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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Methylaminoacetaldehyde Dimethyl Acetal supplier in China

Cas:122-07-6

Min.Order:1 Metric Ton

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Type:Manufacturers

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Hebei yanxi chemical co.,LTD.

hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm

Methylaminoacetaldehyde Dimethyl Acetal CAS NO.122-07-6

Cas:122-07-6

Min.Order:1 Metric Ton

FOB Price: $1.0 / 3.0

Type:Manufacturers

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Henan Allgreen Chemical Co.,Ltd

Good quality Good price Promptly delivery Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:intermediate Transportation:According to t

122-07-6Methylaminoacetaldehyde dimethyl acetal

Cas:122-07-6

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2,2-dimethoxyethylmethylamine

Cas:122-07-6

Min.Order:1

Negotiable

Type:Other

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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price in China. If you are looking for the product’s supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product specifica

Methylaminoacetaldehyde dimethyl acetal

Cas:122-07-6

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

(N-Methylamino)-acetaldehyde dimethylacetal

Cas:122-07-6

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

TIANFU-CHEM 122-07-6 Methylaminoacetaldehyde dimethyl acetal

Cas:122-07-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

New CAS 122-07-6 with high quality products

Cas:122-07-6

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

CAS Number 122-07-6 Product Name Methylaminoacetaldehyde Dimethyl Acetal Synonyms 2,2-dimethoxy-n-methylethanaminium; 2,2-dimeth

Methylaminoacetaldehyde dimethyl acetal

Cas:122-07-6

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Shanghai Minstar Chemical Co., Ltd

Product Name: Methylaminoacetaldehyde dimethyl acetal Synonyms: (methylamino)-acetaldehyddimethylacetal;2,2-Dimethoxyethyl(methyl)amine;2,2-dimethoxy-n-methyl-ethanamin;2,2-Dimethoxy-N-methylethanamine;Acetaldehyde, (methylamino)-, dimethyl acetal

Methylaminoacetaldehyde dimethyl acetal 122-07-6

Cas:122-07-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Ethanamine,2,2-dimethoxy-N-methyl-

Cas:122-07-6

Min.Order:1 Gram

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Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

Methylaminoacetaldehyde dimethyl acetal CAS: 122-07-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high qu

Methylaminoacetaldehyde dimethyl acetal CAS: 122-07-6

Cas:122-07-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

122-07-6 Methylaminoacetaldehyde dimethyl acetal

Cas:122-07-6

Min.Order:1 Kilogram

FOB Price: $15.0 / 50.0

Type:Trading Company

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:122-07-6

Cas:122-07-6

Min.Order:0

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Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

Methylaminoacetaldehyde Dimethyl Acetal

Cas:122-07-6

Min.Order:0

Negotiable

Type:Manufacturers

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Afine Chemicals Limited

Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter

high purity Methylaminoacetaldehyde dimethyl acetal cas no.122-07-6

Cas:122-07-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Methylaminoacetaldehyde dimethyl acetal

Cas:122-07-6

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Methylaminoacetaldehyde dimethyl acetal

Cas:122-07-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Chemlyte Solutions

Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff

Featured products Methylaminoacetaldehyde dimethyl acetal

Cas:122-07-6

Min.Order:100 Gram

Negotiable

Type:Other

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Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

Methylaminoacetaldehyde dimethyl acetal /High quality/Best price

Cas:122-07-6

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Methylaminoacetaldehyde Dimethyl Acetal

Cas:122-07-6

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Siwei Development Group Ltd.

Product name: Methylaminoacetaldehyde Diethyl Acetal CAS No.:122-07-6 Molecule Formula:C5H14NO2 Molecule Weight:120.17 Purity: 99.0% Package: 25kg/drum Description:Clear transparent liquid Manufacture Standards:Enterprise Standard

High Quality Methylaminoacetaldehyde Diethyl Acetal

Cas:122-07-6

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

Methylaminoacetaldehyde dimethyl acetal

Cas:122-07-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Methylaminoacetaldehyde dimethyl acetal

Cas:122-07-6

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Methylaminoacetaldehyde dimethyl acetal

Cas:122-07-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Methylaminoacetaldehyde dimethyl acetal

Cas:122-07-6

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

Methylaminoacetaldehyde dimethyl acetal Cas no.122-07-6 98%

Cas:122-07-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Methylaminoacetaldehyde dimethyl acetal

Cas:122-07-6

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Suzhou Sibian Chemical Technology Co., Ltd

The process is mature and can be mass produced to 100 kg, with good quality and purity up to 99%.The product has a large stock and can be supplied stably. Package:bottle Application:Drug R&D Transportation:Sealed drying(25℃) Port:ShangHai

Methylaminoacetaldehyde dimethyl acetal

Cas:122-07-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

Methylaminoacetaldehyde dimethyl acetal

Cas:122-07-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Synthetic route

chloroacetaldehyde dimethyl acetal
97-97-2

chloroacetaldehyde dimethyl acetal

methylamine
74-89-5

methylamine

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

Conditions
ConditionsYield
In water at 80 - 85℃; for 16h; Autoclave;87%
Stage #1: chloroacetaldehyde dimethyl acetal; methylamine In methanol at 130 - 135℃; under 9000.9 Torr; for 6h; Autoclave; Large scale;
Stage #2: With sodium methylate In methanol at 0 - 10℃; Temperature; Pressure; Large scale;
1-bromo-2,2-dimethoxyethane
7252-83-7

1-bromo-2,2-dimethoxyethane

methylamine
74-89-5

methylamine

A

bis-(2,2-dimethoxy-ethyl)-methyl-amine
70887-96-6

bis-(2,2-dimethoxy-ethyl)-methyl-amine

B

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

Conditions
ConditionsYield
With methanol at 140℃; im Autoklaven;
C10H21NO4

C10H21NO4

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane at 20℃; for 16h; Inert atmosphere;
1-allyl-1H-benzo[d][1,3]oxazine-2,4-dione
50784-07-1

1-allyl-1H-benzo[d][1,3]oxazine-2,4-dione

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

2-allylamino-N-(2,2-dimethoxy-ethyl)-N-methyl-benzamide
266329-99-1

2-allylamino-N-(2,2-dimethoxy-ethyl)-N-methyl-benzamide

Conditions
ConditionsYield
In acetonitrile for 2h; Substitution; Ring cleavage; Heating;100%
N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

3-methoxyphenylacetic acid chloride
6834-42-0

3-methoxyphenylacetic acid chloride

C14H21NO4
118616-03-8

C14H21NO4

Conditions
ConditionsYield
With sodium hydrogencarbonate In chloroform100%
N-Methylisatoic anhydride
10328-92-4

N-Methylisatoic anhydride

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

N-(2,2-dimethoxy-ethyl)-N-methyl-2-methylamino-benzamide
266329-98-0

N-(2,2-dimethoxy-ethyl)-N-methyl-2-methylamino-benzamide

Conditions
ConditionsYield
In acetonitrile for 2h; Substitution; Ring cleavage; Heating;99%
N-benzylisatoic anhydride
35710-05-5

N-benzylisatoic anhydride

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

2-benzylamino-N-(2,2-dimethoxy-ethyl)-N-methyl-benzamide
266330-00-1

2-benzylamino-N-(2,2-dimethoxy-ethyl)-N-methyl-benzamide

Conditions
ConditionsYield
In acetonitrile for 2h; Substitution; Ring cleavage; Heating;99%
2,2,2-trichloro-1-{4-[(2,3-difluoro-phenyl)-acetyl]-1H-pyrrol-2-yl}-ethanone
849069-51-8

2,2,2-trichloro-1-{4-[(2,3-difluoro-phenyl)-acetyl]-1H-pyrrol-2-yl}-ethanone

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

4-[(2,3-difluoro-phenyl)-acetyl]-1H-pyrrole-2-carboxylic acid (2,2-dimethoxy-ethyl)-methyl-amide
849069-23-4

4-[(2,3-difluoro-phenyl)-acetyl]-1H-pyrrole-2-carboxylic acid (2,2-dimethoxy-ethyl)-methyl-amide

Conditions
ConditionsYield
In acetonitrile at 80℃; for 5h;99%
benzoic acid methyl ester
93-58-3

benzoic acid methyl ester

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

N-(2,2-dimethoxyethyl)-N-methylbenzamide

N-(2,2-dimethoxyethyl)-N-methylbenzamide

Conditions
ConditionsYield
Stage #1: benzoic acid methyl ester With potassium phosphate; 2,2,2-trifluoroethanol In 1,4-dioxane at 125℃; for 0.5h; Sealed tube; Schlenk technique; Inert atmosphere;
Stage #2: N-(methyl)aminoacetaldehyde dimethyl acetal In 1,4-dioxane at 125℃; for 22h; Sealed tube; Schlenk technique; Inert atmosphere;
99%
N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

acryloyl chloride
814-68-6

acryloyl chloride

N-methyl-N-(acetaldehyde dimethyl acetal)propenamide
95984-13-7

N-methyl-N-(acetaldehyde dimethyl acetal)propenamide

Conditions
ConditionsYield
With triethylamine In tetrachloromethane at 25℃; for 6h;98%
With triethylamine In dichloromethane at -10 - 20℃; for 2h; Inert atmosphere;60%
trans 2-phenylethenesulfonyl chloride
52147-97-4

trans 2-phenylethenesulfonyl chloride

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

(E)-2-Phenyl-ethenesulfonic acid (2,2-dimethoxy-ethyl)-methyl-amide
198694-02-9

(E)-2-Phenyl-ethenesulfonic acid (2,2-dimethoxy-ethyl)-methyl-amide

Conditions
ConditionsYield
With triethylamine In tetrachloromethane at 25℃; for 6h;98%
formaldehyd
50-00-0

formaldehyd

C-undecylcalix[4]resorcinarene
847018-76-2

C-undecylcalix[4]resorcinarene

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

4,6,10,12,16,18,22,24-octahydroxy-5,11,17,23-tetrakis[(2,2-dimethoxyethyl)(methyl)aminomethyl]-2,8,14,20-tetraundecylpentacyclo[19.3.1.13,7.19,13.115,19]octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene

4,6,10,12,16,18,22,24-octahydroxy-5,11,17,23-tetrakis[(2,2-dimethoxyethyl)(methyl)aminomethyl]-2,8,14,20-tetraundecylpentacyclo[19.3.1.13,7.19,13.115,19]octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene

Conditions
ConditionsYield
In ethanol; benzene at 20℃; for 24h; Mannich reaction;98%
3-Benzyloxybenzaldehyde
1700-37-4

3-Benzyloxybenzaldehyde

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

(3-benzyloxybenzyl)-(2,2-dimethoxyethyl)methylamine

(3-benzyloxybenzyl)-(2,2-dimethoxyethyl)methylamine

Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride In dichloromethane at 20℃; for 18h;98%
N-(Benzyloxycarbonyl)glycine
1138-80-3

N-(Benzyloxycarbonyl)glycine

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

benzyl (2-((2,2-dimethoxyethyl)(methyl)amino)-2-oxoethyl)carbamate
851726-64-2

benzyl (2-((2,2-dimethoxyethyl)(methyl)amino)-2-oxoethyl)carbamate

Conditions
ConditionsYield
Stage #1: N-(Benzyloxycarbonyl)glycine With 4-methyl-morpholine; isobutyl chloroformate In tetrahydrofuran at 0℃; for 0.0333333h;
Stage #2: N-(methyl)aminoacetaldehyde dimethyl acetal In tetrahydrofuran at 20℃; for 16h;
97%
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃;
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In DMF (N,N-dimethyl-formamide) at 20℃;
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃;
carbon disulfide
75-15-0

carbon disulfide

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

C6H12NO2S2(1-)*Na(1+)
1415567-75-7

C6H12NO2S2(1-)*Na(1+)

Conditions
ConditionsYield
With sodium hydroxide In methanol; water at 20℃; for 1h; Cooling with ice;97%
With sodium hydroxide In methanol; water at 20℃; for 1h; Cooling;97%
3-(bromomethyl)-5-(tert-butyl)-2-hydroxybenzaldehyde
367965-70-6

3-(bromomethyl)-5-(tert-butyl)-2-hydroxybenzaldehyde

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

5-tert-butyl-3-(N-methyl-N-(2,2-dimethoxyethyl)amino)methylsalicylaldehyde

5-tert-butyl-3-(N-methyl-N-(2,2-dimethoxyethyl)amino)methylsalicylaldehyde

Conditions
ConditionsYield
With triethylamine In chloroform at 20℃; for 24h;97%
N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

Cinnamoyl chloride
102-92-1

Cinnamoyl chloride

trans N-methyl-N-(acetaldehyde dimethyl acetal)cinnamamide
157059-60-4

trans N-methyl-N-(acetaldehyde dimethyl acetal)cinnamamide

Conditions
ConditionsYield
With triethylamine In tetrachloromethane at 25℃; for 6h;96%
3,4-Dimethoxyphenylboronic acid
122775-35-3

3,4-Dimethoxyphenylboronic acid

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

Glyoxilic acid
298-12-4

Glyoxilic acid

N-(2,2-dimethoxyethyl)-N-methyl-α-(3,4-dimethoxyphenyl)glycine
1370371-79-1

N-(2,2-dimethoxyethyl)-N-methyl-α-(3,4-dimethoxyphenyl)glycine

Conditions
ConditionsYield
In dichloromethane at 20℃; Petasis reaction; Inert atmosphere;96%
C60H88O8
134724-39-3

C60H88O8

formaldehyd
50-00-0

formaldehyd

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

4,6,10,12,16,18,22,24-octahydroxy-5,11,17,23-tetrakis[(2,2-dimethoxyethyl)(methyl)aminomethyl]-2,8,14,20-tetraoctylpentacyclo[19.3.1.13,7.19,13.115,19]octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene

4,6,10,12,16,18,22,24-octahydroxy-5,11,17,23-tetrakis[(2,2-dimethoxyethyl)(methyl)aminomethyl]-2,8,14,20-tetraoctylpentacyclo[19.3.1.13,7.19,13.115,19]octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene

Conditions
ConditionsYield
In ethanol; benzene at 20℃; for 24h; Mannich reaction;95%
2,6-dichloronicotinoyl chloride
58584-83-1

2,6-dichloronicotinoyl chloride

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

2,6-dichloro-N-(2,2-dimethoxyethyl)-N-methylnicotinamide
1255701-47-3

2,6-dichloro-N-(2,2-dimethoxyethyl)-N-methylnicotinamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃;95%
1,2-epoxy-3,4-dihydronaphthalene
2461-34-9

1,2-epoxy-3,4-dihydronaphthalene

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

(1RS,2RS)-1-[(2,2-dimethoxyethyl)methylamino]-1,2,3,4-tetrahydro-2-naphthalenol

(1RS,2RS)-1-[(2,2-dimethoxyethyl)methylamino]-1,2,3,4-tetrahydro-2-naphthalenol

Conditions
ConditionsYield
With Teflon acid for 20h; Autoclave; Heating; Inert atmosphere;95%
trimethylsilyl isocyanate
1118-02-1

trimethylsilyl isocyanate

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

1-(2,2-dimethoxyethyl)-1-methyl-urea

1-(2,2-dimethoxyethyl)-1-methyl-urea

Conditions
ConditionsYield
In dichloromethane at 20 - 25℃; for 8.25h;95%
In dichloromethane at 20℃; for 192h;95%
diphenylcarbamic chloride
83-01-2

diphenylcarbamic chloride

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

1-(2,2-dimethoxyethyl)-1-methyl-3,3-diphenylurea

1-(2,2-dimethoxyethyl)-1-methyl-3,3-diphenylurea

Conditions
ConditionsYield
With triethylamine In benzene at 5 - 7℃; for 2h;95%
N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

4-bromo-2-fluorobenzaldehyde
57848-46-1

4-bromo-2-fluorobenzaldehyde

4-bromo-2-((2, 2-dimethoxyethyl)(methyl)amino) benzaldehyde
1307882-82-1

4-bromo-2-((2, 2-dimethoxyethyl)(methyl)amino) benzaldehyde

Conditions
ConditionsYield
With potassium carbonate In acetonitrile at 100℃; for 48h;94%
(4-nitrophenyl) N-(5-tert-butylisothiazol-3-yl)carbamate

(4-nitrophenyl) N-(5-tert-butylisothiazol-3-yl)carbamate

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

3-(5-tert-butylisothiazol-3-yl)-1-(2,2-dimethoxyethyl)-1-methyl-urea

3-(5-tert-butylisothiazol-3-yl)-1-(2,2-dimethoxyethyl)-1-methyl-urea

Conditions
ConditionsYield
In 1,4-dioxane at 70℃; for 0.666667h; Inert atmosphere;94%
diethyl chlorophosphate
814-49-3

diethyl chlorophosphate

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

diethyl N-(2,2-dimethoxyethyl)-N-methylphosphoramidate
959925-98-5

diethyl N-(2,2-dimethoxyethyl)-N-methylphosphoramidate

Conditions
ConditionsYield
In benzene at 20℃; for 3h;93.6%
(E)-pent-2-enoyl chloride
33698-85-0

(E)-pent-2-enoyl chloride

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

trans N-methyl-N-(acetaldehyde dimethyl acetal)pent-2-enamide
157059-59-1

trans N-methyl-N-(acetaldehyde dimethyl acetal)pent-2-enamide

Conditions
ConditionsYield
With triethylamine In tetrachloromethane at 25℃; for 6h;93%
D-erythronolactone acetonide
25581-41-3

D-erythronolactone acetonide

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

(4R,5R)-5-hydroxymethyl-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid (2,2-dimethoxy-ethyl)-methyl-amide
908027-68-9

(4R,5R)-5-hydroxymethyl-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid (2,2-dimethoxy-ethyl)-methyl-amide

Conditions
ConditionsYield
Stage #1: N-(methyl)aminoacetaldehyde dimethyl acetal With trimethylaluminum In hexane; dichloromethane at 0℃; for 0.5h;
Stage #2: D-erythronolactone acetonide In hexane; dichloromethane at 20℃; for 18h;
93%
formaldehyd
50-00-0

formaldehyd

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

4,6,10,12,16,18,22,24-octahydroxy-5,11,17,23-tetrakis[(2,2-dimethoxyethyl)(methyl)aminomethyl]-2,8,14,20-tetrahexylpentacyclo[19.3.1.13,7.19,13.115,19]octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene

4,6,10,12,16,18,22,24-octahydroxy-5,11,17,23-tetrakis[(2,2-dimethoxyethyl)(methyl)aminomethyl]-2,8,14,20-tetrahexylpentacyclo[19.3.1.13,7.19,13.115,19]octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene

Conditions
ConditionsYield
In ethanol; benzene at 20℃; for 24h; Mannich reaction;93%
In water Mannich reaction;
N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

2-Chloro-6-methyl-chromen-4-one

2-Chloro-6-methyl-chromen-4-one

2-[(2,2-Dimethoxy-ethyl)-methyl-amino]-6-methyl-chromen-4-one
199473-92-2

2-[(2,2-Dimethoxy-ethyl)-methyl-amino]-6-methyl-chromen-4-one

Conditions
ConditionsYield
With triethylamine In ethanol at 20℃; for 24h;92%
2-amino-3-benzylpyridine
130277-16-6

2-amino-3-benzylpyridine

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

(10,11-dihydro-5H-benzo[e]pyrido[2,3-b]azepin-10-ylmethyl)-methyl-amine
1071504-64-7

(10,11-dihydro-5H-benzo[e]pyrido[2,3-b]azepin-10-ylmethyl)-methyl-amine

Conditions
ConditionsYield
sulfuric acid at 20℃; for 0.75h; Product distribution / selectivity;92%
2-Methoxyphenylboronic acid
5720-06-9

2-Methoxyphenylboronic acid

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

Glyoxilic acid
298-12-4

Glyoxilic acid

N-(2,2-dimethoxyethyl)-N-methyl-2-methoxyphenylglycine
1370371-88-2

N-(2,2-dimethoxyethyl)-N-methyl-2-methoxyphenylglycine

Conditions
ConditionsYield
In dichloromethane at 20℃; Petasis reaction; Inert atmosphere;92%
carbon disulfide
75-15-0

carbon disulfide

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

N-(methyl)aminoacetaldehyde dimethyl acetal
122-07-6

N-(methyl)aminoacetaldehyde dimethyl acetal

C12H24CuN2O4S4

C12H24CuN2O4S4

Conditions
ConditionsYield
In diethyl ether at 0 - 20℃; for 4h;91%

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