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(1H-benzo[d]imidazol-6-yl)methanol
1H-1,3-benzodiazol-6-ylmethanamine
Conditions | Yield |
---|---|
Stage #1: (1H-benzo[d]imidazol-6-yl)methanol With diphenylphosphoranyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at 20℃; for 4h; Stage #2: With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; for 96h; | 67% |
5-(azidomethyl)benzimidazole
1H-1,3-benzodiazol-6-ylmethanamine
Conditions | Yield |
---|---|
With water; triphenylphosphine In tetrahydrofuran at 20℃; |
5-benzimidazolecarboxylic acid
1H-1,3-benzodiazol-6-ylmethanamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: lithium aluminium tetrahydride / tetrahydrofuran / 96 h / 0 - 20 °C 2.1: diphenylphosphoranyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 4 h / 20 °C 2.2: 96 h / 20 °C View Scheme |
1H-1,3-benzodiazol-6-ylmethanamine
1,1'-carbonyldiimidazole
N-(1H-1,3-benzodiazol-6-ylmethyl)-4-(4-fluorophenoxy)piperidine-1-carboxamide
Conditions | Yield |
---|---|
Stage #1: 1H-1,3-benzodiazol-6-ylmethanamine; 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide for 1h; Stage #2: 4-(4-Fluorophenoxy)piperidine hydrochloride With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 16h; | 49% |
1H-1,3-benzodiazol-6-ylmethanamine
Conditions | Yield |
---|---|
With 4-methyl-morpholine; ammonia; benzotriazol-1-ol In methanol; dichloromethane; N,N-dimethyl-formamide | 10% |
1H-1,3-benzodiazol-6-ylmethanamine
2-[3-({[(2 R)-1-Cyclopentylpyrrolidinyl]methyl}amino)-6-methyl-2-oxo-1(2 H)-pyrazinyl]acetic acid hydrochloride
1H-1,3-benzodiazol-6-ylmethanamine
6-chloro-2-ethylimidazo[1,2-a]pyridine-3-carboxylic acid
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 70℃; for 2h; Inert atmosphere; |
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