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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

Phosphorodithioic acid,O,O-diethyl ester, ammonium salt (1:1)

Cas:1068-22-0

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

O,O-Diethylphosphorodithioic acid ammonium salt

Cas:1068-22-0

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 1068-22-0 with best quality

Cas:1068-22-0

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Phosphorodithioic acid,O,O-diethyl ester, ammonium salt (1:1)

Cas:1068-22-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

O,O-Diethyl Dithiophosphate AMMoniuM Salt CAS:1068-22-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high

O,O-Diethyl Dithiophosphate AMMoniuM Salt CAS:1068-22-0

Cas:1068-22-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Phosphorodithioic acid,O,O-diethyl ester, ammonium salt (1:1)

Cas:1068-22-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Phosphorodithioic acid,O,O-diethyl ester, ammonium salt (1:1)

Cas:1068-22-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE

Cas:1068-22-0

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Phosphorodithioic acid,O,O-diethyl ester, ammonium salt (1:1)

Cas:1068-22-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

O,O-Diethyl Dithiophosphate Ammonium Salt

Cas:1068-22-0

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providing h

Factory Supply Diethyl dithiophosphate, ammonium salt

Cas:1068-22-0

Min.Order:0

Negotiable

Type:Other

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE

Cas:1068-22-0

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

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Henan Tianfu Chemical Co., Ltd.

Product Name: AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE Synonyms: AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE;AMMONIUM-O,O-DIETHYL PHOSPHORODITHIATE;AMMONIUM DIETHYLDITHIOPHOSPHATE;DIETHYL DITHIOPHOSPHATE, AMMONIUM SALT;ammonium,o,o-diethylphosphorodithioate;a

1068-22-0---AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE

Cas:1068-22-0

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE

Cas:1068-22-0

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE

Cas:1068-22-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE

Cas:1068-22-0

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE

Cas:1068-22-0

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE

Cas:1068-22-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Antimex Chemical Limied

Phosphorodithioic acid,O,O-diethyl ester, ammonium salt (1:1)Appearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:It is an important raw material and intermediate used in Organic Synth

Phosphorodithioic acid,O,O-diethyl ester, ammonium salt (1:1)

Cas:1068-22-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Langyou International Trading Co., Ltd

AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE Application:AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE

AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE

Cas:1068-22-0

Min.Order:0

Negotiable

Type:Other

inquiry

Guangdong Juda Chemical Industrial Co.,Limited

Appearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China

AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE CAS No.1068-22-0

Cas:1068-22-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

BOC Sciences

We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as primary a

Diethyl dithiophosphate, ammonium salt

Cas:1068-22-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Changchun Artel lmport and Export trade company

Supply top quality products with a reasonable price Application:api

1068-22-0

Cas:1068-22-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

Phosphorodithioic acid,O,O-diethyl ester, ammonium salt (1:1) cas 1068-22-0Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE

Cas:1068-22-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou ZeErRui Chemical Co., Ltd.

Hangzhou ZeErRui Chemical Co., Ltd. is focused on customization, research and development and production of APIs and advanced intermediates, which can effectively compensate for the deficiencies of traditional CRO and CMO. Priority of high-tech barri

AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE

Cas:1068-22-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Newgreat Chemical Co., Ltd

Wuhan Xinweiye Chemical Co., Ltd. is mainly engaged in the process development and production of customized synthesis and pharmaceutical intermediates. We have professional researchers in organic synthesis, analytical chemistry and production process

AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE

Cas:1068-22-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan Longxianng Runhui Trading Co.,Ltd

AMMONIUM O,O-DIETHYLDITHIOPHOSPHATEAppearance:as detailed Storage:Room temperature Package:as required Application:1068-22-0 Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by sea LCL/F

AMMONIUM O,O-DIETHYLDITHIOPHOSPHATE

Cas:1068-22-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Chinqesen Biotechnology Co., Ltd.

Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

1068-22-0

Cas:1068-22-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Chemlyte Solutions

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

kejunlin

Cas:1068-22-0

Min.Order:0

Negotiable

Type:Other

inquiry

Synthetic route

{Mo2(N(C6H4CH3))2(S2P(OC2H5)2)2S(O2CCH3)(SNH2)}

{Mo2(N(C6H4CH3))2(S2P(OC2H5)2)2S(O2CCH3)(SNH2)}

O,O-Diethyl hydrogen phosphorodithioate
298-06-6

O,O-Diethyl hydrogen phosphorodithioate

A

ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

B

{Mo2(N(C6H4CH3))2(S2P(OC2H5)2)2S(O2CCH3)(S2PS(OC2H5)2)}

{Mo2(N(C6H4CH3))2(S2P(OC2H5)2)2S(O2CCH3)(S2PS(OC2H5)2)}

Conditions
ConditionsYield
In chloroform The Mo-compd. in CHCl3 is treated with (EtO)2PS2H and stirred 30 min.; Addn. of C6H6, centrifugation and decantation left the ammonium compd., which is further rinsed three times with C6H6, each time followed by centrifugation and decantation, and then dried.;A 87%
B n/a
{Mo2(N(C6H4CH3))2(S2P(OC2H5)2)2S(O2CCH3)(SNH2)}

{Mo2(N(C6H4CH3))2(S2P(OC2H5)2)2S(O2CCH3)(SNH2)}

O,O-Diethyl hydrogen phosphorodithioate
298-06-6

O,O-Diethyl hydrogen phosphorodithioate

A

bis(diethoxyphosphoryl)disulphide
2901-90-8

bis(diethoxyphosphoryl)disulphide

B

ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

C

{Mo(NTo)(S2P(OEt)2)(μ3-S)}4

{Mo(NTo)(S2P(OEt)2)(μ3-S)}4

Conditions
ConditionsYield
In chloroform-d1 byproducts: acetic acid; To the Mo-compd. in CDCl3 is added (EtO)2PS2H, causing rapid darkening.; Pptn. of colorless crystals; (31)P-NMR and (1)H-NMR spectroscopy;
tetrafluoroboric acid diethyl ether
67969-82-8

tetrafluoroboric acid diethyl ether

ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

[(η(5)-indenyl)Mo(η(3)-C3H5)(CO)2]

[(η(5)-indenyl)Mo(η(3)-C3H5)(CO)2]

(η(5)-indenyl)Mo(CO)2(κ(2)-S2P(OEt))
207131-93-9

(η(5)-indenyl)Mo(CO)2(κ(2)-S2P(OEt))

Conditions
ConditionsYield
In dichloromethane Ar-atmosphere; stirring soln. of equimolar amts. of Mo-complex and HBF4 for 10 min, addn. of excess of (EtO)2PS2NH4, stirring for 10 h; filtration, evapn., extn. (hexane); elem. anal.;98%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

zirconium(IV) chloride
10026-11-6

zirconium(IV) chloride

Zr(S2P(OC2H5)2)4

Zr(S2P(OC2H5)2)4

Conditions
ConditionsYield
In dichloromethane byproducts: NH4Cl; addn. of ZrCl4 in CH2Cl2 to a suspn. of the dithiophosphate in CH2Cl2 (1:4 molar ratio) under exclusion of moisture, refluxing (constant stirring, 6 h); filtration from pptd. NH4Cl4, removal of solvent (reduced pressure), washing (n-hexane), drying; elem. anal.;94%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

trichlorodimethoxymolybdenum(V)
51325-41-8

trichlorodimethoxymolybdenum(V)

dichlorodimethoxymolybdenum(V) O,O'-diethylthiophosphate

dichlorodimethoxymolybdenum(V) O,O'-diethylthiophosphate

Conditions
ConditionsYield
In benzene byproducts: NH4Cl; exclusion of moisture, stirring equimolar amts. of trichloromethoxymolybdenum(V) and NH4S2P(OC2H5)2 for 2 h at room temp., change of colour from brown to green; filtering off pptd. NH4Cl, removing the solvent under reduced pressure at room temp., elem. anal.;93.3%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

zinc(II) sulfate
7733-02-0

zinc(II) sulfate

bis(O,O-diethyldithiophosphato)zinc
7268-60-2, 46946-10-5

bis(O,O-diethyldithiophosphato)zinc

Conditions
ConditionsYield
In water mixed; filtered; extd. (diethyl ether); dried (over MgSO4); evapd.; recrystd. (light petroleum); elem. anal.;90%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

ethylphenyltin(IV) dichloride
15649-27-1

ethylphenyltin(IV) dichloride

(C2H5C6H5Sn(SSP(OC2H5)2)2)
116178-60-0

(C2H5C6H5Sn(SSP(OC2H5)2)2)

Conditions
ConditionsYield
In hexane byproducts: NH4Cl; to a susp. of NH4SSP(OEt)2 in hexane a soln. of EtPhSnCl2 was added andthe reaction mixt. was allowed to stir for 2-3 h at room temp; NH4Cl formed during the reaction was filtered off, filtrate was concd. under vac., dissolving in anhydrous hexane, filtration through florisil under N2; elem. anal.;90%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

dimethyltin dichloride
753-73-1

dimethyltin dichloride

(CH3)2SnCl(SSP(OC2H5)2)
116178-66-6

(CH3)2SnCl(SSP(OC2H5)2)

Conditions
ConditionsYield
In hexane byproducts: NH4Cl; to a susp. of NH4SSP(OEt)2 in hexane a soln. of Me2SnCl2 was added in 1:1 stoich. and the reaction mixt. was allowed to stir for 2-3 h at roomtemp; NH4Cl formed during the reaction was filtered off, filtrate was concd. under vac., elem. anal.;90%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

methylphenyltin(IV) dichloride
15649-26-0

methylphenyltin(IV) dichloride

(CH3C6H5Sn(SSP(OC2H5)2)2)
116178-59-7

(CH3C6H5Sn(SSP(OC2H5)2)2)

Conditions
ConditionsYield
In hexane byproducts: NH4Cl; to a susp. of NH4SSP(OEt)2 in hexane a soln. of MePhSnCl2 was added andthe reaction mixt. was allowed to stir for 2-3 h at room temp; NH4Cl formed during the reaction was filtered off, filtrate was concd. under vac., dissolving in anhydrous hexane, filtration through folrisil under N2; elem. anal.;89%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

(C6H5C(NOH)C(NO)C6H5)SbCl2

(C6H5C(NOH)C(NO)C6H5)SbCl2

Sb((C6H5)2C2N2(OH)O)(S2P(OC2H5)2)2

Sb((C6H5)2C2N2(OH)O)(S2P(OC2H5)2)2

Conditions
ConditionsYield
In benzene byproducts: NH4Cl; moisture-free atmosphere; stirring with slight heating (45 - 50°C, 3 - 4 h); filtration, solvent removal (reduced pressure), recrystn. (benzene/petroleum ether = 1 : 1); elem. anal.;88%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

MoI2(CO)3(MeCN)2
102349-56-4

MoI2(CO)3(MeCN)2

1,2-bis-(diphenylphosphino)ethane
1663-45-2

1,2-bis-(diphenylphosphino)ethane

Mo(CO)(S2P(OC2H5)2)2(P(C6H5)2CH2)2

Mo(CO)(S2P(OC2H5)2)2(P(C6H5)2CH2)2

Conditions
ConditionsYield
In dichloromethane byproducts: CO; MoI2(CO)3(NCMe)2 dissolved in CH2Cl2; solid NH4(S2P(OEt)2) added with stirring; after 30 min ppt. filtered off; to filtrate Ph2PCH2CH2PPh2 (ratio 1:1) added; soln. stirred for 30 min; concd.; hexane added; cooled down (-20°C) overnight; elem. anal.;87%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

MoI2(CO)3(MeCN)2
102349-56-4

MoI2(CO)3(MeCN)2

1,2-bis-(diphenylphosphino)ethane
1663-45-2

1,2-bis-(diphenylphosphino)ethane

[Mo(CO)2(S2P(OC2H5)2)2](μ-(C6H5)2PCH2CH2P(C6H5)2)

[Mo(CO)2(S2P(OC2H5)2)2](μ-(C6H5)2PCH2CH2P(C6H5)2)

Conditions
ConditionsYield
In dichloromethane byproducts: CO; MoI2(CO)3(NCMe)2 dissolved in CH2Cl2; solid NH4(S2P(OEt)2) added with stirring; after 30 min ppt. filtered off; to filtrate Ph2PCH2CH2PPh2 added(ratio 2:1); soln. stirred for 30 min; concd.; hexane added; cooled down (-20°C) overnight; elem. anal.;87%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

[Pd(PPh3)Cl]2(μ,η2-SCNMe2)2
79969-97-4, 581106-72-1

[Pd(PPh3)Cl]2(μ,η2-SCNMe2)2

[Pd(triphenylphosphine)(η1-CSNMe2)(η2-diethyldithiophosphate)]
742078-08-6

[Pd(triphenylphosphine)(η1-CSNMe2)(η2-diethyldithiophosphate)]

Conditions
ConditionsYield
In CH2Cl2 under N2; Pd complex treated with NH4(S2P(OEt)2) in CH2Cl2 at ambient temp.;87%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

((Pd(μ-I)((CH2)2S(O)Me))2)

((Pd(μ-I)((CH2)2S(O)Me))2)

Pd{(CH2)2(SO)(CH3)}{S2P(OC2H5)2}

Pd{(CH2)2(SO)(CH3)}{S2P(OC2H5)2}

Conditions
ConditionsYield
In dichloromethane Addn. of org. compd. to suspn. of Pd-complex (CH2Cl2) using n-Bu4NI as phase transfer catalyst and stirring. The yellow suspn. is dissolved within 5 min.;85%
In dichloromethane Addn. of org. compd. to suspn. of Pd-complex (CH2Cl2). After stirring of mixt. (10 min), the yellow suspn. comes into soln. and some white solid is pptd. Further stirring for 1 h.; Washing 3 times with H2O, removal of solvent, recrystn. of residue from n-hexane/CH2Cl2, elem. anal.;63%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

dichlorodiethylstannane
866-55-7

dichlorodiethylstannane

(C2H5)2SnCl(SSP(OC2H5)2)
116178-67-7

(C2H5)2SnCl(SSP(OC2H5)2)

Conditions
ConditionsYield
In hexane byproducts: NH4Cl; to a susp. of NH4SSP(OEt)2 in hexane a soln. of Et2SnCl2 was added in 1:1 stoich. and the reaction mixt. was allowed to stir for 2-3 h at roomtemp; NH4Cl formed during the reaction was filtered off, filtrate was concd. under vac., elem. anal.;85%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

chlorotriphenylgermane
1626-24-0

chlorotriphenylgermane

triphenyl(O,O'-diethyldithiophosphato)germanium
113557-04-3

triphenyl(O,O'-diethyldithiophosphato)germanium

Conditions
ConditionsYield
In benzene byproducts: NH4Cl; soln. of 1.0 mmol of Ph3GeCl and C6H6 added to 1.2 mmol of dry (EtO)2PS(S)NH4 under dry N2, warmed up to 20°C, stirred for 4 h; NH4Cl filtered off, filtrate slowly evapd. in vac.; elem. anal.;85%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

dibutyltin chloride
683-18-1

dibutyltin chloride

dibutyltin(IV) diethyldithiophosphate
21768-68-3

dibutyltin(IV) diethyldithiophosphate

Conditions
ConditionsYield
In benzene byproducts: NH4Cl; to suspn. of ammonium diethyldithiophosphate is added dialkyltindichloride in benzene, exothermic reaction, white ppt. separates at room temp.,refluxing for 0.5 h; ppt. is filtered off, benzene is removed under reduced pressure, distn.(100-102°C/0.01 mm), elem. anal.;85%
In benzene byproducts: NH4Cl; to suspn. of ammonium diethyldithiophosphate is added dialkyltindichloride in benzene, exothermic reaction, white ppt. separates at room temp.,refluxing for 0.5 h; ppt. is filtered off, benzene is removed under reduced pressure, distn., elem. anal.;80%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

cyclopentadienyltrichloromolybdenum(IV)

cyclopentadienyltrichloromolybdenum(IV)

[Mo(η(5)-cyclopentadienyl)Cl2(O,O'-diethyldithiophosphate)]
504408-08-6

[Mo(η(5)-cyclopentadienyl)Cl2(O,O'-diethyldithiophosphate)]

Conditions
ConditionsYield
In dichloromethane under N2 atm. using Schlenk techniques; to suspn. of Mo complex in CH2Cl2 added org. salt at room temp.; stirred for 10 h; mixt. filtered; filtrate concd. to dryness; residue washed (Et2O); elem.anal.;85%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

trichloro(2,2'-bipyridine)ruthenium
69141-04-4

trichloro(2,2'-bipyridine)ruthenium

Ru((C5H4N)2)(SP(S)(OC2H5)2)2
220229-56-1

Ru((C5H4N)2)(SP(S)(OC2H5)2)2

Conditions
ConditionsYield
In methanol elem. anal.;85%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

di[(7,8-benzoquinolyl)(μ-hydroxo)palladium(II)]

di[(7,8-benzoquinolyl)(μ-hydroxo)palladium(II)]

(O,O'-diethyldithiophosphate)(7,8-benzoquinolyl)palladium(II)

(O,O'-diethyldithiophosphate)(7,8-benzoquinolyl)palladium(II)

Conditions
ConditionsYield
In dichloromethane suspn. of Pd complex and protic ligand (1:2) in CH2Cl2 stirred at room temp. for 30 min; concd.(vac.), pptd.(Et2O), filtered, washed (H2O, Et2O), dried (air), recrystd.(CH2Cl2/Et2O), elem. anal.;84%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

MoI2(CO)3(MeCN)2
102349-56-4

MoI2(CO)3(MeCN)2

triphenylphosphine
603-35-0

triphenylphosphine

Mo(CO)2(S2P(OC2H5)2)2(P(C6H5)3)
63339-43-5

Mo(CO)2(S2P(OC2H5)2)2(P(C6H5)3)

Conditions
ConditionsYield
In dichloromethane byproducts: CO; MoI2(CO)3(NCMe)2 dissolved in CH2Cl2; solid NH4(S2P(OEt)2) added with stirring; after 30 min ppt. filtered off; to filtrate PPh3 added; soln. stirred for 30 min; concd.; hexane added; cooled down (-20°C) overnight; elem. anal.;83%
sodium borodeuteride

sodium borodeuteride

ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

tetrakis(actonitrile)copper(I) hexafluorophosphate
64443-05-6

tetrakis(actonitrile)copper(I) hexafluorophosphate

[Cu4(μ4-D)(μ3-Cu)4(S2P(O(i)Pr)2)6](PF6)*5H2O

[Cu4(μ4-D)(μ3-Cu)4(S2P(O(i)Pr)2)6](PF6)*5H2O

Conditions
ConditionsYield
In tetrahydrofuran under inert atm. soln. Cu(MeCN)4PF6, NH4(S2P(O-i-Pr)2), and NaBD4 in THFwere stirred at room temp. for 30 min; soln. was filtered and evapd. to dryness in vacuo, residue was washed with water and dried in vacuo; elem. anal.;83%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

tetrakis(actonitrile)copper(I) hexafluorophosphate
64443-05-6

tetrakis(actonitrile)copper(I) hexafluorophosphate

[Cu8(S2P(OEt)2)6](PF6)2

[Cu8(S2P(OEt)2)6](PF6)2

Conditions
ConditionsYield
In acetone byproducts: NH4PF6; under inert atm. soln. Cu(MeCN)4PF6 and NH4(S2P(OEt)2) in acetone was stirred at room temp. for 1 h; soln. was filtered and evapd. to dryness in vacuo, residue was washed with water; elem. anal.;83%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

diphenyltin(IV) dichloride
1135-99-5

diphenyltin(IV) dichloride

(C6H5)2SnCl(SSP(OC2H5)2)
116178-70-2

(C6H5)2SnCl(SSP(OC2H5)2)

Conditions
ConditionsYield
In hexane byproducts: NH4Cl; to a susp. of NH4SSP(OEt)2 in hexane a soln. of Ph2SnCl2 was added in 1:1 stoich. and the reaction mixt. was allowed to stir for 2-3 h at roomtemp; NH4Cl formed during the reaction was filtered off, filtrate was concd. under vac., elem. anal.;82%
copper(ll) sulfate pentahydrate

copper(ll) sulfate pentahydrate

ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

copper(I) diethyldithiophosphate

copper(I) diethyldithiophosphate

Conditions
ConditionsYield
In water A soln. of CuSO4 in H2O was added NH4S2P(OR)2 in H2O; brown ppt. was extd. with CH2Cl2, evapd., MeOH was added;; ppt. was recrystd. from CH2Cl2-C6H5CH3; elem. anal.;;82%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

dichlorodimethylgermanium
1529-48-2

dichlorodimethylgermanium

dimethylbis(O,O'-diethyldithiophosphato)germanium
113557-02-1

dimethylbis(O,O'-diethyldithiophosphato)germanium

Conditions
ConditionsYield
In benzene byproducts: NH4Cl; soln. of 1.3 mmol of Me2GeCl2 and C6H6 added to 2.8 mmol of dry (EtO)2PS(S)NH4 occasionally cooled to -10°C under dry N2, warmed up to 10°C, stirred for 4 h; NH4Cl filtered off, filtrate slowly evapd. in vac.; elem. anal.;82%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

[W(acetonitrile)2(η3-allyl)(CO)2Br]
62651-74-5

[W(acetonitrile)2(η3-allyl)(CO)2Br]

[W(acetonitrile)(η3-allyl)(CO)2(η2-diethyldithiophosphato)]
520505-25-3

[W(acetonitrile)(η3-allyl)(CO)2(η2-diethyldithiophosphato)]

Conditions
ConditionsYield
In dichloromethane under N2; CH2Cl2 added to equimolar mixt. of W complex and ligand at ambient temp.; stirred for 10 min; solvent removed in vac.; abstracted with Et2O; n-hexane added; filtered;ppt. washed with cold n-hexane; dried in vac.; recrystd. from cold n-he xane-Et2O; elem. anal.;82%
tetrahydrofuran
109-99-9

tetrahydrofuran

sodium tetrahydroborate
16940-66-2

sodium tetrahydroborate

ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

tetrakis(actonitrile)copper(I) hexafluorophosphate
64443-05-6

tetrakis(actonitrile)copper(I) hexafluorophosphate

[Cu4(μ4-H)(μ3-Cu)4(S2P(OEt)2)6](PF6)*0.5THF

[Cu4(μ4-H)(μ3-Cu)4(S2P(OEt)2)6](PF6)*0.5THF

Conditions
ConditionsYield
In tetrahydrofuran under inert atm. soln. Cu(MeCN)4PF6, NH4(S2P(OEt)2), and NaBH4 in THF were stirred at room temp. for 30 min; soln. was filtered and evapd. to dryness in vacuo, residue was washed with water and dried in vacuo; elem. anal.;82%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer

dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer

(C5(CH3)5)RhCl(S2P(OC2H5)2)
243845-44-5

(C5(CH3)5)RhCl(S2P(OC2H5)2)

Conditions
ConditionsYield
In dichloromethane byproducts: NH4Cl; N2-atmosphere; stoich. amts., stirring (room temp., 3 h); filtration off of NH4Cl, concn. (vac.), recrystn. (CH2Cl2/hexane); elem. anal.;81%
ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

MoI2(CO)3(MeCN)2
102349-56-4

MoI2(CO)3(MeCN)2

1,2-bis-(diphenylphosphino)ethane
1663-45-2

1,2-bis-(diphenylphosphino)ethane

MoI(CO)2((C6H5)2PCH2)2(S2P(OC2H5)2)
404579-79-9

MoI(CO)2((C6H5)2PCH2)2(S2P(OC2H5)2)

Conditions
ConditionsYield
In dichloromethane MoI2(CO)3(NCMe)2 dissolved in CH2Cl2; NH4(S2P(OEt)2) added with stirring; after 30 min mixt. filtered; Ph2PCH2CH2PPh2 added to filtrate; soln. stirred for 30 min; hexane added; mixt. kept at 0.°C for 3 ds; elem. anal.;81%
sodium tetrahydroborate
16940-66-2

sodium tetrahydroborate

ammonium O,O-diethyldithiophosphate
1068-22-0

ammonium O,O-diethyldithiophosphate

tetrakis(acetonitrile)copper(I) hexafluorophosphate

tetrakis(acetonitrile)copper(I) hexafluorophosphate

6C4H10O2PS2(1-)*7Cu(1+)*H(1-)

6C4H10O2PS2(1-)*7Cu(1+)*H(1-)

Conditions
ConditionsYield
In chloroform at 20℃; for 1h; Inert atmosphere; Schlenk technique;81%

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