vac., crystals were washed with an SbF5/HF (2:1) mixt., volatiles were removed in vac.; | 87% |
heating at 60-90°C in 1 atm CO; |
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