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Destruxin B (9CI)

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Shanghai Upbio Tech Co.,Ltd

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Destruxin B (9CI)

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Henan Tianfu Chemical Co., Ltd.

destruxin B Basic information Product Name: destruxin B Synonyms: destruxin B;N-[N-[(2R)-1-Oxo-2-hydroxy-4-methylpentyl]-L-Pro-L-Ile-N-methyl-L-V

2503-26-6 destruxin B C30H51N5O7

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We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as primary a

(3R,10R,13S,16S,19S)-16-[(2S)-butan-2-yl]-10,11,14-trimethyl-3-(2-methylpropyl)-13-propan-2-yl-4-oxa-1,8,11,14,17-pentazabicyclo[17.3.0]docosane-2,5,9,12,15,18-hexone

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Antimex Chemical Limied

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Hangzhou Fandachem Co.,Ltd

Destruxin B (9CI) cas 2503-26-6Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

Destruxin B (9CI) cas 2503-26-6

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Zibo Hangyu Biotechnology Development Co., Ltd

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ZHEJIANG JIUZHOU CHEM CO.,LTD

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Sparrow Chemical Co.,Ltd

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NovaChemistry

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Destruxin B

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Synthetic route

: (S)-2-[((S)-2-{[(2S,3S)-2-({(S)-1-[(R)-2-(3-Amino-propionyloxy)-4-methyl-pentanoyl]-pyrrolidine-2-carbonyl}-amino)-3-methyl-pentanoyl]-methyl-amino}-3-methyl-butyryl)-methyl-amino]-propionic acid

: 2503-26-6
destruxin B

Conditions

Conditions	Yield
With sodium hydrogencarbonate In dichloromethane; water	65%

: 187753-76-0
C30H51N5O7N2H4(C5H8O2)2

: 2503-26-6
destruxin B

Conditions

Conditions	Yield
Stage #1: C30H51N5O7N2H4(C5H8O2)2 With trifluoroacetic acid In dichloromethane at 20℃; for 0.5h; Stage #2: With hydrogenchloride; sodium nitrite for 0.25h; Stage #3: With sodium hydrogencarbonate In dichloromethane at 20℃; for 15h; Further stages.;	65%
Multi-step reaction with 3 steps 1: TFA / CH2Cl2 2: NaNO3, HCl / H2O 3: 65 percent / NaHCO3 / CH2Cl2; H2O View Scheme

: 20312-37-2
(R)-2-hydroxy-4-methylpentanoic acid

: 2503-26-6
destruxin B

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1.1: 93 percent / DCC; HOBt hydrate / CH2Cl2 / 21 h / 0 - 20 °C 2.1: 98 percent / DCC; DMAP / CH2Cl2 / 21 h / 0 - 20 °C 3.1: H2 / Pd/C / methanol / 2 h 4.1: 233 mg / DCC; HOBt hydrate / CH2Cl2 / 25 h / 0 - 20 °C 5.1: TFA / CH2Cl2 / 0.5 h / 20 °C 5.2: NaNO2; aq. HCl / 0.25 h 5.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme
Multi-step reaction with 5 steps 1.1: 93 percent / DCC; HOBt hydrate / CH2Cl2 / 21 h / 0 - 20 °C 2.1: H2 / Pd/C / methanol / 2 h 3.1: 250 mg / DCC; HOBt*H2O / CH2Cl2 / 24.17 h / 0 - 20 °C 4.1: 88 percent / DCC; DMAP / CH2Cl2 / 25 h / 0 - 20 °C 5.1: TFA / CH2Cl2 / 0.5 h / 20 °C 5.2: NaNO2; aq. HCl / 0.25 h 5.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme
Multi-step reaction with 7 steps 1: 95 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole 2: 95 percent / dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine 3: H2 / Pd-C 4: 97 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole,iPr2EtN / CH2Cl2 / 24 h / 0 - 20 °C 5: TFA / CH2Cl2 6: NaNO3, HCl / H2O 7: 65 percent / NaHCO3 / CH2Cl2; H2O View Scheme

: 383396-86-9
N'-{(S)-2-[Methyl-((S)-3-methyl-2-methylamino-butyryl)-amino]-propionyl}-hydrazinecarboxylic acid tert-butyl ester

: 2503-26-6
destruxin B

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1.1: 345 mg / BOP-Cl; i-Pr2EtN / CH2Cl2 / 14.5 h / 0 - 20 °C 2.1: H2 / Pd/C / methanol / 2 h 3.1: 233 mg / DCC; HOBt hydrate / CH2Cl2 / 25 h / 0 - 20 °C 4.1: TFA / CH2Cl2 / 0.5 h / 20 °C 4.2: NaNO2; aq. HCl / 0.25 h 4.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme
Multi-step reaction with 5 steps 1.1: 345 mg / BOP-Cl; i-Pr2EtN / CH2Cl2 / 14.5 h / 0 - 20 °C 2.1: H2 / Pd/C / methanol / 2 h 3.1: 250 mg / DCC; HOBt*H2O / CH2Cl2 / 24.17 h / 0 - 20 °C 4.1: 88 percent / DCC; DMAP / CH2Cl2 / 25 h / 0 - 20 °C 5.1: TFA / CH2Cl2 / 0.5 h / 20 °C 5.2: NaNO2; aq. HCl / 0.25 h 5.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme
Multi-step reaction with 6 steps 1: 84 percent / N,N-bis(2-oxo-3-oxazolidinyl)phosphonic chloride, iPr2EtN / CH2Cl2 / 14 h / 0 - 20 °C 2: H2 / Pd-C 3: 97 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole,iPr2EtN / CH2Cl2 / 24 h / 0 - 20 °C 4: TFA / CH2Cl2 5: NaNO3, HCl / H2O 6: 65 percent / NaHCO3 / CH2Cl2; H2O View Scheme

: 187753-73-7
(S)-1-((R)-2-Hydroxy-4-methyl-pentanoyl)-pyrrolidine-2-carboxylic acid benzyl ester

: 2503-26-6
destruxin B

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1.1: 98 percent / DCC; DMAP / CH2Cl2 / 21 h / 0 - 20 °C 2.1: H2 / Pd/C / methanol / 2 h 3.1: 233 mg / DCC; HOBt hydrate / CH2Cl2 / 25 h / 0 - 20 °C 4.1: TFA / CH2Cl2 / 0.5 h / 20 °C 4.2: NaNO2; aq. HCl / 0.25 h 4.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme
Multi-step reaction with 4 steps 1.1: H2 / Pd/C / methanol / 2 h 2.1: 250 mg / DCC; HOBt*H2O / CH2Cl2 / 24.17 h / 0 - 20 °C 3.1: 88 percent / DCC; DMAP / CH2Cl2 / 25 h / 0 - 20 °C 4.1: TFA / CH2Cl2 / 0.5 h / 20 °C 4.2: NaNO2; aq. HCl / 0.25 h 4.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme
Multi-step reaction with 6 steps 1: 95 percent / dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine 2: H2 / Pd-C 3: 97 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole,iPr2EtN / CH2Cl2 / 24 h / 0 - 20 °C 4: TFA / CH2Cl2 5: NaNO3, HCl / H2O 6: 65 percent / NaHCO3 / CH2Cl2; H2O View Scheme

: 1026656-54-1
(S)-1-[(R)-2-(3-tert-Butoxycarbonylamino-propionyloxy)-4-methyl-pentanoyl]-pyrrolidine-2-carboxylic acid

: 2503-26-6
destruxin B

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1.1: 233 mg / DCC; HOBt hydrate / CH2Cl2 / 25 h / 0 - 20 °C 2.1: TFA / CH2Cl2 / 0.5 h / 20 °C 2.2: NaNO2; aq. HCl / 0.25 h 2.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme
Multi-step reaction with 4 steps 1: 97 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole,iPr2EtN / CH2Cl2 / 24 h / 0 - 20 °C 2: TFA / CH2Cl2 3: NaNO3, HCl / H2O 4: 65 percent / NaHCO3 / CH2Cl2; H2O View Scheme

: N'-[(S)-2-({(S)-2-[((2S,3S)-2-Amino-3-methyl-pentanoyl)-methyl-amino]-3-methyl-butyryl}-methyl-amino)-propionyl]-hydrazinecarboxylic acid tert-butyl ester

: 2503-26-6
destruxin B

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1.1: 233 mg / DCC; HOBt hydrate / CH2Cl2 / 25 h / 0 - 20 °C 2.1: TFA / CH2Cl2 / 0.5 h / 20 °C 2.2: NaNO2; aq. HCl / 0.25 h 2.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme
Multi-step reaction with 3 steps 1.1: 250 mg / DCC; HOBt*H2O / CH2Cl2 / 24.17 h / 0 - 20 °C 2.1: 88 percent / DCC; DMAP / CH2Cl2 / 25 h / 0 - 20 °C 3.1: TFA / CH2Cl2 / 0.5 h / 20 °C 3.2: NaNO2; aq. HCl / 0.25 h 3.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme
Multi-step reaction with 4 steps 1: 97 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole,iPr2EtN / CH2Cl2 / 24 h / 0 - 20 °C 2: TFA / CH2Cl2 3: NaNO3, HCl / H2O 4: 65 percent / NaHCO3 / CH2Cl2; H2O View Scheme

: 187753-74-8
Cbz-MeVal-MeAla-NHNHBoc

: 2503-26-6
destruxin B

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1.1: H2 / Pd/C / methanol / 0.5 h / 20 °C 2.1: 345 mg / BOP-Cl; i-Pr2EtN / CH2Cl2 / 14.5 h / 0 - 20 °C 3.1: H2 / Pd/C / methanol / 2 h 4.1: 233 mg / DCC; HOBt hydrate / CH2Cl2 / 25 h / 0 - 20 °C 5.1: TFA / CH2Cl2 / 0.5 h / 20 °C 5.2: NaNO2; aq. HCl / 0.25 h 5.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme
Multi-step reaction with 6 steps 1.1: H2 / Pd/C / methanol / 0.5 h / 20 °C 2.1: 345 mg / BOP-Cl; i-Pr2EtN / CH2Cl2 / 14.5 h / 0 - 20 °C 3.1: H2 / Pd/C / methanol / 2 h 4.1: 250 mg / DCC; HOBt*H2O / CH2Cl2 / 24.17 h / 0 - 20 °C 5.1: 88 percent / DCC; DMAP / CH2Cl2 / 25 h / 0 - 20 °C 6.1: TFA / CH2Cl2 / 0.5 h / 20 °C 6.2: NaNO2; aq. HCl / 0.25 h 6.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme
Multi-step reaction with 7 steps 1: H2 / Pd-C 2: 84 percent / N,N-bis(2-oxo-3-oxazolidinyl)phosphonic chloride, iPr2EtN / CH2Cl2 / 14 h / 0 - 20 °C 3: H2 / Pd-C 4: 97 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole,iPr2EtN / CH2Cl2 / 24 h / 0 - 20 °C 5: TFA / CH2Cl2 6: NaNO3, HCl / H2O 7: 65 percent / NaHCO3 / CH2Cl2; H2O View Scheme

: 55739-22-5
(S)-1-[(R)-2-(3-tert-Butoxycarbonylamino-propionyloxy)-4-methyl-pentanoyl]-pyrrolidine-2-carboxylic acid benzyl ester

: 2503-26-6
destruxin B

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: H2 / Pd/C / methanol / 2 h 2.1: 233 mg / DCC; HOBt hydrate / CH2Cl2 / 25 h / 0 - 20 °C 3.1: TFA / CH2Cl2 / 0.5 h / 20 °C 3.2: NaNO2; aq. HCl / 0.25 h 3.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme
Multi-step reaction with 5 steps 1: H2 / Pd-C 2: 97 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole,iPr2EtN / CH2Cl2 / 24 h / 0 - 20 °C 3: TFA / CH2Cl2 4: NaNO3, HCl / H2O 5: 65 percent / NaHCO3 / CH2Cl2; H2O View Scheme

: 187753-75-9
Cbz-Ile-MeVal-MeAla-NHNHBoc

: 2503-26-6
destruxin B

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: H2 / Pd/C / methanol / 2 h 2.1: 233 mg / DCC; HOBt hydrate / CH2Cl2 / 25 h / 0 - 20 °C 3.1: TFA / CH2Cl2 / 0.5 h / 20 °C 3.2: NaNO2; aq. HCl / 0.25 h 3.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme
Multi-step reaction with 4 steps 1.1: H2 / Pd/C / methanol / 2 h 2.1: 250 mg / DCC; HOBt*H2O / CH2Cl2 / 24.17 h / 0 - 20 °C 3.1: 88 percent / DCC; DMAP / CH2Cl2 / 25 h / 0 - 20 °C 4.1: TFA / CH2Cl2 / 0.5 h / 20 °C 4.2: NaNO2; aq. HCl / 0.25 h 4.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme
Multi-step reaction with 5 steps 1: H2 / Pd-C 2: 97 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole,iPr2EtN / CH2Cl2 / 24 h / 0 - 20 °C 3: TFA / CH2Cl2 4: NaNO3, HCl / H2O 5: 65 percent / NaHCO3 / CH2Cl2; H2O View Scheme

: (S)-1-((R)-2-Hydroxy-4-methyl-pentanoyl)-pyrrolidine-2-carboxylic acid

: 2503-26-6
destruxin B

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: 250 mg / DCC; HOBt*H2O / CH2Cl2 / 24.17 h / 0 - 20 °C 2.1: 88 percent / DCC; DMAP / CH2Cl2 / 25 h / 0 - 20 °C 3.1: TFA / CH2Cl2 / 0.5 h / 20 °C 3.2: NaNO2; aq. HCl / 0.25 h 3.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme

: 383397-18-0
N'-[(S)-2-({(S)-2-[((2S,3S)-2-{[(S)-1-((R)-2-Hydroxy-4-methyl-pentanoyl)-pyrrolidine-2-carbonyl]-amino}-3-methyl-pentanoyl)-methyl-amino]-3-methyl-butyryl}-methyl-amino)-propionyl]-hydrazinecarboxylic acid tert-butyl ester

: 2503-26-6
destruxin B

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1.1: 88 percent / DCC; DMAP / CH2Cl2 / 25 h / 0 - 20 °C 2.1: TFA / CH2Cl2 / 0.5 h / 20 °C 2.2: NaNO2; aq. HCl / 0.25 h 2.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme

: 41324-66-7
H-Pro-OBzl

: 2503-26-6
destruxin B

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1.1: 93 percent / DCC; HOBt hydrate / CH2Cl2 / 21 h / 0 - 20 °C 2.1: 98 percent / DCC; DMAP / CH2Cl2 / 21 h / 0 - 20 °C 3.1: H2 / Pd/C / methanol / 2 h 4.1: 233 mg / DCC; HOBt hydrate / CH2Cl2 / 25 h / 0 - 20 °C 5.1: TFA / CH2Cl2 / 0.5 h / 20 °C 5.2: NaNO2; aq. HCl / 0.25 h 5.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme
Multi-step reaction with 5 steps 1.1: 93 percent / DCC; HOBt hydrate / CH2Cl2 / 21 h / 0 - 20 °C 2.1: H2 / Pd/C / methanol / 2 h 3.1: 250 mg / DCC; HOBt*H2O / CH2Cl2 / 24.17 h / 0 - 20 °C 4.1: 88 percent / DCC; DMAP / CH2Cl2 / 25 h / 0 - 20 °C 5.1: TFA / CH2Cl2 / 0.5 h / 20 °C 5.2: NaNO2; aq. HCl / 0.25 h 5.3: 65 percent / aq. NaHCO3 / CH2Cl2 / 15 h / 20 °C View Scheme
Multi-step reaction with 7 steps 1: 95 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole 2: 95 percent / dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine 3: H2 / Pd-C 4: 97 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole,iPr2EtN / CH2Cl2 / 24 h / 0 - 20 °C 5: TFA / CH2Cl2 6: NaNO3, HCl / H2O 7: 65 percent / NaHCO3 / CH2Cl2; H2O View Scheme

: 3-Amino-propionic acid (R)-1-((S)-2-{(1S,2S)-1-[((S)-1-{[(S)-2-(N'-tert-butoxycarbonyl-hydrazino)-1-methyl-2-oxo-ethyl]-methyl-carbamoyl}-2-methyl-propyl)-methyl-carbamoyl]-2-methyl-butylcarbamoyl}-pyrrolidine-1-carbonyl)-3-methyl-butyl ester

: 2503-26-6
destruxin B

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: NaNO3, HCl / H2O 2: 65 percent / NaHCO3 / CH2Cl2; H2O View Scheme

: C30H53N5O8

: 2503-26-6
destruxin B

Conditions

Conditions	Yield
With 2-methyl-6-nitrobenzoic anhydride; 4-(dimethylamino)pyridine N-oxide In dichloromethane at 30℃; for 48h; Inert atmosphere;

: 2503-26-6
destruxin B

: hydroxydestruxin B

Conditions

Conditions	Yield
With leaves of Sinapis alba cultivar Ochre In water; acetonitrile for 48h;

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