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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 6-Chloro-1-Methyl-1H-Benzo[D][1,3]Oxazine-2,4-Dione supplier in China

Cas:14529-12-5

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Hebei yanxi chemical co.,LTD.

hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm

High quality 6-Chloro-1-Methyl-1H-Benzo[D][1,3]Oxazine-2,4-Dione supplier in China

Cas:14529-12-5

Min.Order:1 Metric Ton

FOB Price: $1.0 / 3.0

Type:Manufacturers

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Quality 99% 5-Chloro-N-methylisatoic anhydride 14529-12-5 ISO Producer

Cas:14529-12-5

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

6-CHLORO-1-METHYL-1H-BENZO[D][1,3]OXAZINE-2,4-DIONE

Cas:14529-12-5

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. High quality and competitive price: 1) Standard: BP/USP/EP/ enterprise standard 2) All purity ≥99% 3) We are manufacturers and can provide high quality products at factory prices. 2. Fast and safe delivery 1) The package c

6-chloro-1-methyl-2H-3,1-benzoxazine-2,4(1H)-dione

Cas:14529-12-5

Min.Order:1 Kilogram

FOB Price: $2.0 / 5.0

Type:Trading Company

inquiry

Hangzhou Sartort Biopharma Co., Ltd

Appearance:White powder Storage:Room temperature Package:25kg/Barrel Application:APIS Transportation:Express/Sea/Air Port:Any port in china

Factory supply 5-Chloro-N-methylisatoicanhydride

Cas:14529-12-5

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

5-Chloro-N-methylisatoic anhydride 14529-12-5

Cas:14529-12-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

6-chloro-1-methyl-2H-3,1-benzoxazine-2,4(1H)-dione CAS:14529-12-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializin

6-chloro-1-methyl-2H-3,1-benzoxazine-2,4(1H)-dione CAS:14529-12-5

Cas:14529-12-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

5-Chloro-N-methylisatoic anhydride

Cas:14529-12-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

5-Chloro-N-methylisatoic anhydride

Cas:14529-12-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

6-Chloro-1-Methyl-1H-Benzo[D][1,3]Oxazine-2,4-Dione

Cas:14529-12-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

N-methyl-5-Chloro-isatoic anhydride

Cas:14529-12-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 6-Chloro-1-Methyl-1H-Benzo[D][1,3]Oxazine-2,4-Dione

Cas:14529-12-5

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

TaiChem Taizhou Limited

Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site

6-chloro-1-methyl-2H-3,1-benzoxazine-2,4(1H)-dione

Cas:14529-12-5

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

6-CHLORO-1-METHYL-1H-BENZO[D][1,3]OXAZINE-2,4-DIONE

Cas:14529-12-5

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Top Purity 6-chloro-1-methyl-2H-3,1-benzoxazine-2,4(1H)-dione

Cas:14529-12-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

High quality 6-Chloro-1-Methyl-1H-Benzo[D][1,3]Oxazine-2,4-Dione supplier in China

Cas:14529-12-5

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Hangzhou Huarong Pharm Co., Ltd.

We Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O

6-chloro-1-methyl-2H-3,1-benzoxazine-2,4(1H)-dione

Cas:14529-12-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

6-chloro-1-methyl-2H-3,1-benzoxazine-2,4(1H)-dione

Cas:14529-12-5

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

High quality 6-Chloro-1-Methyl-1H-Benzo[D][1,3]Oxazine-2,4-Dione supplier in China

Cas:14529-12-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

High quality 6-Chloro-1-Methyl-1H-Benzo[D][1,3]Oxazine-2,4-Dione supplier in China

Cas:14529-12-5

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Golden Pharma Co., Limited

GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

6-chloro-1-methyl-2H-3,1-benzoxazine-2,4(1H)-dione

Cas:14529-12-5

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

High quality 6-Chloro-1-Methyl-1H-Benzo[D][1,3]Oxazine-2,4-Dione supplier in China

Cas:14529-12-5

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Hebei Mojin Biotechnology Co.,Ltd

We produce carbomer by our own factory,carbomer 940 is our best seller.It is used for cosmetic and medical.And we also become agent for lubrizol.Our carbomer 940 get high viscosity and good transparency.The price will depond on the market,surely supp

5-Chloro-N-methylisatoic anhydride

Cas:14529-12-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

6-Chloro-1-methyl-3,1-benzoxazine-2,4-dione cas no. 14529-12-5 98%

Cas:14529-12-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

N-Methyl-5-Chloro-Isatoic Anhydride

Cas:14529-12-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

2H-3,1-Benzoxazine-2,4(1H)-dione,6-chloro-1-methyl-

Cas:14529-12-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

6-Chloro-1-Methyl-1H-Benzo[D][1,3]Oxazine-2,4-Dione

Cas:14529-12-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Xi`an Eastling Biotech Co., Ltd.

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou

6-chloro-1-methyl-2H-3,1-benzoxazine-2,4(1H)-dione

Cas:14529-12-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

5-Chloro-N-methylisatoic anhydride

Cas:14529-12-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

5-Chloroisatoic anhydride
4743-17-3

5-Chloroisatoic anhydride

methyl iodide
74-88-4

methyl iodide

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

Conditions
ConditionsYield
In ice-water; ISOPROPYLAMIDE90%
With sodium carbonate In N,N-dimethyl-formamide85.2%
With sodium hydride In N,N-dimethyl-formamide at 20℃; for 18h; Inert atmosphere;83%
carbon monoxide
201230-82-2

carbon monoxide

N-methyl(p-chloroaniline)
932-96-7

N-methyl(p-chloroaniline)

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

Conditions
ConditionsYield
With oxygen; copper diacetate; palladium diacetate; potassium iodide; Trimethylacetic acid In acetonitrile at 60℃; under 760.051 Torr; regioselective reaction;78%
5-Chloroisatoic anhydride
4743-17-3

5-Chloroisatoic anhydride

methyl bromide
74-83-9

methyl bromide

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

Conditions
ConditionsYield
Stage #1: 5-Chloroisatoic anhydride With sodium hydride In N,N-dimethyl-formamide at 20℃; for 1h;
Stage #2: methyl bromide In N,N-dimethyl-formamide for 18h;
72%
With potassium carbonate In N,N-dimethyl-formamide at 80℃;
carbon monoxide
201230-82-2

carbon monoxide

4-chloro-N,N-dimethylaniline
698-69-1

4-chloro-N,N-dimethylaniline

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

Conditions
ConditionsYield
With dichloro bis(acetonitrile) palladium(II); oxygen; copper diacetate In N,N-dimethyl-formamide; toluene at 100℃;71%
With dichloro bis(acetonitrile) palladium(II); oxygen; copper diacetate In N,N-dimethyl-formamide; toluene at 100℃; under 760.051 Torr; for 24h;71%
chloroformic acid ethyl ester
541-41-3

chloroformic acid ethyl ester

dimethyl sulfate
77-78-1

dimethyl sulfate

5-chloroanthranilic acid
635-21-2

5-chloroanthranilic acid

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

Conditions
ConditionsYield
(i) aq. NaOH, (ii) /BRN= 385653/, (iii) AcCl; Multistep reaction;
5-Chloroisatoic anhydride
4743-17-3

5-Chloroisatoic anhydride

CH3-Hal

CH3-Hal

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

Conditions
ConditionsYield
With sodium hydride 1.) DMF, 2 h, 2.) 8 h; Multistep reaction;
5-Chloroisatoic anhydride
4743-17-3

5-Chloroisatoic anhydride

methyl halide

methyl halide

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

Conditions
ConditionsYield
(i) NaH, AcNMe2, (ii) methyl halide; Multistep reaction;
5-chloro-1-methylindoline-2, 3-dione
60434-13-1

5-chloro-1-methylindoline-2, 3-dione

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

Conditions
ConditionsYield
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 20℃;
N-(4-chlorophenyl)-2-(hydroxyimino)ethanamide
65798-06-3, 17122-56-4

N-(4-chlorophenyl)-2-(hydroxyimino)ethanamide

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: H2SO4 / 80 °C
2: NaH / N,N-dimethyl-acetamide / 20 °C
3: mCPBA / CH2Cl2 / 20 °C
View Scheme
5-chloroindole 2,3-dione
17630-76-1

5-chloroindole 2,3-dione

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: NaH / N,N-dimethyl-acetamide / 20 °C
2: mCPBA / CH2Cl2 / 20 °C
View Scheme
4-chloro-aniline
106-47-8

4-chloro-aniline

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: NH2OH*HCl; Na2SO4; aq. conc. HCl / Heating
2: H2SO4 / 80 °C
3: NaH / N,N-dimethyl-acetamide / 20 °C
4: mCPBA / CH2Cl2 / 20 °C
View Scheme
5-chloroanthranilic acid
635-21-2

5-chloroanthranilic acid

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triethylamine / 20 - 100 °C / Inert atmosphere
2: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: 1,2-dichloro-ethane / 4 h / Reflux
2: N,N-dimethyl-formamide / 18 h / 20 °C / Alkaline conditions
View Scheme
Multi-step reaction with 2 steps
1: 1,2-dichloro-ethane / 3.25 h / Reflux
2: potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C
View Scheme
6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

glycine
56-40-6

glycine

7-chloro-1-methyl-3,4-dihydro-1H-1,4-benzodiazepine-2,5-dione
5973-28-4

7-chloro-1-methyl-3,4-dihydro-1H-1,4-benzodiazepine-2,5-dione

Conditions
ConditionsYield
Stage #1: 6-chloro-N-methylisatoic anhydride; glycine With acetic acid at 130℃; for 7h;
Stage #2: With sodium hydroxide; water; sodium hydrogencarbonate pH=~ 9 - 10;
100%
With acetic acid at 130℃; for 7h;
With acetic acid at 130℃; for 7h;
6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

diethyl malonate
105-53-3

diethyl malonate

ethyl 6-chloro-1,2-dihydro-4-hydroxy-1-methyl-2-oxo-3-quinolinecarboxylate
52851-65-7

ethyl 6-chloro-1,2-dihydro-4-hydroxy-1-methyl-2-oxo-3-quinolinecarboxylate

Conditions
ConditionsYield
Stage #1: diethyl malonate With sodium hydride In N,N-dimethyl acetamide at 20 - 90℃; for 0.5h;
Stage #2: 6-chloro-N-methylisatoic anhydride In N,N-dimethyl acetamide at 20 - 110℃;
97%
Stage #1: diethyl malonate With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.5h; Inert atmosphere;
Stage #2: 6-chloro-N-methylisatoic anhydride In N,N-dimethyl-formamide at 50℃; for 5h; Inert atmosphere;
30%
4-(4-bromophenyl)-4-vinyl-1,3-dioxolan-2-one
1459246-69-5

4-(4-bromophenyl)-4-vinyl-1,3-dioxolan-2-one

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

(Z)-6-(4-bromophenyl)-11-chloro-1-methyl-4,7-dihydro-2H-benzo[d][1,7]dioxa[3]azacycloundecine-2,9(1H)-dione

(Z)-6-(4-bromophenyl)-11-chloro-1-methyl-4,7-dihydro-2H-benzo[d][1,7]dioxa[3]azacycloundecine-2,9(1H)-dione

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); triphenylphosphine In ethyl acetate at 60℃; for 2h;93%
4-(4-bromophenyl)-4-vinyl-1,3-dioxolan-2-one
1459246-69-5

4-(4-bromophenyl)-4-vinyl-1,3-dioxolan-2-one

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

C19H15BrClNO4

C19H15BrClNO4

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); triphenylphosphine In ethyl acetate at 60℃; for 2h;93%
4-phenyl-4-vinyl-1,3-dioxolan -2-one
1459246-62-8

4-phenyl-4-vinyl-1,3-dioxolan -2-one

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

(Z)-11-chloro-1-methyl-6-phenyl-4,7-dihydro-2H-benzo[d][1,7]dioxa[3]azacycloundecine-2,9(1H)-dione

(Z)-11-chloro-1-methyl-6-phenyl-4,7-dihydro-2H-benzo[d][1,7]dioxa[3]azacycloundecine-2,9(1H)-dione

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); triphenylphosphine In ethyl acetate at 60℃; for 4h;87%
With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In toluene at 20℃; for 4h; Schlenk technique; Inert atmosphere;83%
4-(4-methylphenyl)-4-vinyl-1,3-dioxolan-2-one
1638152-34-7

4-(4-methylphenyl)-4-vinyl-1,3-dioxolan-2-one

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

(Z)-11-chloro-1-methyl-6-(p-tolyl)-4,7-dihydro-2H-benzo[d][1,7]dioxa[3]azacycloundecine-2,9(1H)-dione

(Z)-11-chloro-1-methyl-6-(p-tolyl)-4,7-dihydro-2H-benzo[d][1,7]dioxa[3]azacycloundecine-2,9(1H)-dione

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); triphenylphosphine In ethyl acetate at 60℃; for 8h;87%
4-phenyl-4-vinyl-1,3-dioxolan -2-one
1459246-62-8

4-phenyl-4-vinyl-1,3-dioxolan -2-one

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

C19H16ClNO4

C19H16ClNO4

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); triphenylphosphine In ethyl acetate at 60℃; for 4h;87%
N,N-diethylethylenediamine
100-36-7

N,N-diethylethylenediamine

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

5-chloro-N-[2-(diethylamino)ethyl]-2-methylaminobenzamide
159619-29-1

5-chloro-N-[2-(diethylamino)ethyl]-2-methylaminobenzamide

Conditions
ConditionsYield
In 1,4-dioxane at 60℃; for 2h;85%
4-(4-chlorophenyl)-4-vinyl-1,3-dioxolan-2-one
1459246-68-4

4-(4-chlorophenyl)-4-vinyl-1,3-dioxolan-2-one

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

(Z)-11-chloro-6-(4-chlorophenyl)-1-methyl-4,7-dihydro-2H-benzo[d][1,7]dioxa[3]azacycloundecine-2,9(1H)-dione

(Z)-11-chloro-6-(4-chlorophenyl)-1-methyl-4,7-dihydro-2H-benzo[d][1,7]dioxa[3]azacycloundecine-2,9(1H)-dione

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); triphenylphosphine In ethyl acetate at 60℃; for 2h;85%
4-(4-methoxyphenyl)-4-vinyl-1,3-dioxolan-2-one
1459246-67-3

4-(4-methoxyphenyl)-4-vinyl-1,3-dioxolan-2-one

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

(Z)-11-chloro-6-(4-methoxyphenyl)-1-methyl-4,7-dihydro-2H-benzo[d][1,7]dioxa[3]azacycloundecine-2,9(1H)-dione

(Z)-11-chloro-6-(4-methoxyphenyl)-1-methyl-4,7-dihydro-2H-benzo[d][1,7]dioxa[3]azacycloundecine-2,9(1H)-dione

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); triphenylphosphine In ethyl acetate at 60℃; for 6h;85%
4-(4-chlorophenyl)-4-vinyl-1,3-dioxolan-2-one
1459246-68-4

4-(4-chlorophenyl)-4-vinyl-1,3-dioxolan-2-one

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

C19H15Cl2NO4

C19H15Cl2NO4

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); triphenylphosphine In ethyl acetate at 60℃; for 2h;85%
4-(4-methoxyphenyl)-4-vinyl-1,3-dioxolan-2-one
1459246-67-3

4-(4-methoxyphenyl)-4-vinyl-1,3-dioxolan-2-one

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

C20H18ClNO5

C20H18ClNO5

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); triphenylphosphine In ethyl acetate at 60℃; for 6h;85%
phenylhydrazine
100-63-0

phenylhydrazine

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

ortho-bromobenzaldehyde
6630-33-7

ortho-bromobenzaldehyde

2-(2-bromophenyl)-6-chloro-1-methyl-3-(phenylamino)-2,3-dihydroquinazolin-4(1H)-one
1452386-56-9

2-(2-bromophenyl)-6-chloro-1-methyl-3-(phenylamino)-2,3-dihydroquinazolin-4(1H)-one

Conditions
ConditionsYield
Stage #1: phenylhydrazine; 6-chloro-N-methylisatoic anhydride In acetonitrile Reflux;
Stage #2: ortho-bromobenzaldehyde With toluene-4-sulfonic acid In acetonitrile at 81℃;
84%
6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

glycine
56-40-6

glycine

A

5-chloro-2-(methylamino)hippuric acid
72952-53-5

5-chloro-2-(methylamino)hippuric acid

B

5-chloro-2-methylamino-benzoic acid
33280-14-7

5-chloro-2-methylamino-benzoic acid

Conditions
ConditionsYield
With sodium carbonate In waterA 83.9%
B 7%
6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

1,3-Diphenylcarbodiimide
622-16-2

1,3-Diphenylcarbodiimide

(Z)-6-chloro-1-methyl-3-phenyl-2-(phenylimino)-2,3-dihydroquinazolin-4(1H)-one

(Z)-6-chloro-1-methyl-3-phenyl-2-(phenylimino)-2,3-dihydroquinazolin-4(1H)-one

Conditions
ConditionsYield
With bis(triphenylphosphine)nickel(II) chloride; zinc In acetonitrile at 100℃; for 10h; Sealed tube; Inert atmosphere;83%
6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

diethylaminopropylamine
104-78-9

diethylaminopropylamine

5-chloro-N-[3-(diethylamino)propyl]-2-methylamino benzamide

5-chloro-N-[3-(diethylamino)propyl]-2-methylamino benzamide

Conditions
ConditionsYield
In 1,4-dioxane; ethyl acetate81%
In 1,4-dioxane at 60℃; for 5h;80%
1-(2-aminoethyl)pyrrolidine
7154-73-6

1-(2-aminoethyl)pyrrolidine

petroleum ether-isopropanol-ammonia

petroleum ether-isopropanol-ammonia

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

5-chloro-2-methylamino-N-[2-(1-pyrrolidinyl)ethyl] benzamide

5-chloro-2-methylamino-N-[2-(1-pyrrolidinyl)ethyl] benzamide

Conditions
ConditionsYield
With sodium hydroxide In 1,4-dioxane; dichloromethane80%
N-benzyl-N-(methoxymethyl)-N-[(trimethylsilyl)methyl]amine
93102-05-7

N-benzyl-N-(methoxymethyl)-N-[(trimethylsilyl)methyl]amine

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

3-benzyl-7-chloro-1-methyl-3,4-dihydro-1H-benzo[d][1,3]diazepine-5(2H)-one
1261594-23-3

3-benzyl-7-chloro-1-methyl-3,4-dihydro-1H-benzo[d][1,3]diazepine-5(2H)-one

Conditions
ConditionsYield
With lithium fluoride In acetonitrile at 35℃; for 3h; Inert atmosphere; Molecular sieve; Sonication;76%
1-(phenylmethyl)pyrrolidine-2,4-dione
30125-76-9

1-(phenylmethyl)pyrrolidine-2,4-dione

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

2-benzyl-7-chloro-4-methyl-2,3-dihydro-1H-pyrrolo[3,4-b]quinoline-1,9(4H)-dione

2-benzyl-7-chloro-4-methyl-2,3-dihydro-1H-pyrrolo[3,4-b]quinoline-1,9(4H)-dione

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 50℃; for 2h; Sealed tube; Inert atmosphere; Molecular sieve;76%
4-(2-AMINOETHYL)MORPHOLINE
2038-03-1

4-(2-AMINOETHYL)MORPHOLINE

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

5-chloro-2-methylamino-N-<2-(4-morpholinyl)ethyl>-benzamide
92299-77-9

5-chloro-2-methylamino-N-<2-(4-morpholinyl)ethyl>-benzamide

Conditions
ConditionsYield
In 1,4-dioxane for 2h; Ambient temperature;75%
ethanolamine
141-43-5

ethanolamine

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

5-Chlor-N-(2-hydroxy-aethyl)-2-methylamino-benzamid
4927-76-8

5-Chlor-N-(2-hydroxy-aethyl)-2-methylamino-benzamid

Conditions
ConditionsYield
In 1,4-dioxane at 60℃; for 1.5h;74%
tryptamine
61-54-1

tryptamine

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

3-chloro-14-methyl-8,13,13b,14-tetrahydro-7H-indolo[2',3':3,4]pyrido[2,1-b]quinazolin-5-one

3-chloro-14-methyl-8,13,13b,14-tetrahydro-7H-indolo[2',3':3,4]pyrido[2,1-b]quinazolin-5-one

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane; trifluoroacetic anhydride In N,N-dimethyl acetamide at 100℃; for 5h;74%
dimethyl(prop-2-yn-1-yl)sulfonium bromide
23451-62-9

dimethyl(prop-2-yn-1-yl)sulfonium bromide

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

6-chloro-1,2-dimethyl-3-(methylthio)quinolin-4(1H)-one

6-chloro-1,2-dimethyl-3-(methylthio)quinolin-4(1H)-one

Conditions
ConditionsYield
With dmap In acetonitrile at 60℃; for 5h;70%
6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

4,9-dihydro-6-methoxy-3H-pyrido[3,4-b]indole
7212-59-1

4,9-dihydro-6-methoxy-3H-pyrido[3,4-b]indole

C20H18ClN3O2
1394329-48-6

C20H18ClN3O2

Conditions
ConditionsYield
In dichloromethane at 45℃; for 6h;69%
p-chlorophenylalanine
14173-39-8

p-chlorophenylalanine

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

(S)-7-chloro-3-(4-chlorobenzyl)-1-methyl-3,4-dihydro-1H-benzo[e][1,4]diazepine-2,5-dione

(S)-7-chloro-3-(4-chlorobenzyl)-1-methyl-3,4-dihydro-1H-benzo[e][1,4]diazepine-2,5-dione

Conditions
ConditionsYield
With acetic acid for 18h; Reflux;67%
With acetic acid for 16h; Reflux;67%
4-(4-(benzyloxy)phenyl)-4-vinyl-1,3-dioxolan-2-one

4-(4-(benzyloxy)phenyl)-4-vinyl-1,3-dioxolan-2-one

6-chloro-N-methylisatoic anhydride
14529-12-5

6-chloro-N-methylisatoic anhydride

(Z)-6-(4-(benzyloxy)phenyl)-11-chloro-1-methyl-4,7-dihydro-2H-benzo[d][1,7]dioxa[3]azacycloundecine-2,9(1H)-dione

(Z)-6-(4-(benzyloxy)phenyl)-11-chloro-1-methyl-4,7-dihydro-2H-benzo[d][1,7]dioxa[3]azacycloundecine-2,9(1H)-dione

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); triphenylphosphine In ethyl acetate at 60℃; for 3h;67%

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