1,10-Dichlorodecane supplier

Name
1,10-Dichlorodecane
EINECS 218-489-6
CAS No. 2162-98-3
Article Data21
CAS DataBase
Density 0.976 g/cm³
Solubility
Melting Point 15.6 °C
Formula C₁₀H₂₀Cl₂
Boiling Point 284.3 °C at 760 mmHg
Molecular Weight 211.175
Flash Point 108.4 °C
Transport Information UN 3082
Appearance colourless liquid or white solid
Safety 37/39-26-61-60
Risk Codes 38-36/37/38-50/53
Molecular Structure
Hazard Symbols Xi,N
Synonyms NSC 9484;
PSA 0.00000
LogP 4.58480

Synthetic route

: 56757-75-6
1,10-decamethylene glycol dichloroformate

: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
With N,N-dimethyl-formamide at 130 - 140℃;	97%
With hexabutylguanidinium chloride at 120℃; for 4h;	97%

: 112-47-0
1,10-Decanediol

: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
With pyridine; thionyl chloride for 1h; Heating;	83%
With thionyl chloride
With pyridine; thionyl chloride
With thionyl chloride
Multi-step reaction with 2 steps 1: cooling 2: 97 percent / hexabutylguanidinium chloride / 4 h / 120 °C View Scheme

: (5-chloropentyl)zinc bromide

: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
With Desyl chloride; dichloro[2,2'-bis(diphenylphosphino)-1,1'-binaphthyl]palladium(II) In tetrahydrofuran at 20℃;	72%

: 111-20-6
1,10-decanedioic acid

: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
With gallium(III) trichloride; Hexamethyldisiloxane; copper dichloride In 1,2-dichloro-ethane at 60℃; for 5h; Sealed tube; Inert atmosphere;	71%

: 54512-75-3
1-bromo-5-chloropentane

: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
With dilithium trichlorocuprate; magnesium In tetrahydrofuran; diethyl ether for 0.416667h; Ambient temperature;	53%
Multi-step reaction with 2 steps 1: (i) Na, liq. NH3, Fe(NO3)3, (ii) /BRN= 1732341/ 2: H2 / Raney-Ni View Scheme
Multi-step reaction with 2 steps 1: liquid ammonia 2: H2 / Raney-Ni View Scheme
With pyridine; manganese; trifluoroacetic acid; cobalt(II) bromide In acetonitrile at 50℃; Reagent/catalyst;	80 %Chromat.

: 4224-62-8
6-chlorohexanoic acid

: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
With methanol; sodium Electrolysis;
With sodium In methanol (electrolysis);

: 90943-97-8
1,5,5,6,6,10-hexachloro-decane

: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: zinc; ethanol 2: palladium/barium sulfate; methanol. ammonia / Hydrogenation View Scheme
With ammonia; platinum Hydrogenation;

: 63616-36-4
1,5,6,10-tetrachloro-dec-5-ene

: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
With Pd-BaSO4; ammonia Hydrogenation;

: 60274-61-5
1,10-dichloro-dec-4-yne

: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
With hydrogen; nickel

: 1129-89-1
cis-cyclododecene

: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
With oxygen; ozone 1.) ethanol, r.t.; 2.) ethanol, reflux; Yield given. Multistep reaction;

: 112-47-0
1,10-Decanediol

A: 51309-10-5
10-chlorodecanol

B: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
With hydrogenchloride; zinc(II) chloride for 2h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

: 7719-09-7
thionyl chloride

: 112-47-0
1,10-Decanediol

: 2162-98-3
1,10-dichlorodecane

: 1002-69-3
decyl chloride

A: 34619-32-4
1,2-dichlorodecane

B: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
With chlorine UV-irradiation;

: 124-18-5
decane

: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: chlorine / UV-irradiation 2: chlorine / UV-irradiation View Scheme

: 110-40-7
diethyl sebacate

: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 86 percent / lithium aluminum hydride / diethyl ether / 1 h / Heating 2: 83 percent / thionyl chloride; pyridine / 1 h / Heating View Scheme

: 2467-10-9
1,1,1,5-tetrachloropentane

: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: ethanolic ammonia / beim anschliessenden Behandeln mit Wasserstoff in Gegenwart von Platin 2: zinc; ethanol 3: palladium/barium sulfate; methanol. ammonia / Hydrogenation View Scheme
Multi-step reaction with 2 steps 1: methanol.ammonia; platinum / Hydrogenation 2: palladium/barium sulfate; methanol. ammonia / Hydrogenation View Scheme

: 2009-83-8
6-chloro-1-hexanol

: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: chromium (VI)-oxide; aqueous acetic acid 2: sodium; methanol / Electrolysis View Scheme

: 10471-28-0
diethyl dodecanedioate

: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: Na / ethanol 2: SOCl2 View Scheme

: 14267-92-6
1-chloro-4-pentyne

: 2162-98-3
1,10-dichlorodecane

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: (i) Na, liq. NH3, Fe(NO3)3, (ii) /BRN= 1732341/ 2: H2 / Raney-Ni View Scheme

: 2162-98-3
1,10-dichlorodecane

: 4168-73-4
trihexylphosphine

: 1,10-di(trihexylphosphonium chloride)decane

Conditions

Conditions	Yield
at 140℃; for 24h; Inert atmosphere;	99%
at 140℃; for 24h; Inert atmosphere;	99%
at 140℃; for 24h; Inert atmosphere;	99%

: 280-57-9
1,4-diaza-bicyclo[2.2.2]octane

: 2162-98-3
1,10-dichlorodecane

: C22H44N4(2+)*2Cl(1-)

Conditions

Conditions	Yield
In acetonitrile at 20℃; for 24h;	92%

: 2162-98-3
1,10-dichlorodecane

: 6637-29-2
2-(phenoxymethyl)-1H-benzimidazole

: 1039358-76-3
C24H31ClN2O

Conditions

Conditions	Yield
With sodium hydroxide Heating;	92%

: 2162-98-3
1,10-dichlorodecane

: 16355-92-3
1,10-diiododecane

Conditions

Conditions	Yield
With sodium iodide In acetone for 24h; Heating;	90%
With sodium iodide In acetone at 125℃;	62%
With acetone; sodium iodide
With sodium iodide In acetone

: 616-47-7
1-methyl-1H-imidazole

: 2162-98-3
1,10-dichlorodecane

: C18H32N4(2+)*2Cl(1-)

Conditions

Conditions	Yield
In acetonitrile at 120℃; for 48h; Inert atmosphere; Green chemistry;	90%

: 621-72-7
2-benzylbenzimidazole

: 2162-98-3
1,10-dichlorodecane

: 1039358-84-3
C24H31ClN2

Conditions

Conditions	Yield
With sodium hydroxide Heating;	86%

: 2162-98-3
1,10-dichlorodecane

: 64690-19-3
4-(octylamino)pyridine

: 70775-75-6
octenidine dihydrochloride

Conditions

Conditions	Yield
In acetic acid butyl ester for 12h; Reflux;	85.1%
In N,N-dimethyl-formamide at 120 - 180℃;	39%
In water

: 2162-98-3
1,10-dichlorodecane

: 143998-20-3
4-[tris-(4-tert-butylphenyl)methyl]phenol

: 1-chloro-10-{4'-[tris(p-t-butylphenyl)methyl]phenoxy}decane

Conditions

Conditions	Yield
Stage #1: 4-[tris-(4-tert-butylphenyl)methyl]phenol With potassium carbonate In acetonitrile for 2h; Reflux; Stage #2: 1,10-dichlorodecane In acetonitrile for 96h; Reflux;	85%

: 2162-98-3
1,10-dichlorodecane

: 90-05-1
2-methoxy-phenol

: C17H27ClO2

Conditions

Conditions	Yield
With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide In water for 16h; Inert atmosphere; Schlenk technique; Reflux;	83%

: 2162-98-3
1,10-dichlorodecane

: 3069-25-8
N-methyl-3-trimethoxysilylpropylamine

: N,N'-bis(trimethoxysilylpropyl)-N,N'-dimethyl-1,10-decanediamine

Conditions

Conditions	Yield
at 130℃; for 5h; Inert atmosphere;	78.8%

: 2162-98-3
1,10-dichlorodecane

: N-methylaminopropylmethyldiethoxysilane

: N,N'-bis(methyldiethoxysilylpropyl)-N,N'-dimethyl-1,10-decanediamine

Conditions

Conditions	Yield
at 130℃; for 5h; Inert atmosphere;	76.8%

: 504-24-5
4-aminopyridine

: 2162-98-3
1,10-dichlorodecane

: N,N′-(decane-1,10-diyl)bis(4-aminopyridinium)dichloride

Conditions

Conditions	Yield
In pentan-1-ol for 21h; Reflux; Inert atmosphere;	75%

: 2162-98-3
1,10-dichlorodecane

: 52217-62-6
1,10-bis(trichlorosilyl)decane

Conditions

Conditions	Yield
With trichlorosilane; tetra-n-butylphosphonium chloride at 150℃; for 6h; Inert atmosphere; Sealed tube;	74.8%

: 3179-63-3
3-Dimethylamino-1-propanol

: 2162-98-3
1,10-dichlorodecane

: C20H46N2O2(2+)*2Cl(1-)

Conditions

Conditions	Yield
In acetonitrile at 20℃; for 48h;	71%

: 4668-00-2
chlorotrimethoxysilane

: 2162-98-3
1,10-dichlorodecane

: 1,10-Bis(trimethoxysilyl)decane

Conditions

Conditions	Yield
With magnesium In tetrahydrofuran at 20℃; for 12h; Condensation;	70%

: 2162-98-3
1,10-dichlorodecane

: 108-95-2
phenol

: 172174-16-2
1-chloro-10-phenoxydecane

Conditions

Conditions	Yield
With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate for 16h; Heating;	69%

: 2162-98-3
1,10-dichlorodecane

: 25364-47-0
1-(2,6-diisopropylphenyl)-1H-imidazole

: 1,1'-di(2,6-diisopropropylphenyl)-3,3'-(1,10-decanediyl)diimidazolium dichloride

Conditions

Conditions	Yield
at 130℃; for 8h; neat (no solvent);	69%

: 2162-98-3
1,10-dichlorodecane

: 25364-44-7
N-(2,4,6-trimethylphenyl)imidazole

: 1,1'-dimesityl-3,3'-(1,10-decanediyl)bisimidazolium dichloride

Conditions

Conditions	Yield
at 115℃; for 6h; neat (no solvent);	66%

: 2162-98-3
1,10-dichlorodecane

: C12H16N2

: C34H48Cl2N4

Conditions

Conditions	Yield
at 110℃;	66%

: 616-47-7
1-methyl-1H-imidazole

: 2162-98-3
1,10-dichlorodecane

: 1-(10-chlorodecyl)-3-methylimidazolium chloride

Conditions

Conditions	Yield
In chloroform for 360h; Reflux;	61%

: 2162-98-3
1,10-dichlorodecane

: 25372-09-2
1-(2,6-dimethylphenyl)-1H-imidazole

: 1,1'-bis(2,6-dimethylphenyl)-3,3'-(1,10-decanediyl)bisimidazolium dichloride

Conditions

Conditions	Yield
at 120℃; for 6h; neat (no solvent);	59%

: 626-61-9
4-Chloropyridine

: 2162-98-3
1,10-dichlorodecane

: 1,10-bis-(4-chloropyridin-1 (4H)-yl)decane

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 150℃; for 20h;	57%

: 2162-98-3
1,10-dichlorodecane

: 89-95-2
2-methyl-benzyl alcohol

: 664326-18-5
2-(10-chlorodecyloxy)benzaldehyde

Conditions

Conditions	Yield
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 3h;	54%

: 2162-98-3
1,10-dichlorodecane

: 626-41-5
3,5-dibromophenol

: C16H23Br2ClO

Conditions

Conditions	Yield
With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide In water for 16h; Inert atmosphere; Schlenk technique; Reflux;	52%

: 2162-98-3
1,10-dichlorodecane

: 1076-22-8
3-methylxanthine

: 125663-72-1
1,7-Bis(ω-chlorodecyl)-3-methyl-xanthine

Conditions

Conditions	Yield
With sodium hydroxide In N,N-dimethyl-formamide at 85 - 105℃;	51%

1,10-Dichlorodecane Specification

The CAS register number of 1,10-Dichlorodecane is 2162-98-3. It also can be called as Decane, 1,10-dichloro- and the IUPAC name about this chemical is 1,10-dichlorodecane. The molecular formula about this chemical is C₁₀H₂₀Cl₂and the molecular weight is 211.17. It belongs to the following product categories which include Building blocks; Alpha,omega-Dichloroalkanes; Alpha,omega-Bifunctional Alkanes; Monofunctional & Alpha,omega-Bifunctional Alkanes; Alkyl; Halogenated Hydrocarbons; Organic Building Blocks and so on. This chemical can be obtained by thionyl chloride chlorination of Sebacic alcohol.

Physical properties about 1,10-Dichlorodecane are: (1)ACD/LogP: 5.43; (2)# of Rule of 5 Violations: 1; (3)ACD/LogD (pH 5.5): 5.43; (4)ACD/LogD (pH 7.4): 5.43; (5)ACD/BCF (pH 5.5): 7935.91; (6)ACD/BCF (pH 7.4): 7935.91; (7)ACD/KOC (pH 5.5): 21523.95; (8)ACD/KOC (pH 7.4): 21523.95; (9)#Freely Rotating Bonds: 9; (10)Index of Refraction: 1.449; (11)Molar Refractivity: 58.07 cm³; (12)Molar Volume: 216.3 cm³; (13)Polarizability: 23.02x10^-24cm³; (14)Surface Tension: 30.1 dyne/cm; (15)Enthalpy of Vaporization: 50.23 kJ/mol; (16)Boiling Point: 284.3 °C at 760 mmHg; (17)Vapour Pressure: 0.00515 mmHg at 25°C.

Preparation: this chemical can be prepared by 1,10-Bis-chlorformyloxy-decan. This reaction will need reagent DMF. The reaction temperature is 130 - 140 ℃. The yield is about 97%.

Uses of 1,10-Dichlorodecane: it can be used to produce 1-chloro-10-phenoxydecane with phenol at heating. This reaction will need reagent tetrabutylammonium hydrogen sulfate, 3 M aq. NaOH with reaction time of 16 hours. The yield is about 69%.

When you are using this chemical, please be cautious about it as the following:
This chemical is very toxic to aquatic organisms, may cause long-term adverse effects in the aquatic environment. It is irritating to eyes, respiratory system and skin. This material and its container must be disposed of as hazardous waste. If you want to use it, please avoid release to the environment and refer to special instructions / safety data sheets. When you are using it, wear suitable gloves and eye/face protection. After contact with skin, please wash immediately with plenty of soap-suds. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.

You can still convert the following datas into molecular structure:
(1)SMILES: ClCCCCCCCCCCCl
(2)InChI: InChI=1/C10H20Cl2/c11-9-7-5-3-1-2-4-6-8-10-12/h1-10H2
(3)InChIKey: RBBNTRDPSVZESY-UHFFFAOYAX
(4)Std. InChI: InChI=1S/C10H20Cl2/c11-9-7-5-3-1-2-4-6-8-10-12/h1-10H2
(5)Std. InChIKey: RBBNTRDPSVZESY-UHFFFAOYSA-N

Product Name

1,10-Dichlorodecane

Synthetic route

1,10-Dichlorodecane Specification

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