With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:119804-96-5
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inquiryNewCan Biotech Limited was established in 2021 and is primarily engaged in the research, development, production, and sales of sugars, nucleosides, nucleotides, phosphorylated monomers, as well as next-generation antiviral and antitumor drug intermed
Cas:119804-96-5
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:119804-96-5
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou
Cas:119804-96-5
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inquiry1. Product advantages? High purity, all above 98.5%, no impurities after dissolution? We will test each batch to ensure quality? OEM and private brand services designed for free? Various cap colors available? We can also provide MT1 peptide powder2.
factory?direct?sale Application:healing drugs
Cas:119804-96-5
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inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white solid Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as primary an
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:119804-96-5
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Type:Lab/Research institutions
inquiry3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-2'-deoxy-2'-methylidenecytidine
2'-deoxy-2'-methylenecytidine
Conditions | Yield |
---|---|
With n-Bu4F In tetrahydrofuran for 1.5h; Ambient temperature; | 92% |
With tetrabutyl ammonium fluoride In tetrahydrofuran for 2h; Yield given; |
4-ethoxy-(2-deoxy-2'-methylidene-β-D-ribofuranosyl)-2-(1H)-pyrimidinone
2'-deoxy-2'-methylenecytidine
Conditions | Yield |
---|---|
With ammonia In methanol at 100℃; for 48h; | 81% |
3',5'-bis-O-tert-butyldimethylsilyl-2'-deoxy-2'-methylidenecytidine
2'-deoxy-2'-methylenecytidine
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran for 2h; Yield given; |
2'-deoxy-2'-methylenecytidine
Conditions | Yield |
---|---|
With ammonia In methanol at 20℃; |
4-etoxy-1-<2-deoxy-2-methylidene-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-2-(1H)-pyrimidinone
2'-deoxy-2'-methylenecytidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 91 percent / tetra-n-butylammonium fluoride / tetrahydrofuran 2: 81 percent / ammonia / methanol / 48 h / 100 °C View Scheme |
4-ethoxy-1-<3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-erythro-2-pentulofuranosyl>-2(1H)-pyrimidinone
2'-deoxy-2'-methylenecytidine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 41 percent 2: 91 percent / tetra-n-butylammonium fluoride / tetrahydrofuran 3: 81 percent / ammonia / methanol / 48 h / 100 °C View Scheme |
1-((6aR,8R,9aS)-2,2,4,4-tetraisopropyl-9-methylenetetrahydro-6H-furo[3,2-f][1,3,5,2,4]trioxadisilocin-8-yl)-pyrimidine-2,4(1H,3H)-dione
2'-deoxy-2'-methylenecytidine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 99 percent / POCl3, triethylamine / acetonitrile / 2 h / Ambient temperature 2: 30 percent aq. NH3 / dioxane / 12 h / Ambient temperature 3: tetrabutylammonium fluoride / tetrahydrofuran / 2 h View Scheme | |
Multi-step reaction with 3 steps 1: 77 percent / 4-chlorophenyl phosphorodichloridate, pyridine / 48 h / Ambient temperature 2: NH4OH / dioxane / Ambient temperature 3: 92 percent / n-Bu4F / tetrahydrofuran / 1.5 h / Ambient temperature View Scheme |
1-<3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-2-deoxy-2-methylidene-β-D-ribofuranosyl>-4-(1,2,4-triazol-1-yl)-1H-pyrimidin-2-one
2'-deoxy-2'-methylenecytidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 30 percent aq. NH3 / dioxane / 12 h / Ambient temperature 2: tetrabutylammonium fluoride / tetrahydrofuran / 2 h View Scheme | |
Multi-step reaction with 2 steps 1: NH4OH / dioxane / Ambient temperature 2: 92 percent / n-Bu4F / tetrahydrofuran / 1.5 h / Ambient temperature View Scheme |
1-((2R,5R)-4-((tert-butyldimethylsilyl)oxy)-5-((tert-butyldimethylsilyl)oxy)tetrahydrofuran-2-yl)pyrimidine-2,4 (1H,3H)-dione
2'-deoxy-2'-methylenecytidine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 99 percent / POCl3, triethylamine / acetonitrile / 2 h / Ambient temperature 2: 30 percent aq. NH3 / dioxane / 12 h / Ambient temperature 3: tetrabutylammonium fluoride / tetrahydrofuran / 2 h View Scheme |
1-[(2R,4S,5R)-4-(tert-Butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-3-methylene-tetrahydro-furan-2-yl]-4-[1,2,4]triazol-1-yl-1H-pyrimidin-2-one
2'-deoxy-2'-methylenecytidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 30 percent aq. NH3 / dioxane / 12 h / Ambient temperature 2: tetrabutylammonium fluoride / tetrahydrofuran / 2 h View Scheme |
2'-deoxy-2'-methylenecytidine
α-[2-(trimethylsilyl)ethoxy]-2-N-[2-(trimethylsilyl)ethoxycarbonyl]folic acid
1-(2-deoxy-2-methylene-β-D-erythro-pentofuranosyl)-4-N-[γ-[α-[2-(trimethylsilyl)ethoxy]-2-N-[2-(trimethylsilyl)ethoxycarbonyl]folyl]]cytosine
Conditions | Yield |
---|---|
With triethylamine; isobutyl chloroformate In N,N-dimethyl-formamide at 20℃; for 2h; Substitution; | 66% |
2'-deoxy-2'-methylenecytidine
n-decanoyl chloride
2'-DEOXY-2'-METHYLIDENE-N4-DECANOYLCYTIDINE
Conditions | Yield |
---|---|
With chloro-trimethyl-silane In pyridine; water | 45.6% |
chloro-trimethyl-silane
2'-deoxy-2'-methylenecytidine
Stearoyl chloride
2'-DEOXY-2'-METHYLIDENE-N4-STEAROYLCYTIDINE
Conditions | Yield |
---|---|
In pyridine; water | 39.6% |
2'-deoxy-2'-methylenecytidine
Conditions | Yield |
---|---|
With triethyl phosphate; trichlorophosphate at 5℃; for 1h; | 30% |
dipalmitoylphosphatidylcholine
2'-deoxy-2'-methylenecytidine
Conditions | Yield |
---|---|
With sodium acetate buffer; Dianion WK-20 resin (Na(1+) form); phospholipase D 1.) CHCl3, 40 deg C, 6 h; Yield given. Multistep reaction; |
2'-deoxy-2'-methylenecytidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) phospholipase D, sodium acetate buffer (pH 4.5), 2.) Dianion WK-20 resin (Na(1+) form) / 1.) CHCl3, 40 deg C, 6 h 2: aq. sodium deoxycholate, phospholipase A2, CaCl2, 3,3-dimethylglutarate-NaOH buffer (pH 7.0) / 37 °C View Scheme |
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