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inquiryProduct name Chlorotrifluoroethylene Synonyms Chlorotrifluoroethylene/CTFE;TRIFLUORO CHLORO ETHYLENE;1,1,2-Trifluoro-2-chloroethylene;1-Chloro-1,2,2-trifluoroethene;1-Chloro-1,2,2-trifluoroethylene;2
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inquiryProduct Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
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inquiryConditions | Yield |
---|---|
With potassium zinc trihydride at 250 - 320℃; under 7500.75 Torr; for 5h; Temperature; Pressure; Inert atmosphere; Large scale; | 99.22% |
With ammonium chloride; zinc(II) chloride In methanol; water electrochemical process; | 90% |
With zinc(II) chloride; zinc In ethanol at 50℃; for 3h; Dehalogenation; | 75% |
1,1,2-Trichloro-1,2,2-trifluoroethane
A
1,2-dichloro-1,2,2-trifluoroethane
B
Chlorotrifluoroethylene
C
1,1,2-trifluoroethylene
Conditions | Yield |
---|---|
With hydrogen; silica gel; nickel at 450℃; under 760 Torr; Title compound not separated from byproducts; | A n/a B 95.8% C n/a |
bismuth(III) chloride; silica gel; palladium at 250℃; Yield given. Yields of byproduct given; | |
With hydrogen; silica gel; nickel at 450℃; under 760 Torr; Product distribution; other supported Ni catalysts and metal oxides; | |
bismuth(III) chloride; silica gel; palladium at 250℃; under 760 Torr; Product distribution; other catalysts and modifier; variation of condition: selectivity; |
Conditions | Yield |
---|---|
With zinc In dichloromethane; ethyl acetate at 0 - 20℃; for 2h; | 93% |
With hexaethylphosphoric triamide In benzonitrile ice-salt bath; | 92% |
With 1,4-dioxane; zinc | |
With zinc In dichloromethane; acetic anhydride for 3h; Ambient temperature; |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: SiFCl3, SiF2Cl2, SiFCl3; pyrolysis at 220°C, 15 hours;; | 90% |
In neat (no solvent) byproducts: SiFCl3, SiF2Cl2, SiFCl3; pyrolysis at 220°C, 15 hours;; | 90% |
at 220℃; |
(2,2-dichloro trifluoro ethyl) trichloro silane
A
Chlorotrifluoroethylene
B
1,1-dichloro-1,2-difluoroethane
Conditions | Yield |
---|---|
With sodium hydroxide; water hydrolysis at 25°C, 30 minutes;; | A 13% B 87% |
With NaOH; H2O hydrolysis at 25°C, 30 minutes;; | A 13% B 87% |
Conditions | Yield |
---|---|
With hexaethylphosphoric triamide In benzonitrile other perhalogenated alkanes; | 80% |
With hexaethylphosphoric triamide In benzonitrile ice-salt bath; | 80% |
Conditions | Yield |
---|---|
With hexaethylphosphoric triamide In benzonitrile ice-salt bath; | 78% |
1,2-dichloro-1,2,2-trifluoro-1-iodoethane
perfluoroisopropyl iodide
A
1,1,1,2,3,3,3-Heptafluoropropane
B
Chlorotrifluoroethylene
C
perfluoro(2,3-dimethylbutane)
D
perfluoro-1,2,3,4-tetrachlorobutane
Conditions | Yield |
---|---|
With acetic anhydride; zinc In dichloromethane at 40℃; | A n/a B n/a C 47% D 47% |
1,2-dichloro-1,2,2-trifluoro-1-iodoethane
perfluoroisopropyl iodide
A
1,1,1,2,3,3,3-Heptafluoropropane
B
Chlorotrifluoroethylene
C
perfluoro(2,3-dimethylbutane)
D
perfluoro-1,2,3,4-tetrachlorobutane
E
C5Cl2F10
Conditions | Yield |
---|---|
With acetic anhydride; zinc In dichloromethane at 40℃; | A n/a B n/a C 27% D 28% E 40% |
With acetic anhydride; zinc In dichloromethane at 50℃; | A n/a B n/a C 31% D 32% E 30% |
xenon difluoride
1-chlorodifluoroethenyldifluoroborane
A
Chloropentafluoroethane
B
Chlorotrifluoroethylene
C
1-chloro-2,2-difluoroethenylxenon(II) tetrafluoroborate
D
boron trifluoride
Conditions | Yield |
---|---|
In further solvent(s) soln. of CF2=CClBF2 in 1,1,1,3,3-pentafluoropropane cooled to -65°C and XeF2 added in small portions within 6 min; stirring stopped after2 h; mother liquor decanted; precipitate separated and dried in vacuum at -60°C; | A n/a B n/a C 19% D n/a |
Conditions | Yield |
---|---|
at 656.9 - 712.9℃; Thermodynamic data; | |
With potassium hydroxide at 25 - 50℃; | |
With sodium hydroxide at 25 - 50℃; |
Conditions | Yield |
---|---|
at 545℃; | |
at 545℃; | |
at 570℃; |
trans-1,1,2,2,3,4-hexafluoro-3,4-dichlorocyclobutane
Chlorotrifluoroethylene
Conditions | Yield |
---|---|
at 426 - 514℃; under 30 - 140 Torr; Rate constant; Dissoziation; |
1,2-dichloro-1,2,2-trifluoroethane
A
cis-1,2-dichloro-1,2-difluoroethene
B
Chlorotrifluoroethylene
C
1,1,2-trifluoroethylene
Conditions | Yield |
---|---|
Product distribution; Rate constant; Irradiation; IR laser pulse irradiation; |
Chlorodifluoromethane
A
polytetrafluoroethylene
B
perfluoropropylene
C
trifluoromethan
D
2-chloro-1,1,2,2-tetrafluoroethane
E
Chlorotrifluoroethylene
F
1,1,2-trifluoroethylene
Conditions | Yield |
---|---|
for 8.33333E-05h; Product distribution; Heating; varying temperatures; |
Conditions | Yield |
---|---|
Irradiation; radiation > 237 nm; |
1,2-difluoro-1,2-dichloroethene
A
polytetrafluoroethylene
B
trans-1-chloro-2-fluoroethylene
C
Chlorotrifluoroethylene
D
(Z)-1,2-difluoro-ethene
E
(E)-1,2-difluoroethene
F
cis-1,2-difluoro-1-chloroethene
Conditions | Yield |
---|---|
Mechanism; Irradiation; |
2-chloro-1,1,2,2-tetrafluoroethane
A
polytetrafluoroethylene
B
perfluoropropylene
C
Chlorotrifluoroethylene
Conditions | Yield |
---|---|
at 681.9℃; Kinetics; Mechanism; other temperatures, He-flow system; Arrhenius equation; |
1,1,1-trifluoro-2,2-dichloroethane
A
1-Chloro-2,2-difluoroethene
B
Chlorotrifluoroethylene
C
1,1,1,4,4,4-hexa-fluoro-2,2,3,3-tetrachlorobutane
D
1,1,2-trifluoroethylene
Conditions | Yield |
---|---|
With nitric oxide In neat (no solvent) at 23℃; under 1.2 - 23.8 Torr; Quantum yield; Rate constant; Mechanism; Irradiation; |
1,1,2-Trichloro-1,2,2-trifluoroethane
A
1,2-dichloro-1,2,2-trifluoroethane
B
Chlorotrifluoroethylene
Conditions | Yield |
---|---|
With potassium hydroxide at 25℃; electrolysis; Yield given; | |
With propane at 475℃; for 0.000833333h; Gas phase; |
1,1,2-Trichloro-1,2,2-trifluoroethane
A
methane
B
Chlorotrifluoroethylene
C
1,1,2-trifluoroethylene
Conditions | Yield |
---|---|
With hydrogen; nickel(II) oxide; chromium(III) oxide at 400℃; for 0.25h; Mechanism; var. temp. and catalysts; |
1,1,2-Trichloro-1,2,2-trifluoroethane
A
Chlorotrifluoroethylene
B
1,1,2-trifluoroethylene
Conditions | Yield |
---|---|
With hydrogen; nickel(II) oxide; chromium(III) oxide In gas at 350℃; Product distribution; other catalysts, other temperature; | |
With hydrogen at 550℃; for 0.000833333h; Gas phase; |
1,2-dichloro-1,2,2-trifluoro-1-iodoethane
A
Chlorotrifluoroethylene
B
perfluoro-1,2,3,4-tetrachlorobutane
C
1,2,3,5,6-pentachloro-1,1,2,3,4,4,5,6,6-nonafluoro-hexane
Conditions | Yield |
---|---|
With cadmium In acetonitrile for 1h; Ambient temperature; | A 60 % Chromat. B 21 % Chromat. C 10 % Chromat. D 3 % Chromat. |
1-chloro-1,1,2,2,3,3-hexafluoropropane
A
polytetrafluoroethylene
B
perfluoropropylene
C
Chlorotrifluoroethylene
Conditions | Yield |
---|---|
at 722.9℃; Kinetics; Mechanism; other temperatures, He-flow system; Arrhenius equation; | |
In various solvent(s) at 800℃; for 8.61111E-05h; Product distribution; Mechanism; flow pyrolysis, oth. temperature, oth. time; | A 75.54 % Chromat. B 4.14 % Chromat. C 3.58 % Chromat. |
3-chloro-3-(trifluoromethyl)diazirine
A
1,1,1-trifluoro-2-chloroethane
B
Chlorotrifluoroethylene
Conditions | Yield |
---|---|
Irradiation; | |
Irradiation; radiation > 300 nm; |
Conditions | Yield |
---|---|
With iodine for 288h; Equilibrium constant; Irradiation; various kind of irradiation, variousd times and mole ratio; |
1,1,1-trifluoro-2-bromo-2-chloroethane
A
1,1,1-trifluoro-2,2-dichloroethane
B
1,2-dibromo-1,1,2,2-tetrafluoroethane
C
Chlorotrifluoroethylene
D
1,1,2-trifluoroethylene
Conditions | Yield |
---|---|
under 7.6 Torr; Product distribution; Irradiation; var. pressure; |
Conditions | Yield |
---|---|
at 450℃; |
Conditions | Yield |
---|---|
With iodine Ambient temperature; Irradiation; | 100% |
With benzophenone; iodine at -80℃; | 95% |
With iodine In dichloromethane at 28 - 30℃; for 6h; | 42% |
With iodine | |
With iodine at 55℃; Irradiation; Yield given; |
Chlorotrifluoroethylene
dimethyl 7,12-diiodo-3,8,13,17-tetramethylporphyrin-2,18-dipropionate
Conditions | Yield |
---|---|
Stage #1: Chlorotrifluoroethylene With sec.-butyllithium; zinc(II) chloride In diethyl ether; cyclohexane at -60 - 20℃; Metallation; Stage #2: dimethyl 7,12-diiodo-3,8,13,17-tetramethylporphyrin-2,18-dipropionate; tetrakis(triphenylphosphine) palladium(0) In diethyl ether; dichloromethane; cyclohexane at 20℃; for 40h; Coupling reaction; Stage #3: With sulfuric acid In various solvents at 20℃; for 1h; Substitution; Demetallation; | 100% |
Chlorotrifluoroethylene
4-methoxy-phenol
1-(2-chloro-1,1,2-trifluoroethoxy)-4-methoxybenzene
Conditions | Yield |
---|---|
With caesium carbonate In tetrahydrofuran Reagent/catalyst; regiospecific reaction; | 99% |
With sodium hydride 1.) THF; 2.) reflux; Multistep reaction; |
2,2,3,3-tetrafluoropropanol
Chlorotrifluoroethylene
3-(2-Chloro-1,1,2-trifluoro-ethoxy)-1,1,2,2-tetrafluoro-propane
Conditions | Yield |
---|---|
With potassium hydroxide In water at 75 - 85℃; under 3000.3 Torr; Inert atmosphere; Autoclave; | 98% |
With potassium hydroxide In N,N-dimethyl-formamide |
Chlorotrifluoroethylene
perfluoro-(2,4,4,7,7,9-hexamethyl-3,8-dioxa-2,5,6,9-tetra-azadec-5-ene)
A
perfuoro-(2,9-dimethyl-4,5,7-trichloro-2,9-diazadecane)
B
Hexafluoroacetone
Conditions | Yield |
---|---|
at 140℃; for 1h; | A 31% B 98% |
at 140℃; for 1h; Product distribution; | A 31% B 98% |
Chlorotrifluoroethylene
(-)-α-methylbenzylamine
N-α-Methylbenzyl-α-chloro-α-fluoroacetimidyl fluoride
Conditions | Yield |
---|---|
In diethyl ether 1.) 1 h, 60 deg C, 2.) 12 h, 20 deg C; | 96% |
tetrachloromethane
Chlorotrifluoroethylene
pentachloro-1,2,2-trifluoro-propane
Conditions | Yield |
---|---|
With copper dichloride In acetonitrile at 127℃; for 15h; | 95% |
With aluminium trichloride | |
With 2-hydroxy-2-phenylacetophenone; CuCl2*4H2O In acetonitrile at 150℃; |
4-bromo-phenol
Chlorotrifluoroethylene
1-bromo-4-(2-chloro-1,1,2-trifluoroethoxy)benzene
Conditions | Yield |
---|---|
With caesium carbonate In tetrahydrofuran regiospecific reaction; | 95% |
With potassium hydroxide In acetone at 25℃; for 5h; | 51% |
With potassium hydroxide; acetone |
Conditions | Yield |
---|---|
With bromine at 0℃; | 95% |
With benzophenone; bromine at -80℃; | 95% |
With benzophenone | 91% |
Chlorotrifluoroethylene
Phenylselenyl bromide
1-chloro-2-bromo-1,2,2-trifluoroethyl phenyl selenide
Conditions | Yield |
---|---|
In acetonitrile at 60℃; for 15h; in a tube; | 95% |
Chlorotrifluoroethylene
1-benzyl-3-hydroxy-1H-indazole
1-benzyl-3-(2-chloro-1,1,2-trifluoroethoxy)-1H-indazole
Conditions | Yield |
---|---|
Stage #1: 1-benzyl-3-hydroxy-1H-indazole With potassium In N,N-dimethyl-formamide at 20℃; for 4h; Stage #2: Chlorotrifluoroethylene In N,N-dimethyl-formamide at 115℃; | 95% |
Chlorotrifluoroethylene
4-tert-butylphenylboronic acid
Conditions | Yield |
---|---|
With potassium phosphate; tri-tert-butylphosphonium tetrafluoroborate; bis(dibenzylideneacetone)-palladium(0) In water; N,N-dimethyl-formamide; toluene at 80℃; for 2h; Schlenk technique; Inert atmosphere; | 94% |
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate In 1,4-dioxane; water at 100℃; for 2h; Suzuki-Miyaura coupling; Inert atmosphere; | 87% |
With [1,4-bis(diphenylphosphino)butane] palladium(ll) dichloride; cesium fluoride In 1,4-dioxane; water at -196 - 100℃; for 1h; Inert atmosphere; | 84% |
Conditions | Yield |
---|---|
With xenon difluoride; silicon tetrafluoride at 20℃; for 4h; Fluorination; | 93% |
With sulfur tetrafluoride; lead dioxide at 100℃; for 2h; | |
With antimony pentafluoride at 95℃; under 500 - 700 Torr; |
chlorotripropylsilane
Chlorotrifluoroethylene
trifluorovinyltripropylsilane
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; diethyl ether; hexane; pentane 1.) -130 deg C; 2.) up to RT, 3.5 h; | 93% |
Chlorotrifluoroethylene
benzyl(chloro)dimethylsilane
benzyl(trifluorovinyl)dimethylsilane
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; diethyl ether; hexane; pentane 1.) -130 deg C; 2.) up to RT, 8 h; | 93% |
Chlorotrifluoroethylene
para-nitrobenzenethiol
(2-chloro-1,1,2-trifluoroethyl)(4-nitrophenyl)sulfane
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 40℃; under 2660.18 Torr; for 6h; Inert atmosphere; | 93% |
With potassium hydroxide In ethanol |
Conditions | Yield |
---|---|
Irradiation (UV/VIS); irradiation with Philips 500-W SPEC D8 lamp, distance 30-50 cm, 20°C, 40 h; | 93% |
Irradiation (UV/VIS); irradiation with Philips 500-W SPEC D8 lamp, distance 30-50 cm, 20°C, 40 h; | 93% |
Phenylselenyl chloride
Chlorotrifluoroethylene
1,2-dichloro-1,2,2-trifluoroethyl phenyl selenide
Conditions | Yield |
---|---|
In acetonitrile at 60℃; for 15h; in a tube; | 92% |
Chlorotrifluoroethylene
N-bromobis(trifluoromethyl)amine
bis(trifluoromethyl)-2-chloro-2-bromotrifluoroethylamine
Conditions | Yield |
---|---|
25°C, 24 h, 100°C, 24 h in dark; | 92% |
25°C, 24 h, 100°C, 24 h in dark; | 92% |
Conditions | Yield |
---|---|
With copper(l) iodide; sodium azide; 1,10-Phenanthroline In dimethyl sulfoxide; N,N-dimethyl-formamide at 20℃; for 12h; Autoclave; Inert atmosphere; | 92% |
Chlorotrifluoroethylene
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate In 1,4-dioxane; water at -196 - 100℃; for 2h; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
With benzophenone; chlorine at -80℃; | 92% |
Conditions | Yield |
---|---|
With tert-butyl peroxypivalate In ethyl acetate at 80℃; for 4h; | 91.6% |
Conditions | Yield |
---|---|
With tert-butyl peroxypivalate In acetic acid methyl ester at 80℃; for 4h; | 91.6% |
vinyl acetate
Chlorotrifluoroethylene
poly[chlorotrifluoroethylene-co-(vinyl acetate)], fluoromonomer in copolymer: 20.5 mol percent (NMR), 25.6 mol percent (elemental analysis), Mw: 282 kg/mol, Mn: 119 kg/mol, PDI: 2.37, Tg: 48 deg C; monomer(s): chlorotrifluoroethylene; vinyl acetate
Conditions | Yield |
---|---|
With Peroxydikohlensaeure-diethylester In carbon dioxide at 45℃; under 150012 - 172514 Torr; for 24h; | 91% |
2-Methyl-1H-benzimidazole
Chlorotrifluoroethylene
1-(2-Chloro-1,1,2-trifluoroethyl)-2-methylbenzimidazole
Conditions | Yield |
---|---|
With potassium hydroxide In acetone for 1.3h; | 90% |
With potassium fluoride In acetone for 89h; | 62% |
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