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inquiryBenzeneethanamine,3-methoxy-4-(phenylmethoxy)-, hydrochloride (1:1)Appearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:It is an important raw material and intermediate used in Organic
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inquiryBenzeneethanamine,3-methoxy-4-(phenylmethoxy)-, hydrochloride (1:1) Application:Organic Chemicals
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inquiryBenzeneethanamine,3-methoxy-4-(phenylmethoxy)-, hydrochloride (1:1) cas 1860-57-7Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiry3-methoxy-4-benzyloxy-ω-nitrostyrolene
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
Conditions | Yield |
---|---|
Stage #1: 3-methoxy-4-benzyloxy-ω-nitrostyrolene With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 2.5h; Reflux; Stage #2: With water In tetrahydrofuran at 0℃; Stage #3: With hydrogenchloride In diethyl ether | 75% |
3-Methoxy-4-benzyloxy-N-tert.-butyloxycarbonyl-phenaethylamin
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
Conditions | Yield |
---|---|
Stage #1: 3-Methoxy-4-benzyloxy-N-tert.-butyloxycarbonyl-phenaethylamin With trifluoroacetic acid In dichloromethane at 0℃; for 0.666667h; Stage #2: With sodium hydrogencarbonate In dichloromethane; water Cooling with ice; Stage #3: With hydrogenchloride In diethyl ether | 64% |
Multi-step reaction with 2 steps 1: trifluoroacetic acid / dichloromethane / 0.67 h / 0 °C 2: hydrogenchloride / diethyl ether View Scheme |
2-(4-(benzyloxy)-3-methoxyphenyl)acetonitrile
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; sodium tetrahydroborate; cobalt(II) chloride 1.) MeOH, 20 deg C, 1 h; Multistep reaction; |
3-methoxy-4-(phenylmethoxy)benzaldehyde
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 96.6 percent / NaBH4 / methanol / 3 h 2: 93.5 percent / thionyl chloride / diethyl ether / 6 h 3: dimethylformamide / 168 h / Ambient temperature 4: 1.) cobaltous chloride hexahydrate, NaBH4, 2.) 3 N HCl / 1.) MeOH, 20 deg C, 1 h View Scheme | |
Multi-step reaction with 2 steps 1.1: ammonium acetate; acetic acid / 4 h / 90 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 2.5 h / 0 °C / Reflux 2.2: 0 °C View Scheme |
4-benzyloxy-3-methoxybenzyl alcohol
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 93.5 percent / thionyl chloride / diethyl ether / 6 h 2: dimethylformamide / 168 h / Ambient temperature 3: 1.) cobaltous chloride hexahydrate, NaBH4, 2.) 3 N HCl / 1.) MeOH, 20 deg C, 1 h View Scheme |
1-(benzyloxy)-4-(chloromethyl)-2-methoxybenzene
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dimethylformamide / 168 h / Ambient temperature 2: 1.) cobaltous chloride hexahydrate, NaBH4, 2.) 3 N HCl / 1.) MeOH, 20 deg C, 1 h View Scheme |
2-[4-(benzyloxy)-3-methoxyphenyl]ethylamine
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In diethyl ether |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: potassium carbonate / acetone / 2 h / Reflux 2.1: ammonium acetate; acetic acid / 4 h / 90 °C 3.1: lithium aluminium tetrahydride / tetrahydrofuran / 2.5 h / 0 °C / Reflux 3.2: 0 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: potassium carbonate / acetone / 2 h / Reflux 2.1: ammonium acetate; acetic acid / 4 h / 90 °C 3.1: lithium aluminium tetrahydride / tetrahydrofuran / 2.5 h / 0 °C / Reflux 3.2: 0 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: triethylamine / chloroform / 24 h / 20 °C 2: potassium carbonate / acetone / 12 h / Heating / reflux 3: trifluoroacetic acid / dichloromethane / 0.67 h / 0 °C 4: hydrogenchloride / diethyl ether View Scheme |
tert-butyl 4-hydroxy-3-methoxyphenethylcarbamate
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: potassium carbonate / acetone / 12 h / Heating / reflux 2: trifluoroacetic acid / dichloromethane / 0.67 h / 0 °C 3: hydrogenchloride / diethyl ether View Scheme |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
isobutyryl chloride
N-[2-(4-benzyloxy-3-methoxyphenyl)ethyl]isobutyramide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 96% |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
butyryl chloride
N-[2-(4-benzyloxy-3-methoxyphenyl)ethyl]butyramide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 94% |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
isopentanoyl chloride
N-[2-(4-benzyloxy-3-methoxyphenyl)ethyl]-3-methylbutyramide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 93% |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
propionyl chloride
N-[2-(4-benzyloxy-3-methoxyphenyl)ethyl]propionamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 90% |
With triethylamine In dichloromethane at 0℃; for 0.5 - 1h; | 90% |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
propionic acid anhydride
N-[2-(4-benzyloxy-3-methoxyphenyl)ethyl]propionamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; | 90% |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
cyclopropanecarboxylic acid chloride
N-[2-(4-benzyloxy-3-methoxyphenyl)ethyl]-2-cyclopropanecarboxamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 88% |
m-methoxyphenylacetic acid
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
N-(2-(4-(benzyloxy)-3-methoxyphenyl)ethyl)-2-(3-methoxyphenyl)acetamide
Conditions | Yield |
---|---|
Stage #1: m-methoxyphenylacetic acid With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 0.5h; Stage #2: [2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride In dichloromethane at 20℃; for 8h; | 87% |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
1-(4-(benzyloxy)-3-methoxyphenethyl)-4-(3-phenylpropyl)piperazine
Conditions | Yield |
---|---|
With potassium carbonate; sodium iodide In N,N-dimethyl-formamide at 70℃; for 5h; | 83% |
(3,5-dimethoxyphenyl)acetic acid
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
N-(2-(4-(benzyloxy)-3-methoxyphenyl)ethyl)-2-(3,5-dimethoxyphenyl)acetamide
Conditions | Yield |
---|---|
Stage #1: (3,5-dimethoxyphenyl)acetic acid With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 0.5h; Stage #2: [2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride In dichloromethane at 20℃; for 8h; | 81% |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
Cyclobutanecarbonyl chloride
N-[2-(4-benzyloxy-3-methoxyphenyl)ethyl]-2-cyclobutanecarboxamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 79% |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
phenylacetyl chloride
N-[2-(4-benzyloxy-3-methoxyphenyl)ethyl]-2-phenylacetylamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 63% |
5-benzyloxy-4-methoxy-2-nitrophenylacetic acid
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
N-<4-Benzyloxy-4-methoxyphenethyl>-5-benzyloxy-4-methoxy-2-nitrophenylacetamide
Conditions | Yield |
---|---|
With sodium hydroxide In chloroform; water for 4h; Ambient temperature; | 56% |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
1-<5-benzyloxy-4-methoxy-2-nitrobenzyl>-7-benzyloxy-6-methoxy-3,4-dihydroisoquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 56 percent / 2 N NaOH / CHCl3; H2O / 4 h / Ambient temperature 2: 72 percent / POCl3 / acetonitrile / 2 h / Heating View Scheme |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
1-<5-Benzyloxy-4-methoxy-2-nitrobenzyl>-7-benzyloxy-6-methoxy-1,2,3,4-tetrahydroisoquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 56 percent / 2 N NaOH / CHCl3; H2O / 4 h / Ambient temperature 2: 72 percent / POCl3 / acetonitrile / 2 h / Heating 3: 81 percent / NaBH4 / methanol / 2 h / Ambient temperature View Scheme |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
Conditions | Yield |
---|---|
With thionyl chloride; triethylamine In water; ethyl acetate |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
Conditions | Yield |
---|---|
With triethylamine In ethyl acetate |
C16H14O6S
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
C32H33NO8S
Conditions | Yield |
---|---|
With triethylamine In methanol for 5h; Reflux; |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
(S)-2-hydroxy-3,11-dimethoxy-5,8,13,13a-tetrahydro-6H-dibenzo[a,g]quinolizine
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 20 °C 1.2: 8 h / 20 °C 2.1: trichlorophosphate / acetonitrile / 0.5 h / Reflux 3.1: [N-[(1R,2R)-2-(amino-κN)-1,2-diphenylethyl]-4-methylbenzenesulfonamidato-κN]chloro[(1,2, 3,4,5,6-η)-1-methyl-4-(1-methylethyl)benzene]-ruthenium; formic acid; triethylamine / N,N-dimethyl-formamide / 10 h / 20 °C 3.2: 20 °C / pH 8 4.1: formic acid / 2 h / 25 °C 5.1: hydrogenchloride / ethanol; water / Reflux 5.2: 0 °C / pH 9 View Scheme |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
(S)-2-hydroxy-3,9,11-trimethoxy-5,8,13,13a-tetrahydro-6H-dibenzo-[a,g]quinolizine
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 20 °C 1.2: 8 h / 20 °C 2.1: trichlorophosphate / acetonitrile / 0.5 h / Reflux 3.1: [N-[(1R,2R)-2-(amino-κN)-1,2-diphenylethyl]-4-methylbenzenesulfonamidato-κN]chloro[(1,2, 3,4,5,6-η)-1-methyl-4-(1-methylethyl)benzene]-ruthenium; formic acid; triethylamine / N,N-dimethyl-formamide / 10 h / 20 °C 3.2: 20 °C / pH 8 4.1: formic acid / 2 h / 50 °C 5.1: hydrogenchloride / ethanol; water / Reflux 5.2: 0 °C / pH 9 View Scheme |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
7-(benzyloxy)-1-((3,5-dimethoxyphenyl)methyl)-6-methoxy-3,4-dihydroisoquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 20 °C 1.2: 8 h / 20 °C 2.1: trichlorophosphate / acetonitrile / 0.5 h / Reflux View Scheme |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
C25H27NO3
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 20 °C 1.2: 8 h / 20 °C 2.1: trichlorophosphate / acetonitrile / 0.5 h / Reflux 3.1: [N-[(1R,2R)-2-(amino-κN)-1,2-diphenylethyl]-4-methylbenzenesulfonamidato-κN]chloro[(1,2, 3,4,5,6-η)-1-methyl-4-(1-methylethyl)benzene]-ruthenium; formic acid; triethylamine / N,N-dimethyl-formamide / 10 h / 20 °C 3.2: 20 °C / pH 8 View Scheme |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
(S)-7-(benzyloxy)-1-((3,5-dimethoxyphenyl)methyl)-6-methoxy-1,2,3,4-tetrahydroisoquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 20 °C 1.2: 8 h / 20 °C 2.1: trichlorophosphate / acetonitrile / 0.5 h / Reflux 3.1: [N-[(1R,2R)-2-(amino-κN)-1,2-diphenylethyl]-4-methylbenzenesulfonamidato-κN]chloro[(1,2, 3,4,5,6-η)-1-methyl-4-(1-methylethyl)benzene]-ruthenium; formic acid; triethylamine / N,N-dimethyl-formamide / 10 h / 20 °C 3.2: 20 °C / pH 8 View Scheme |
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride
(S)-2-benzyloxy-3,11-dimethoxy-5,8,13,13a-tetrahydro-6H-dibenzo[a,g]quinolizine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 20 °C 1.2: 8 h / 20 °C 2.1: trichlorophosphate / acetonitrile / 0.5 h / Reflux 3.1: [N-[(1R,2R)-2-(amino-κN)-1,2-diphenylethyl]-4-methylbenzenesulfonamidato-κN]chloro[(1,2, 3,4,5,6-η)-1-methyl-4-(1-methylethyl)benzene]-ruthenium; formic acid; triethylamine / N,N-dimethyl-formamide / 10 h / 20 °C 3.2: 20 °C / pH 8 4.1: formic acid / 2 h / 25 °C View Scheme |
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