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2-phenethyl propanoate
Conditions | Yield |
---|---|
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; cesium acetate; isopropyl alcohol at 100℃; Schlenk technique; Inert atmosphere; | 67% |
With [RhCl2(p-cymene)]2; cesium acetate In isopropyl alcohol at 20 - 100℃; for 20h; Inert atmosphere; | 67% |
Multi-step reaction with 2 steps 1: sodium iodide / acetone / 50 °C 2: [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; cesium acetate; isopropyl alcohol / 100 °C / Schlenk technique; Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
With pyridine; N-Bromosuccinimide; triphenylphosphine In dichloromethane; pentane for 2h; Ambient temperature; | 93% |
With ion-exchange resin KU-2-8 In benzene at 80 - 85℃; | 92% |
With dmap; triphenylphosphine; iodosodilactone In chloroform for 2h; Reflux; | 92% |
Conditions | Yield |
---|---|
With zirconocene bis(perfluorooctanesulfonate) trihydrate*(tetrahydrofuran) In neat (no solvent) at 65℃; for 6h; Sealed tube; Green chemistry; chemoselective reaction; | 90% |
Conditions | Yield |
---|---|
zinc(II) perchlorate at 20℃; for 1.25h; | 99% |
With dmap for 0.05h; Irradiation; microwave; | 95% |
Conditions | Yield |
---|---|
With tetradecyl(trihexyl)phosphonium bistriflamide; N-ethyl-N,N-diisopropylamine at 75℃; | 98% |
With tetradecyl(trihexyl)phosphonium bistriflimide at 75℃; for 6h; | 98% |
Conditions | Yield |
---|---|
With N,N,N,N,N,N-hexamethylphosphoric triamide; bromine; sodium hydrogencarbonate In dichloromethane; water | 89% |
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane for 0.166667h; Ambient temperature; | 70% |
Conditions | Yield |
---|---|
Stage #1: 2-phenylethanol With bis(cyclopentadienyl)titanium dichloride; manganese; diiodomethane In tetrahydrofuran at 20℃; for 2.5h; Inert atmosphere; Stage #2: Ethyl propionate In tetrahydrofuran at 20℃; for 1.5h; Inert atmosphere; | |
With recombinant acyltransferase from Mycobacterium smegmatis In aq. phosphate buffer at 25℃; for 0.5h; pH=8; Concentration; Green chemistry; Enzymatic reaction; |
2-phenethyl propanoate
Conditions | Yield |
---|---|
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; cesium acetate; isopropyl alcohol at 100℃; Schlenk technique; Inert atmosphere; | 71% |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: benzene / 3 h / Ambient temperature 2: 2-propanol, di-tert-butyl hyponitrite / 5 h / 60 °C / average chain length radical chain View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: pyridine / dichloromethane / 0 - 20 °C 2: [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; cesium acetate; isopropyl alcohol / 100 °C / Schlenk technique; Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: pyridine / dichloromethane / 0 - 20 °C 2: sodium iodide / acetone / 50 °C 3: [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; cesium acetate; isopropyl alcohol / 100 °C / Schlenk technique; Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; isopropyl alcohol; potassium tert-butylate / 100 °C / Schlenk technique; Inert atmosphere 2: pyridine / dichloromethane / 0 - 20 °C 3: [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; cesium acetate; isopropyl alcohol / 100 °C / Schlenk technique; Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1: [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; isopropyl alcohol; potassium tert-butylate / 100 °C / Schlenk technique; Inert atmosphere 2: pyridine / dichloromethane / 0 - 20 °C 3: sodium iodide / acetone / 50 °C 4: [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; cesium acetate; isopropyl alcohol / 100 °C / Schlenk technique; Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: anhydrous aluminum chloride / 4 h / 6 - 7 °C 1.2: 90 percent / water 2.1: 92 percent / ion-exchange resin KU-2-8 / benzene / 80 - 85 °C View Scheme |
2-phenethyl propanoate
Conditions | Yield |
---|---|
With 1,2,2,6,6-pentamethylpiperidine; trans-di-O-tert-butyl hyponitrite In acetonitrile at 60℃; for 5h; | |
With isopropyl alcohol; trans-di-O-tert-butyl hyponitrite at 60℃; for 5h; average chain length radical chain; |
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