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inquirymethanol
1-(3-bromophenyl)-1-propanone
1-(3-bromophenyl)-2-methylpropane-1-one
Conditions | Yield |
---|---|
With C34H27IrN2P(1+)*C32H12BF24(1-); caesium carbonate at 65℃; for 24h; Inert atmosphere; | 93% |
With C21H17ClN5ORu(1+)*Cl(1-); potassium tert-butylate at 85℃; for 24h; Inert atmosphere; Schlenk technique; Glovebox; Sealed tube; | 87% |
With C34H27MnNO3P2(1+)*Br(1-); caesium carbonate at 85℃; for 24h; Schlenk technique; Inert atmosphere; | 79% |
methanol
1-(3-Bromophenyl)ethanone
1-(3-bromophenyl)-2-methylpropane-1-one
Conditions | Yield |
---|---|
With C21H17ClN5ORu(1+)*Cl(1-); potassium tert-butylate at 100℃; for 24h; Inert atmosphere; Schlenk technique; Glovebox; Sealed tube; | 87% |
1-(2-methylprop-1-en-1-yl)pyrrolidine
3-bromobenzoic acid isopropylamide
1-(3-bromophenyl)-2-methylpropane-1-one
Conditions | Yield |
---|---|
Stage #1: 3-bromobenzoic acid isopropylamide With 2-fluoropyridine; trifluoromethylsulfonic anhydride In dichloromethane at 0℃; for 0.333333h; Stork Enamine Alkylation; Inert atmosphere; Schlenk technique; Stage #2: 1-(2-methylprop-1-en-1-yl)pyrrolidine In dichloromethane at 0 - 20℃; for 3h; Stork Enamine Alkylation; Inert atmosphere; Schlenk technique; Stage #3: With hydrogenchloride In dichloromethane; water at 20℃; Stork Enamine Alkylation; Inert atmosphere; Schlenk technique; | 81% |
3-bromobenzoyl chloride
isopropylmagnesium chloride
1-(3-bromophenyl)-2-methylpropane-1-one
Conditions | Yield |
---|---|
With Bis<2-(N,N-dimethylamino)aethyl>aether In tetrahydrofuran Grignard reaction; cooling; | 75% |
(3-bromophenyl)oxoacetic acid
isobutyraldehyde
1-(3-bromophenyl)-2-methylpropane-1-one
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; iron(III)-acetylacetonate; di-tert-butyl peroxide In ethyl acetate at 120℃; for 2h; Sealed tube; | 65% |
With dipotassium peroxodisulfate; iron(III)-acetylacetonate; di-tert-butyl peroxide In ethyl acetate at 120℃; for 12h; | 65% |
1-(3-bromophenyl)-1-propanone
methyl iodide
1-(3-bromophenyl)-2-methylpropane-1-one
Conditions | Yield |
---|---|
(i) NaNH2, toluene, (ii) /BRN= 969135/; Multistep reaction; |
1-(3-bromophenyl)-2-methylpropane-1-one
Conditions | Yield |
---|---|
With aluminum oxide; pyridinium chlorochromate In dichloromethane at 20℃; for 1h; | 2.1 g |
Conditions | Yield |
---|---|
Stage #1: m-trifluoromethylphenyl iodide With TurboGrignard In tetrahydrofuran at -20℃; for 0.5h; Inert atmosphere; Stage #2: 1-(3-bromophenyl)-2-methylpropane-1-one With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In tetrahydrofuran at 25℃; for 0.0833333h; Kumada coupling reaction; Inert atmosphere; | 87% |
Conditions | Yield |
---|---|
With sodium t-butanolate In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; | 86% |
1-(3-bromophenyl)-2-methylpropane-1-one
trimethyl orthoformate
2-(3-bromophenyl)-2-isopropyl-1,3-dioxolane
Conditions | Yield |
---|---|
toluene-4-sulfonic acid In toluene at 60℃; for 48h; | 80% |
4-iodobenzoic acid ethyl ester
1-(3-bromophenyl)-2-methylpropane-1-one
3'-isobutyrylbiphenyl-4-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
Stage #1: 4-iodobenzoic acid ethyl ester With TurboGrignard In tetrahydrofuran at -20℃; for 0.5h; Inert atmosphere; Stage #2: 1-(3-bromophenyl)-2-methylpropane-1-one With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In tetrahydrofuran at 25℃; for 0.0833333h; Kumada coupling reaction; Inert atmosphere; | 75% |
1-(3-bromophenyl)-2-methylpropane-1-one
1-(2-bromoethynyl)naphthalene
C22H17BrO
Conditions | Yield |
---|---|
With sodium t-butanolate In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; | 64% |
1-(3-bromophenyl)-2-methylpropane-1-one
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In tetrahydrofuran; dimethyl sulfoxide at 25℃; for 24h; Negishi Coupling; Inert atmosphere; diastereoselective reaction; | 58% |
3-bromo-1-trifluoromethylbenzene
1-(3-bromophenyl)-2-methylpropane-1-one
2-methyl-1-(3'-trifluoromethylbiphenyl-3-yl)-propan-1-one
Conditions | Yield |
---|---|
Stage #1: 3-bromo-1-trifluoromethylbenzene With TurboGrignard Inert atmosphere; Stage #2: 1-(3-bromophenyl)-2-methylpropane-1-one With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In tetrahydrofuran at 25℃; for 1h; Kumada coupling reaction; Inert atmosphere; | 46% |
1-(3-bromophenyl)-2-methylpropane-1-one
fullerene-C60
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; palladium diacetate; trifluoroacetic acid In chlorobenzene at 120℃; for 10h; | 28% |
1-(3-bromophenyl)-2-methylpropane-1-one
methyl iodide
3'-bromo-2,2-dimethylpropiophenone
Conditions | Yield |
---|---|
(i) NaNH2, toluene, (ii) /BRN= 969135/; Multistep reaction; |
1-(3-bromophenyl)-2-methylpropane-1-one
m-Brom-neopentyl-benzol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (i) NaNH2, toluene, (ii) /BRN= 969135/ 2: N2H4, KOH View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: (i) NaNH2, toluene, (ii) /BRN= 969135/ 2: N2H4, KOH 3: (i) nBuLi, Et2O, hexane, (ii) /BRN= 1209232/ View Scheme |
1-(3-bromophenyl)-2-methylpropane-1-one
C13H15BrN2O2
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium cyanide / 120 °C 2: 100 °C View Scheme |
1-(3-bromophenyl)-2-methylpropane-1-one
C13H15BrN2OS
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: potassium cyanide / 120 °C 2: 100 °C 3: Lawessons reagent / 100 °C View Scheme |
1-(3-bromophenyl)-2-methylpropane-1-one
C13H16BrN3O
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: potassium cyanide / 120 °C 2: 100 °C 3: Lawessons reagent / 100 °C 4: tert.-butylhydroperoxide; ammonium hydroxide View Scheme |
1-(3-bromophenyl)-2-methylpropane-1-one
C19H20ClN3O
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: potassium cyanide / 120 °C 2: 100 °C 3: Lawessons reagent / 100 °C 4: tert.-butylhydroperoxide; ammonium hydroxide 5: potassium carbonate / isopropyl alcohol / 110 °C / Microwave irradiation View Scheme |
1-(3-bromophenyl)-2-methylpropane-1-one
ammonium carbonate
C12H13BrN2O2
Conditions | Yield |
---|---|
With potassium cyanide at 120℃; Bucherer-Bergs reaction; |
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride In ethanol; water at 80℃; for 2h; Overall yield = 81 %; Overall yield = 1150.2 mg; | A n/a B n/a |
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