we mainly supply high performance oxyanthraquinone at competitive price. Appearance:yellowish acicular crystal Package:In 25kg plastic woven bags or 25kg iron drum Application:used as dye intermediates, used in papermaking industry,and to applied t
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inquiry1,ISO Certificate 2,Factory price 3,Free sample and Fast delivery Appearance:Yellow needle crystal Storage:All products should be stored at a dry and ventilated location away from fire and other dangerous goods, and should avoid direct sunlight. Pa
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Min.Order:1 Kilogram
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryAbout Product Details Anthraquinone Chemical Properties Melting point 284-286 °C (
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Min.Order:1 Kilogram
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inquiryAnthraquinone Basic information Product Name: Anthraquinone Synonyms: MORKIT;9,10(9H,10H)-anthracenedione;9,10-Anthracenedione;9,10-anthracenequinone;9,10-Anthrachinon;9,10-dihydro-9,10-
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inquiryName: 9,10-Anthraquinone CAS NO.: 84-65-1 Molecular formula: C14H8O2 Relative molecular weight: 208.21 Appearance:faint yellow or light gray crystal Storage:Store in cool and dry place, away from sun light. Package:25kg Application: used in producin
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inquiryProduct Name: Anthraquinone MF: C14H8O2 MW: 208.21 EINECS: 201-549-0 Mol File: 84-65-1.mol Anthraquinone Structure Anthraquinone Chemical Properties Melting point 284-286 °C (lit.) Boiling point 379-381 °C (lit.) dens
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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Anthraquinone CAS 84-65-1 Description Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing a strict quality
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inquiryConditions | Yield |
---|---|
With oxygen In acetone at 20℃; under 760.051 Torr; for 10h; Reagent/catalyst; Solvent; Irradiation; | 100% |
With [bis(acetoxy)iodo]benzene; tert-butyl hydroxyperoxide; 3-chloro-benzenecarboperoxoic acid In 2,2,2-trifluoroethanol at 20℃; for 9h; | 99% |
With 2-Picolinic acid; manganese(II) perchlorate hexahydrate; dihydrogen peroxide; sodium acetate In acetonitrile at 0 - 20℃; | 99% |
Conditions | Yield |
---|---|
With nicotinium dichromate In acetic acid for 0.75h; Heating; | 100% |
With potassium bromate In acetic acid Heating; | 100% |
With ruthenium trichloride; dihydrogen peroxide; acetic acid | 100% |
Conditions | Yield |
---|---|
With aluminum oxide; potassium permanganate; water In 1,2-dichloro-ethane for 75h; Ambient temperature; | 100% |
With aluminum oxide; potassium permanganate for 75h; | 100% |
With cerium(III) sulfate; barium bromate In water; acetonitrile for 20h; Heating; | 97% |
9,10-dihydro-9,10-dihydroxyanthracene
9,10-phenanthrenequinone
Conditions | Yield |
---|---|
In neat (no solvent) at 20℃; for 0.0333333h; Microwave irradiation; | 100% |
With tert.-butylhydroperoxide; RhCl(PPh3)3 In benzene at 70℃; for 48h; | 87% |
With tert.-butylhydroperoxide; RhCl(PPh3)3 In benzene at 70℃; for 48h; | 87% |
Conditions | Yield |
---|---|
Stage #1: 9-methylsulfinyl-10-(methylthio)anthracene With air; sulfuric acid In dichloromethane at 20℃; for 0.0833333h; Rearrangement; Stage #2: With water; sodium hydrogencarbonate Hydrolysis; | A n/a B 100% |
9,10-phenanthrenequinone
Conditions | Yield |
---|---|
With osmium(VIII) oxide; trimethylamine-N-oxide In tetrahydrofuran; pyridine; water at 65℃; | 100% |
anthracene-9-boronic acid
9,10-phenanthrenequinone
Conditions | Yield |
---|---|
With water; sodium hydroxide In tetrahydrofuran at 20℃; for 2h; Reagent/catalyst; | 99.03% |
Conditions | Yield |
---|---|
With zinc(II) nitrate; silica gel In tetrachloromethane for 0.25h; Heating; | 98% |
With hydrogenchloride; iodosylbenzene for 0.0833333h; Oxidation; | 79% |
With air; acetic acid Irradiation; | |
With bromine | |
With iodine |
Conditions | Yield |
---|---|
With aluminum oxide; potassium permanganate In dichloromethane at 20℃; for 72h; | 98% |
Conditions | Yield |
---|---|
With oxygen; pyrographite In 5,5-dimethyl-1,3-cyclohexadiene; toluene at 120℃; under 760.051 Torr; for 48h; Schlenk technique; Cooling with ice; | 98% |
Conditions | Yield |
---|---|
With sulfuric acid at 100℃; | 97.8% |
With sulfuric acid 1.) 140-200 deg C, vacuum 100-20 mm Hg, 2.) 180-200 deg C, 10 min; | 93% |
With Nafion-H In various solvent(s) at 180℃; for 3h; Acylation; Friedel-Crafts intramolecular acylation; | 90% |
Conditions | Yield |
---|---|
With N-Bromosuccinimide In water; N,N-dimethyl-formamide at 20 - 80℃; for 4h; Reagent/catalyst; Solvent; | 97% |
With water; potassium bromide In chloroform at 25℃; for 1.56667h; pH=12; pH-value; Electrochemical reaction; | 96% |
With 1-ethyl-2,3-dimethylimidazolium iodide; sodium hydride In tetrahydrofuran at 20℃; for 72h; | 46% |
With potassium bromate In acetic acid for 0.5h; Heating; | 80 mg |
With tetrabutylammomium bromide; oxygen In dimethylsulfoxide-d6; chloroform-d1 at 25℃; for 8h; Reagent/catalyst; Irradiation; |
N-(anthracen-9-yl)acetamide
9,10-phenanthrenequinone
Conditions | Yield |
---|---|
With Selectfluor In methanol at 30℃; for 0.5h; | 97% |
9,10-dihydroanthracene
A
[(1,10-phenanthroline)2Mn(η1-OClO3)2]
B
anthracene
C
anthracen-9(10H)-one
D
9,10-phenanthrenequinone
Conditions | Yield |
---|---|
In acetonitrile Kinetics; the soln. in acetonitrile was allowed to stand overnight at room temp.; the organic products were detected by GC/MS; the soln. was layered with ether; | A n/a B 97% C 0.8% D 2% |
9,10-bromoanthracene-9-carbaldehyde
9,10-phenanthrenequinone
Conditions | Yield |
---|---|
With N-Bromosuccinimide In water; N,N-dimethyl-formamide at 20 - 80℃; for 4h; | 97% |
With water; potassium bromide In chloroform at 25℃; pH=9; Electrochemical reaction; | 95% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1h; | 97% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 60℃; | 74% |
Conditions | Yield |
---|---|
With water; potassium bromide In chloroform at 25℃; pH=9; Electrochemical reaction; | 96% |
With air; ethanol Irradiation.Sonnenlicht; | |
With osmium(VIII) oxide In hexane at 25℃; for 4.75h; Irradiation; | |
Multi-step reaction with 3 steps 1: potassium thioacetate; potassium phosphate; bis(dibenzylideneacetone)-palladium(0); 1,1'-bis-(diphenylphosphino)ferrocene / toluene; acetone / 48 h / Inert atmosphere; Reflux 2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / Reflux 3: oxygen / 12 h / Irradiation View Scheme | |
Multi-step reaction with 2 steps 1.1: n-butyllithium / tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere 1.2: 2 h / -78 - 20 °C / Inert atmosphere 1.3: Inert atmosphere 2.1: oxygen / acetonitrile / 0.5 h / Irradiation View Scheme |
Conditions | Yield |
---|---|
With N-Bromosuccinimide In water; N,N-dimethyl-formamide at 20 - 80℃; for 3.5h; | 96% |
With water; potassium bromide In chloroform at 25℃; pH=9; Electrochemical reaction; | 91% |
With chromium(VI) oxide; acetic acid | |
With air | |
With perchloric acid; water In acetonitrile at 20℃; Electrochemical reaction; Inert atmosphere; |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; H5PV2Mo10O40(1,11) In toluene for 24h; Ambient temperature; | A 96% B 4% |
With dinitrogen monoxide; Ru(5,10,15,20-tetramesitylporphyrin)(O)2 In benzene at 200℃; under 7600 Torr; for 20h; Product distribution; Further Variations:; Solvents; Reagents; Temperatures; | A 9% B 90% |
With dinitrogen monoxide; dioxo(tetramesitylporphyrinato)ruthenium(VI) In benzene at 200℃; under 7600 Torr; for 20h; Product distribution; Further Variations:; Reagents; Solvents; Temperatures; | A 9% B 90% |
Conditions | Yield |
---|---|
With water; potassium bromide In chloroform at 25℃; pH=9; Electrochemical reaction; | 96% |
Conditions | Yield |
---|---|
With methyl 3,5-bis((1H-1,2,4-triazol-1-yl)methyl)benzoate; oxygen; sodium acetate; nickel dibromide at 120℃; under 760.051 - 912.061 Torr; for 48h; chemoselective reaction; | A 94% B 96% |
1-<<(4-fluorophenyl)sulfonyl>oxy>-9,10-anthraquinone
9,10-phenanthrenequinone
Conditions | Yield |
---|---|
With triethylammonium formate; palladium diacetate; 1,3-bis-(diphenylphosphino)propane In 1,4-dioxane at 90℃; for 0.5h; Product distribution; | 95% |
Conditions | Yield |
---|---|
With sodium bromate; nitric acid; Nafion-Ce(IV) In acetonitrile for 1h; Heating; | 95% |
With sodium bromate; Nafion-Ce(IV); Nafion-H In water; acetonitrile for 4h; Heating; | 90% |
With water; potassium bromide In chloroform at 25℃; pH=9; Electrochemical reaction; | 84% |
With air In water-d2 |
9,10-phenanthrenequinone
Conditions | Yield |
---|---|
Stage #1: anthracene; phenanthrene; mixture of With manganese(II)carbonate; oxygen; acetic anhydride; acetic acid; sodium bromide at 100℃; for 24h; Stage #2: With water; dihydrogen peroxide at 50℃; for 2h; | 95% |
9,10-Diaminoanthrazene
9,10-phenanthrenequinone
Conditions | Yield |
---|---|
With sodium periodate In water; ethyl acetate at 20℃; for 0.166667h; | 95% |
With [bis(acetoxy)iodo]benzene In acetone at 20℃; for 0.25h; | 90% |
Conditions | Yield |
---|---|
palladium on activated charcoal In toluene for 12h; Heating; | 94% |
With air |
9-methoxyanthracene-10-carboxaldehyde
9,10-phenanthrenequinone
Conditions | Yield |
---|---|
With water; potassium bromide In chloroform at 25℃; pH=9; Electrochemical reaction; | 94% |
With N-Bromosuccinimide In water; N,N-dimethyl-formamide at 20 - 80℃; for 3h; | 92% |
bei der Oxydation; | |
With (bipyH2)-CrOCl5 In dichloromethane for 12h; Ambient temperature; other reagents, variation of conditions protic or aprotic media; |
9,10-phenanthrenequinone
Conditions | Yield |
---|---|
With sodium hydroxide In water; acetonitrile at 20℃; for 5h; | 94% |
9,10-dihydroanthracen-9,10-dicarbaldehyde
9,10-phenanthrenequinone
Conditions | Yield |
---|---|
With tetrafluoroboric acid diethyl ether; iodosylbenzene In diethyl ether; dichloromethane at 20℃; for 2h; | 93% |
9,10-bis(trimethylsilyloxy)anthracene
9,10-phenanthrenequinone
Conditions | Yield |
---|---|
With lithium perchlorate In acetonitrile anode potential 1.0 V vs. SCE, graphite felt anode, 2.5 F mol-1; | 92% |
Conditions | Yield |
---|---|
at 24.84℃; Kinetics; Quantum yield; UV-irradiation; | 100% |
With aluminium(III) iodide In acetonitrile for 1h; Heating; | 70% |
With sodiumsulfide nonahydrate In ethanol at 78℃; for 2h; Inert atmosphere; | 10% |
Conditions | Yield |
---|---|
With sodium azide; sulfuric acid In dichloromethane at 0 - 20℃; | 100% |
With sodium azide; sulfuric acid In chloroform at 20 - 40℃; for 4h; | 97% |
Stage #1: 9,10-phenanthrenequinone With sulfuric acid In dichloromethane at 0℃; Schlenk technique; Inert atmosphere; Stage #2: With sodium azide In dichloromethane at 0 - 20℃; for 16h; Schlenk technique; Inert atmosphere; | 96% |
9,10-phenanthrenequinone
dimethyl 4,5-bis(methylthio)-1,3-dithiole phosphonate ester
bis[4,5-di(methylsulfanyl)-1,3-dithiol-2-ylidene]-9,10-dihydroanthracene
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran at -78℃; for 0.166667h; | 100% |
With n-butyllithium In tetrahydrofuran; hexane 1.) -78 deg C, 0.5 h, 2.) -78 deg C, 1 h; -78 deg C to r.t., overnight; | 38% |
9,10-phenanthrenequinone
10-[1-(prop-2-enyl)]-10-hydroxy-9(10H)-anthracenone
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at -23℃; for 3h; | 100% |
N-benzylglycine
9,10-phenanthrenequinone
Conditions | Yield |
---|---|
With formaldehyd In 1,4-dioxane; benzene for 3h; Reflux; Dean-Stark; | 100% |
Conditions | Yield |
---|---|
In 1,4-dioxane; benzene for 3h; Dean-Stark; Reflux; | 100% |
Conditions | Yield |
---|---|
With oxygen; nickel In xylene in a cyclic oxidation process, anthraquinone in xylol/2-octanol (1:1) is reduced over Ni/H2, the cat. is removed and sodium metaborate (containing seed crystals of peroxoborate) is added; subsequent oxidation with O2 at 30°C for 20-30 min.;; containing 10% of active oxygene;; | 99.5% |
With O2; nickel In xylene; further solvent(s) in a cyclic oxidation process, anthraquinone in xylol/2-octanol (1:1) is reduced over Ni/H2, the cat. is removed and sodium metaborate (containing seed crystals of peroxoborate) is added; subsequent oxidation with O2 at 30°C for 20-30 min.;; containing 10% of active oxygene;; | 99.5% |
Conditions | Yield |
---|---|
In water; nitric acid | 99.2% |
With phosphoric acid; sulfuric acid; nitric acid In tetrachloromethane for 6h; Ambient temperature; | 90% |
With nitric acid In water | 71% |
9,10-phenanthrenequinone
formamide
9,10-bis(formamido)anthracene
Conditions | Yield |
---|---|
for 12h; Reflux; | 99% |
Conditions | Yield |
---|---|
With hydrogen iodide; acetic acid for 120h; Heating; | 99% |
With phenylphosphane at 140℃; for 72h; | 91% |
With potassium hydroxide; Raney Ni-Al alloy In water at 90℃; for 8h; | 91% |
Conditions | Yield |
---|---|
With triphenylphosphine In benzene at 20℃; for 24h; Corey-Fuchs olefination; | 99% |
With triphenylphosphine In benzene at 20℃; for 24h; | 96% |
With triphenylphosphine In dichloromethane at 20℃; | 91% |
Conditions | Yield |
---|---|
Stage #1: 9,10-phenanthrenequinone With sulfuric acid; hydrogen; sodium dodecyl-sulfate In chlorobenzene under 10501.1 Torr; Heating; Stage #2: glycerol With sulfuric acid In chlorobenzene Reagent/catalyst; Pressure; Heating; | 98.8% |
in schwefelsaurer Loesung; | |
With sulfuric acid; acetic anhydride |
Conditions | Yield |
---|---|
In nitric acid-treated palladium; sulfuric acid | 98% |
With sulfuric acid; sulfur trioxide; mercury at 130℃; | |
With mercurosulfate; sulfuric acid; sulfur trioxide at 150℃; |
9,10-phenanthrenequinone
cis-11,12-Dicyano-9,10-ethano-9,10-dihydro-9,10-dihydroxyanthracene
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In pyridine for 2h; | 98% |
9,10-phenanthrenequinone
dimethyl 1,3-benzodithiol-2-ylphosphonate
9,10-bis-(1,3-benzdithiol-2-ylidene)-9,10-dihydroanthracene
Conditions | Yield |
---|---|
Stage #1: dimethyl 1,3-benzodithiol-2-ylphosphonate With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.25h; Wittig-Horner reaction; Stage #2: 9,10-phenanthrenequinone In tetrahydrofuran; hexane at 20℃; | 98% |
With n-butyllithium 1.) THF, -78 deg C, 20 min, 2.) -78 deg C, 1 h -> r.t., 24 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With aluminum (III) chloride; triethylamine In chloroform at 20℃; for 2h; | 97.2% |
With boric acid; tin(ll) chloride | |
With aluminium trichloride | |
With aluminum tri-bromide |
9,10-phenanthrenequinone
phenyltellurotrimethylsilane
9,10-bis(trimethylsilyloxy)anthracene
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 0.5h; reductive silylation; | 97% |
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