As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:26201-32-1
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inquiryhigh purity Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:meet customer's demand Application:organic synthesis Transportation:by sea or by air Port:Shanghai, Qingdao
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Min.Order:1 Gram
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Min.Order:5 Kiloliter
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inquiryTitanium,oxo[29H,31H-phthalocyaninato(2-)-kN29,kN30,kN31,kN32]-, (SP-5-12)- Henan Tianfu Chemical Co.,LTD was built in 2009 with an ISO certificate in the past 5 years, we have grown up as a famous fine chemicals supplier in china and we had esta
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Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
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Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryTitanyl phthalocyanine CAS:26201-32-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
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Min.Order:1 Gram
Negotiable
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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Min.Order:1 Kilogram
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Cas:26201-32-1
Min.Order:1 Kilogram
Negotiable
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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Cas:26201-32-1
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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Type:Other
inquirydichloro(phthalocyaninato)titanium(IV)
water
oxotitanium(IV) phthalocyanine
Conditions | Yield |
---|---|
In pyridine Ti-complex was boiled in aq. pyridine for 2 h, cooled; filtered, washed with water, dried in vacuo at 100°C; elem. anal.; | 97% |
With hydrogenchloride In DMF (N,N-dimethyl-formamide); water at 100 - 120℃; for 1h; |
Conditions | Yield |
---|---|
In quinoline at 180℃; for 6h; Product distribution / selectivity; | 76.8% |
With thiourea In further solvent(s) TiCl4 was mixed with heptanol, heated to boiling, ligand was added, withor without thiourea, heated to 170°C, kept for 6 h; cooled, filtered, washed with toluene and MeOH, extd. with MeOH in Soxhlet for 4 h, dried in air; elem. anal.; | 60% |
In ethanol at -20.01℃; under 46504.7 Torr; for 1h; | 60% |
isoindole-1,3-diylidenediamine
titanium tetra-n-propoxide
phthalonitrile
oxotitanium(IV) phthalocyanine
Conditions | Yield |
---|---|
In 1-methyl-pyrrolidin-2-one at 198℃; for 2h; Product distribution / selectivity; Heating / reflux; | 76% |
isoindole-1,3-diylidenediamine
oxotitanium(IV) phthalocyanine
B
butan-1-ol
Conditions | Yield |
---|---|
In 1-chloronaphthalene (CINp) at 140 - 200℃; for 2h; Product distribution / selectivity; | A 72% B n/a |
Conditions | Yield |
---|---|
In 1-Chloronaphthalene at 195℃; for 3h; Product distribution / selectivity; Heating / reflux; | 70% |
In 1-methyl-pyrrolidin-2-one at 50 - 95℃; for 6h; Product distribution / selectivity; | 1.5% |
In 1-methyl-pyrrolidin-2-one at 24 - 100℃; Product distribution / selectivity; Electrochemical reaction; | |
In ethylene glycol at 24 - 100℃; Product distribution / selectivity; Electrochemical reaction; | |
In sulfolane Inert atmosphere; |
dichlorotitanium phthalocyanine
oxotitanium(IV) phthalocyanine
Conditions | Yield |
---|---|
With hydrogenchloride; N,N-dimethyl-formamide In water at 100 - 120℃; for 1h; pH=>= 6; |
Conditions | Yield |
---|---|
With pentan-1-ol; benzamide In xylene at 144℃; for 6h; Heating / reflux; |
oxygen
titanium tetrachloride
phthalonitrile
oxotitanium(IV) phthalocyanine
Conditions | Yield |
---|---|
In 1-Chloronaphthalene at 25 - 210℃; for 5h; | |
In Diphenylmethane; 1,1,2,2-tetrachloroethane at 40 - 210℃; for 6 - 8h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
With tetrabutoxytitanium In nonyl alcohol at 160 - 170℃; for 0.1 - 6h; Product distribution / selectivity; Microwave and ultrasonic energy; |
isoindole-1,3-diylidenediamine
oxotitanium(IV) phthalocyanine
Conditions | Yield |
---|---|
With quinoline; tetrabutoxytitanium at 170 - 180℃; for 0.1 - 6h; Product distribution / selectivity; |
4,5-dichlorophthalonitrile
phthalonitrile
oxotitanium(IV) phthalocyanine
Conditions | Yield |
---|---|
With benzamide In pentan-1-ol; xylene Reflux; |
Conditions | Yield |
---|---|
With tin(IV) chloride In octanol at 155 - 159℃; for 6h; Inert atmosphere; | 22.77 g |
oxotitanium(IV) phthalocyanine
2,6-diisopropylphenyl isocyanate
(2,6-diisopropylphenylimido)phthalocyaninatotitanium(IV)
Conditions | Yield |
---|---|
In further solvent(s) byproducts: CO2; under N2; mixt. of Ti complex and ((CH3)2CH)2C6H3NCO (20-fold excess) inchloronaphthalene heated at 180°C for 6 h, released CO2 replaced by N2 from time to time; mixt. cooled, pptn. by addn. of hexane, solid filtered off, extd. repeatedly with MeCN and toluene (10x50 mL each) under reflux, washed with pentane, dried at 120°C under vac. for 3 h; elem. anal.; | 83% |
oxotitanium(IV) phthalocyanine
p-Tolylisocyanate
(N,N'-di(p-tolyl)ureato-κ2N,N')phthalocyaninatotitanium(IV)
Conditions | Yield |
---|---|
In further solvent(s) byproducts: CO2; under N2; mixt. of Ti complex and p-tolyl isocyanate in chloronaphthalene heated at 180°C for 6 h, released CO2 replaced by N2 from time to time; soln. cooled, pptn. by addn. of hexane, solid filtered off, extd. with rMeCN and toluene (10x50 mL each) under reflux, washed with pentane, dried at 120°C under vac. for 3 h; elem. anal.; | 76% |
In further solvent(s) according to Darwish, W. et al., Acta Cryst. E61 2005, m1280-1282; Darwish, W., Dissertation, Philipps University, Marburg, Germany, 2006; solvent: chloronaphthalene; |
Conditions | Yield |
---|---|
With fluorenone radical anion sodium contact ion pair In 1,2-dichloro-benzene at 80℃; for 24h; | 74% |
Conditions | Yield |
---|---|
In further solvent(s) byproducts: CO2; under N2; mixt. of Ti complex and mesityl isocyanate in chloronaphthalene heated at 180°C for 6 h, released CO2 replaced by N2 from time to time; soln. cooled, pptn. by addn. of hexane, solid filtered off, extd. with rMeCN and toluene (10x50 mL each) under reflux, washed with pentane, dried at 120°C under vac. for 3 h; elem. anal.; | 73% |
oxotitanium(IV) phthalocyanine
tetrahexylammonium bromide
1,2-dichloro-benzene
Conditions | Yield |
---|---|
With fluorenone radical anion sodium contact ion pair at 80℃; for 24h; | 66% |
oxotitanium(IV) phthalocyanine
triptycene
tetramethylphosphonium bromide
1,2-dichloro-benzene
Conditions | Yield |
---|---|
Stage #1: oxotitanium(IV) phthalocyanine; tetramethylphosphonium bromide; 1,2-dichloro-benzene With fluorenone radical anion sodium contact ion pair at 100℃; for 2h; Glovebox; Inert atmosphere; Stage #2: triptycene In benzonitrile at 20 - 100℃; for 3h; | 65% |
Conditions | Yield |
---|---|
With triphenylphosphine In further solvent(s) (N2); Schlenk techniques; phthalocyanine deriv. and P4S10 heated in chloronaphthalene at 160°C for 10 h; pptd. by addn. of hexane; washedby extn. with refluxing MeCN, toluene; washed with pentane; dried at 12 0.degre.C for 1 h under 1E-3 mbar; heated with triphenylphosphine to a melt at 160°C for 4 h; washedwith refluxing MeCN, toluene; washed with ether; dried at 120.degre.C f or 1 h under 1E-3 mbar; | 57% |
oxotitanium(IV) phthalocyanine
4-aza-1-methylazoniabicyclo<2.2.2>octane iodide
Conditions | Yield |
---|---|
With fluorenone radical anion sodium contact ion pair In 1,2-dichloro-benzene at 100℃; for 24h; | 43% |
oxotitanium(IV) phthalocyanine
4-aza-1-methylazoniabicyclo<2.2.2>octane iodide
Conditions | Yield |
---|---|
With fluorenone radical anion sodium contact ion pair In 1,2-dichloro-benzene at 100℃; for 24h; | 38% |
Conditions | Yield |
---|---|
Stage #1: oxotitanium(IV) phthalocyanine; N-methyl-1,4-diazabicyclo<2.2.2>octanium iodide With fluorenone radical anion sodium contact ion pair In 1,2-dichloro-benzene at 100℃; for 24h; Stage #2: triptycene In benzonitrile; 1,2-dichloro-benzene at 20℃; for 4h; | 27% |
oxotitanium(IV) phthalocyanine
haematoxylin
Conditions | Yield |
---|---|
In further solvent(s) Ti-complex was dissolved in 1-chloronaphthalene at 180°C under N2, hematoxylin was added, the soln. was stirred for 15 min; filtd., hexane was added to induce pptn., ppt. was collected and recrystd. from 1-chloronaphthalene/MeOH; | 19.1% |
oxotitanium(IV) phthalocyanine
gallium phthalocyanine hydroxide
Conditions | Yield |
---|---|
With hydrogenchloride; N,N-dimethyl-formamide In water at 100 - 120℃; for 1h; pH=>= 6; |
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