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pentan-1-ol
2-propylheptan-1-ol
Conditions | Yield |
---|---|
With dichloro(pentamethylcyclopentadienyl) iridium; potassium tert-butylate; 1,7-Octadiene In para-xylene at 120℃; for 4h; Guerbet reaction; | 71% |
2-pentyl-pent-4-en-1-ol
2-propylheptan-1-ol
Conditions | Yield |
---|---|
With ethanol; platinum Hydrogenation; dextrorotatory form of 4-oxymethyl-nonane; |
Conditions | Yield |
---|---|
With copper |
2-propyl-1-heptene
2-propylheptan-1-ol
Conditions | Yield |
---|---|
(i) NaBH4, AlCl3, diglyme, (ii) aq. NaOH, aq. H2O2; Multistep reaction; |
Conditions | Yield |
---|---|
With nickel |
2-propylheptan-1-ol
Conditions | Yield |
---|---|
With air at 500℃; for 0.0277778h; Formation of xenobiotics; |
nonan-4-one
2-propylheptan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (i) NaNH2, liq. NH3, (ii) /BRN= 1743603/, benzene 2: (i) NaBH4, AlCl3, diglyme, (ii) aq. NaOH, aq. H2O2 View Scheme |
A
2-propylheptan-1-ol
B
2-propyl-1-heptene
C
2-propylheptyl acrylate
D
2-propyleheptyl methacrylate
Conditions | Yield |
---|---|
at 450℃; Pyrolysis; |
A
2-propylheptan-1-ol
B
methane
C
carbon dioxide
D
carbon monoxide
E
2-propylheptyl acrylate
F
2-propyleheptyl methacrylate
Conditions | Yield |
---|---|
at 550℃; Pyrolysis; |
A
2-propylheptan-1-ol
B
2-propyl-1-heptene
C
2-propylheptyl acrylate
Conditions | Yield |
---|---|
at 350℃; Pyrolysis; |
2-propylheptenal
2-propylheptan-1-ol
Conditions | Yield |
---|---|
With hydrogen; Ru/Al2O3 at 180℃; under 18751.9 Torr; Product distribution / selectivity; |
Conditions | Yield |
---|---|
With hydrogen at 200℃; under 22502.3 Torr; for 6h; Catalytic behavior; Reagent/catalyst; Autoclave; | |
Stage #1: pentanal at 200℃; for 1.5h; Aldol Condensation; Autoclave; Inert atmosphere; Stage #2: With hydrogen under 30003 Torr; for 8h; Catalytic behavior; Pressure; Temperature; Autoclave; | |
With hydrogen at 200℃; under 22502.3 Torr; for 6h; Reagent/catalyst; Autoclave; |
pentanal
A
2-propylheptan-1-ol
B
pentan-1-ol
C
2-propylheptenal
D
2-(n-propyl)-heptanal
Conditions | Yield |
---|---|
With hydrogen at 200℃; under 22502.3 Torr; for 6h; Autoclave; | |
With hydrogen at 200℃; under 22502.3 Torr; for 6h; Autoclave; |
pentanal
A
2-propylheptan-1-ol
B
pentan-1-ol
C
2-(n-propyl)-heptanal
Conditions | Yield |
---|---|
Stage #1: pentanal at 190℃; for 1.5h; Aldol Condensation; Autoclave; Inert atmosphere; Stage #2: With hydrogen under 15001.5 Torr; for 6h; Pressure; Autoclave; | |
With hydrogen at 200℃; under 22502.3 Torr; for 6h; Autoclave; |
pentanal
butyraldehyde
A
2-propylheptan-1-ol
B
2-Ethylhexyl alcohol
C
2-propylhexanol
D
2-ethylheptanol
Conditions | Yield |
---|---|
Stage #1: pentanal; butyraldehyde With sodium hydroxide In water at 20 - 130℃; for 3.25h; Stage #2: With hydrogen In water |
2-propylheptan-1-ol
acrylic acid methyl ester
2-propylheptyl acrylate
Conditions | Yield |
---|---|
With sodium methylate; dimethyltin dichloride; 4-methoxy-phenol In methanol; cyclohexane at 86 - 114℃; Solvent; Large scale; | 99.6% |
Conditions | Yield |
---|---|
With dimethylphosphinic acid; toluene-4-sulfonic acid; 4-methoxy-phenol; copper dichloride In cyclohexane; water at 85 - 99℃; for 5h; | 99% |
With methanesulfonic acid; hypophosphorous acid; 4-methoxy-phenol; copper dichloride In cyclohexane; water at 60 - 75℃; for 2h; Reflux; | 97% |
With methanesulfonic acid In water at 120℃; Industrial scale; |
2-propylheptan-1-ol
benzene-1,2-dicarboxylic acid
di(2-propylheptyl) phthalate
Conditions | Yield |
---|---|
With titanium(IV) isopropylate at 170 - 220℃; under 760.051 Torr; for 4.5h; Inert atmosphere; Large scale; | 99% |
In 5,5-dimethyl-1,3-cyclohexadiene at 140℃; for 6h; Reagent/catalyst; Solvent; Temperature; |
2-propylheptan-1-ol
Conditions | Yield |
---|---|
With sulfuric acid; hydrogen bromide at 109.84℃; for 3.5h; | 95% |
2-propylheptan-1-ol
trifluoromethylsulfonic anhydride
2-propyl-1-heptyl triflate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 0.333333h; | 94.1% |
In dichloromethane at 20℃; for 0.333333h; | 94.1% |
In dichloromethane at 20℃; for 0.333333h; |
2-propylheptan-1-ol
2-propyl-1-heptyl triflate
Conditions | Yield |
---|---|
With trifluoromethanesulfonic acid anhydride In dichloromethane | 94.1% |
With trifluoromethanesulfonic acid anhydride In dichloromethane | 94.1% |
2-propylheptan-1-ol
Conditions | Yield |
---|---|
With tetrabutoxytitanium; trichlorophosphate at 60 - 80℃; under 600.06 - 750.075 Torr; for 5h; Reagent/catalyst; Pressure; Green chemistry; | 92.5% |
2-propylheptan-1-ol
dimethyl 2,5-dimethylhexanedioate
Conditions | Yield |
---|---|
With sulfuric acid at 140℃; for 2h; | 66.7% |
Conditions | Yield |
---|---|
Stage #1: 2-propylheptan-1-ol With boron trifluoride diethyl etherate at 20 - 50℃; Stage #2: epichlorohydrin at 50℃; for 4.5h; | 60% |
With tin(IV) chloride at 90℃; for 19h; | |
boron trifluoride diethyl etherate at 50℃; for 4.5h; Neat (no solvent); | |
With tin(ll) chloride at 90℃; for 19h; |
2-propylheptan-1-ol
furan-2,5-dicarboxylic acid
Conditions | Yield |
---|---|
With sulfuric acid In water; toluene Reflux; | 58% |
2-propylheptan-1-ol
Conditions | Yield |
---|---|
In tetrahydrofuran; n-heptane at 100 - 126℃; for 22h; | 58% |
Conditions | Yield |
---|---|
With sodium hydrogen sulfate In toluene at 130℃; for 19h; Inert atmosphere; Schlenk technique; | 55.4% |
2-propylheptan-1-ol
Conditions | Yield |
---|---|
With potassium permanganate; sulfuric acid und Behandeln des Reaktionsprodukts mit Thionylchlorid; |
2-propylheptan-1-ol
bis-(2-propyl-heptyloxy)-disulfane
Conditions | Yield |
---|---|
With disulfur dichloride; triethylamine In dichloromethane at 5 - 15℃; |
Conditions | Yield |
---|---|
dextrorotatory form of 4-oxymethyl-nonane; |
2-propylheptan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 94.1 percent / CH2Cl2 / 0.33 h / 20 °C 2: CH2Cl2 / 12 h / 20 °C View Scheme |
2-propylheptan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 94.1 percent / CH2Cl2 / 0.33 h / 20 °C 2: CH2Cl2 / 4 h / 20 °C View Scheme |
2-propylheptan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: CH2Cl2 / 0.33 h / 20 °C 2.1: CH2Cl2 / 12 h / 20 °C 2.2: 66.9 percent / sodium methoxide / methanol; CH2Cl2 / 0.17 h / 20 °C View Scheme |
2-propylheptan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: CH2Cl2 / 0.33 h / 20 °C 2.1: CH2Cl2 / 4 h / 20 °C 2.2: 65.7 percent / sodium methoxide / methanol; CH2Cl2 / 0.17 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
boron trifluoride diethyl etherate In xylene at 80℃; for 5h; |
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