Product name: 15S-(±)-Cloprostenol Cas No:40665-93-8 Assay: 98%min Hangzhou Verychem Science And Technology Co. Ltd. was set up in year 2004, it’s a young but fast growing company. In the twelve years hi
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inquiryName: (1S,3R,6S)-Ethyl Octahydrocyclopenta[c] pyrrole-1-carboxylate HCl Synonyms: (1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride CAS:1147103-42-1 MF: C10H17NO2 Appearance: white powder Storage:Store in cool and dr
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryhigh purity, manufacturer Application:Intermediate
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inquiryOur clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
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inquiry(1S,3aR,6aS)-2-(tert-butoxycarbonyl)octahydrocyclo-penta[c]pyrrole-1-carboxylic acid
ethanol
C10H17NO2*ClH
Conditions | Yield |
---|---|
With thionyl chloride for 2h; Reflux; | 71% |
(1S,3aR,6aS)-hexahydro-cyclopenta[c]pyrrole-1,2-dicarboxylic acid 2-tert-butyl ester ethyl ester
C10H17NO2*ClH
Conditions | Yield |
---|---|
With hydrogenchloride In ethyl acetate at 30 - 35℃; for 4h; Inert atmosphere; Cooling with ice; | 70% |
C10H17NO2*ClH
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: ethyl acetate / 12 h / 20 °C 2: sodium hydrogen sulfate / tert-butyl methyl ether; water 3: thionyl chloride / 2 h / Reflux View Scheme |
C10H17NO2*ClH
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: sodium hydrogensulfite / tert-butyl methyl ether; water / 2 h / 20 °C 2: 3 h / 10 °C / pH 9 3: hydrogenchloride / water; dichloromethane / 1 h 4: sodium hydroxide / dichloromethane / 10 - 20 °C / pH 8 5: ethyl acetate / 12 h / 20 °C 6: sodium hydrogen sulfate / tert-butyl methyl ether; water 7: thionyl chloride / 2 h / Reflux View Scheme |
(3aR,6aS)-octahydrocyclopenta[c]pyrrole hydrochloride
C10H17NO2*ClH
Conditions | Yield |
---|---|
Multi-step reaction with 8 steps 1: sodium hypochlorite solution / tert-butyl methyl ether / 2 h / 15 °C 2: sodium hydrogensulfite / tert-butyl methyl ether; water / 2 h / 20 °C 3: 3 h / 10 °C / pH 9 4: hydrogenchloride / water; dichloromethane / 1 h 5: sodium hydroxide / dichloromethane / 10 - 20 °C / pH 8 6: ethyl acetate / 12 h / 20 °C 7: sodium hydrogen sulfate / tert-butyl methyl ether; water 8: thionyl chloride / 2 h / Reflux View Scheme |
C10H17NO2*ClH
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 3 h / 10 °C / pH 9 2: hydrogenchloride / water; dichloromethane / 1 h 3: sodium hydroxide / dichloromethane / 10 - 20 °C / pH 8 4: ethyl acetate / 12 h / 20 °C 5: sodium hydrogen sulfate / tert-butyl methyl ether; water 6: thionyl chloride / 2 h / Reflux View Scheme |
C10H17NO2*ClH
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: hydrogenchloride / water; dichloromethane / 1 h 2: sodium hydroxide / dichloromethane / 10 - 20 °C / pH 8 3: ethyl acetate / 12 h / 20 °C 4: sodium hydrogen sulfate / tert-butyl methyl ether; water 5: thionyl chloride / 2 h / Reflux View Scheme |
C10H17NO2*ClH
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: sodium hydroxide / dichloromethane / 10 - 20 °C / pH 8 2: ethyl acetate / 12 h / 20 °C 3: sodium hydrogen sulfate / tert-butyl methyl ether; water 4: thionyl chloride / 2 h / Reflux View Scheme |
(1S,3aR,6aS)-2-(tert-butoxycarbonyl)octahydrocyclo-penta[c]pyrrole-1-carboxylic acid
ethanol
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
Conditions | Yield |
---|---|
With thionyl chloride for 2h; Reflux; | 71% |
(1S,3aR,6aS)-hexahydro-cyclopenta[c]pyrrole-1,2-dicarboxylic acid 2-tert-butyl ester ethyl ester
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In ethyl acetate at 30 - 35℃; for 4h; Inert atmosphere; Cooling with ice; | 70% |
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: ethyl acetate / 12 h / 20 °C 2: sodium hydrogen sulfate / tert-butyl methyl ether; water 3: thionyl chloride / 2 h / Reflux View Scheme |
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: sodium hydrogensulfite / tert-butyl methyl ether; water / 2 h / 20 °C 2: 3 h / 10 °C / pH 9 3: hydrogenchloride / water; dichloromethane / 1 h 4: sodium hydroxide / dichloromethane / 10 - 20 °C / pH 8 5: ethyl acetate / 12 h / 20 °C 6: sodium hydrogen sulfate / tert-butyl methyl ether; water 7: thionyl chloride / 2 h / Reflux View Scheme |
(3aR,6aS)-octahydrocyclopenta[c]pyrrole hydrochloride
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 8 steps 1: sodium hypochlorite solution / tert-butyl methyl ether / 2 h / 15 °C 2: sodium hydrogensulfite / tert-butyl methyl ether; water / 2 h / 20 °C 3: 3 h / 10 °C / pH 9 4: hydrogenchloride / water; dichloromethane / 1 h 5: sodium hydroxide / dichloromethane / 10 - 20 °C / pH 8 6: ethyl acetate / 12 h / 20 °C 7: sodium hydrogen sulfate / tert-butyl methyl ether; water 8: thionyl chloride / 2 h / Reflux View Scheme |
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 3 h / 10 °C / pH 9 2: hydrogenchloride / water; dichloromethane / 1 h 3: sodium hydroxide / dichloromethane / 10 - 20 °C / pH 8 4: ethyl acetate / 12 h / 20 °C 5: sodium hydrogen sulfate / tert-butyl methyl ether; water 6: thionyl chloride / 2 h / Reflux View Scheme |
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: hydrogenchloride / water; dichloromethane / 1 h 2: sodium hydroxide / dichloromethane / 10 - 20 °C / pH 8 3: ethyl acetate / 12 h / 20 °C 4: sodium hydrogen sulfate / tert-butyl methyl ether; water 5: thionyl chloride / 2 h / Reflux View Scheme |
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: sodium hydroxide / dichloromethane / 10 - 20 °C / pH 8 2: ethyl acetate / 12 h / 20 °C 3: sodium hydrogen sulfate / tert-butyl methyl ether; water 4: thionyl chloride / 2 h / Reflux View Scheme |
(1S,3aR,6aS)-ethyl 2-boc-4-oxooctahydrocyclopenta[c]pyrrole-1-carboxylate
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ethanol / 3 h / Reflux 2: sodium tetrahydroborate; methanol / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere 3: sodium acetate / ethanol / 5 h / Reflux 4: hydrogenchloride / ethyl acetate / 4 h / 30 - 35 °C / Inert atmosphere; Cooling with ice View Scheme |
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sodium tetrahydroborate; methanol / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere 2: sodium acetate / ethanol / 5 h / Reflux 3: hydrogenchloride / ethyl acetate / 4 h / 30 - 35 °C / Inert atmosphere; Cooling with ice View Scheme |
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium acetate / ethanol / 5 h / Reflux 2: hydrogenchloride / ethyl acetate / 4 h / 30 - 35 °C / Inert atmosphere; Cooling with ice View Scheme |
3-Ethoxycarbonylmethyl-5-(2-hydroxy-ethyl)-4-methyl-thiazol-3-ium; bromide
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: triethylamine / water; N,N-dimethyl-formamide / 16 h / 0 - 20 °C 2.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 8 h / 70 - 75 °C / Inert atmosphere 2.2: 8 h / 0 - 20 °C 3.1: ethanol / 3 h / Reflux 4.1: sodium tetrahydroborate; methanol / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere 5.1: sodium acetate / ethanol / 5 h / Reflux 6.1: hydrogenchloride / ethyl acetate / 4 h / 30 - 35 °C / Inert atmosphere; Cooling with ice View Scheme |
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 8 h / 70 - 75 °C / Inert atmosphere 1.2: 8 h / 0 - 20 °C 2.1: ethanol / 3 h / Reflux 3.1: sodium tetrahydroborate; methanol / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere 4.1: sodium acetate / ethanol / 5 h / Reflux 5.1: hydrogenchloride / ethyl acetate / 4 h / 30 - 35 °C / Inert atmosphere; Cooling with ice View Scheme |
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
(1S,3aR,6aS)-2-((S)-2-((S)-2-cyclohexyl-2-(pyrazine-2-carboxamido)acetamido)-3,3-dimethylbutanoyl)octahydrocyclopenta[c]pyrrole-1-carboxylic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diisopropyl-carbodiimide; 4-methyl-morpholine; copper dichloride / N,N-dimethyl-formamide / 5 h / 20 °C 2: sodium hydroxide; water / tetrahydrofuran / 18 h / 20 °C View Scheme |
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: diisopropyl-carbodiimide; 4-methyl-morpholine; copper dichloride / N,N-dimethyl-formamide / 5 h / 20 °C 2: sodium hydroxide; water / tetrahydrofuran / 18 h / 20 °C 3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 6 h / 20 °C / Cooling with ice View Scheme |
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
(1S,3aR,6aS)-2-((S)-2-((S)-2-cyclohexyl-2-(pyrazine-2-carboxamido)acetamido)-3,3-dimethylbutanoyl)-N-((S)-1-(cyclopropylamino)-1,2-dioxohexan-3-yl)octahydrocyclopenta[c]pyrrole-1-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: diisopropyl-carbodiimide; 4-methyl-morpholine; copper dichloride / N,N-dimethyl-formamide / 5 h / 20 °C 2: sodium hydroxide; water / tetrahydrofuran / 18 h / 20 °C 3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 6 h / 20 °C / Cooling with ice 4: sodium hydrogencarbonate; potassium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite / dichloromethane / 20 h / 20 °C / Cooling with ice View Scheme |
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
(S)-2-((S)-2-cyclohexyl-2-(pyrazine-2-carboxamido)acetamido)-3,3-dimethylbutanoic acid
(1S,3aR,6aS)-ethyl 2-((S)-2-((S)-2-cyclohexyl-2-(pyrazine-2-carboxamido)acetamido)-3,3-dimethylbutanoyl)octahydrocyclopenta[c]pyrrole-1-carboxylate
Conditions | Yield |
---|---|
With 4-methyl-morpholine; copper dichloride; diisopropyl-carbodiimide In N,N-dimethyl-formamide at 20℃; for 5h; | 98.1 mg |
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