CAS No.29394-58-9,(S)-(+)-1-Iodo-2-methylbutane Suppliers,MSDS download

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(S)-(+)-1-Iodo-2-methylbutane

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1-Iodo-2-methylbutane

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Henan Allgreen Chemical Co.,Ltd

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2,1,3-Benzothiadiazole-4-carbonyl chloride, 95%

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Butane,1-iodo-2-methyl-, (2S)-

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Antimex Chemical Limied

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(S)-(+)-1-Iodo-2-methylbutane, stabilized with copper, 97%

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Hangzhou Fandachem Co.,Ltd

(S)-(+)-1-IODO-2-METHYLBUTANECASAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

(S)-(+)-1-IODO-2-METHYLBUTANECAS

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(S)-(+)-1-Iodo-2-methylbutane CAS NO.29394-58-9

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Yinghao Pharm Co.,Ltd.

Yinghao Pharm products include: leader molecule, heterocyclic compounds,chiral compounds, photoelectric materials, biochemical reagents etc. For example:benzene, pyrimidine, boricacid,pyridine, pyrazole, imidazole, pyrrole, fluorine and other derivat

(S)-(+)-1-Iodo-2-methylbutane

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Finetech Industry Limited

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(S)-(+)-1-Iodo-2-methylbutane

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Sigma-Aldrich Chemie GmbH

Package:5 g in ampule Application:(S)-(+)-1-Iodo-2-methylbutane may be used in the synthesis of 4 -trimethylenebis(1-methyl-1-(2-methylbutyl)piperidinium) cation (TMBP2+), to be used as a structure-directing agent (SDA) during the...

(S)-(+)-1-Iodo-2-methylbutane

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NovaChemistry

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(S)-(+)-1-Iodo-2-methylbutane

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FAR Chemical's

1-iodo-2-methylbutane

Butane,1-iodo-2-methyl-, (2S)-

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Far Research Inc.

(S)-(+)-1-Iodo-4-methylbutane

Butane,1-iodo-2-methyl-, (2S)-

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Butane,1-iodo-2-methyl-, (2S)-

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Synthetic route

: 534-00-9
(S)-2-methylbutyl bromide

: 29394-58-9
(S)-1-iodo-2-methyl-butane

Conditions

Conditions	Yield
With sodium iodide In acetone 1) 1 h, 25 deg C, 2) 3 h, reflux;	91%

: 38261-81-3
(S)-2-methylbutyl tosylate

: 29394-58-9
(S)-1-iodo-2-methyl-butane

Conditions

Conditions	Yield
With sodium iodide In N,N-dimethyl-formamide at 60℃; for 1h;	89%
With sodium iodide In acetone for 6h; Heating;	75%
With iodine; magnesium In diethyl ether at 20℃; for 13h;	71%

: 1565-80-6
(2S)-2-methyl-1-butanol

: 29394-58-9
(S)-1-iodo-2-methyl-butane

Conditions

Conditions	Yield
With 1H-imidazole; iodine; triphenylphosphine In dichloromethane at 20℃; for 2h; Inert atmosphere;	83%
With 1H-imidazole; iodine; triphenylphosphine In dichloromethane at 20℃; for 5h;	79%
With triphenyl phosphite; iodine In dichloromethane	77%

: tris-((R)-2-methyl-butyl)-borane

: 29394-58-9
(S)-1-iodo-2-methyl-butane

Conditions

Conditions	Yield
With sodium hydroxide; iodine In tetrahydrofuran; water

: 1565-80-6
(2S)-2-methyl-1-butanol

benzoic acid ester of (-)(S)-2-methyl-butanol-(1): benzoic acid ester of (-)(S)-2-methyl-butanol-(1)

: 29394-58-9
(S)-1-iodo-2-methyl-butane

Conditions

Conditions	Yield
With diethyl ether; magnesium iodide

: 130797-59-0
(S)-2-Methylbutyl tetrahydropyranyl ether

: 29394-58-9
(S)-1-iodo-2-methyl-butane

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: p-TsOH*H2O / methanol / 4 h / Heating 2: pyridine / 12 h / 0 - 5 °C 3: 75 percent / NaI / acetone / 6 h / Heating View Scheme
Multi-step reaction with 3 steps 1: 96 percent / pyridinium p-toluenesulfonate / ethanol / 12 h / Ambient temperature 2: 98 percent / pyridine / 12 h / 0 - 5 °C 3: 66 percent / sodium iodide / acetone / 12 h / Heating View Scheme

: 104418-40-8
(S)-2-methyl-1-butyl methanesulfonate

: 29394-58-9
(S)-1-iodo-2-methyl-butane

Conditions

Conditions	Yield
With sodium iodide In acetone Finkelstein reaction; Reflux;

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 68314-54-5
1-bromo-2-(methoxymethoxy)benzene

: 1361331-82-9
(S)-1-(methoxymethoxy)-2-(2-methylbutyl)benzene

Conditions

Conditions	Yield
Stage #1: 1-bromo-2-(methoxymethoxy)benzene With magnesium In tetrahydrofuran Kumada coupling reaction; Inert atmosphere; Reflux; Stage #2: (S)-1-iodo-2-methyl-butane With iron(III)-acetylacetonate; N,N,N,N,-tetramethylethylenediamine; hexamethylenetetramine In tetrahydrofuran at 0℃; for 1.5h; Kumada coupling reaction;	98%
Stage #1: (S)-1-iodo-2-methyl-butane With magnesium In tetrahydrofuran for 1h; Inert atmosphere; Heating; Stage #2: 1-bromo-2-(methoxymethoxy)benzene With N,N,N,N,N,N-hexamethylphosphoric triamide; iron(III)-acetylacetonate; N,N,N,N,-tetramethylethylenediamine In tetrahydrofuran at 0℃; for 1.5h; Kumada coupling reaction; Inert atmosphere;	98%

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 185745-69-1
((S)-9-Methyl-tridecane-1-sulfonyl)-benzene

: 185745-73-7
((3S,13S)-3,13-Dimethyl-heptadecane-5-sulfonyl)-benzene

Conditions

Conditions	Yield
With n-butyllithium In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane 1.) -78 deg C to -30 deg C, 2.) -78 deg C to r.t., 5 h;	95%

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 69856-85-5, 69856-87-7
N-((R)-2-Hydroxy-1-methyl-2-phenyl-ethyl)-N-methyl-propionamide

: 192060-48-3
(2S,4S)-N-[(1'R,2'R)-2'-hydroxy-1'-methyl-2'-phenylethyl]-N-methyl-2,4-dimethylhexanamide

Conditions

Conditions	Yield
With n-butyllithium; diisopropylamine; lithium chloride In tetrahydrofuran at 23℃; for 18h;	94%

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 159213-03-3
N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylpropionamide

: 192060-47-2
(2R,4S)-N-((1S,2S)-1-hydroxy-1-phenylpropan-2-yl)-N,2,4-trimethylhexanamide

Conditions

Conditions	Yield
With n-butyllithium; diisopropylamine; lithium chloride In tetrahydrofuran at 23℃; for 20h;	94%
Stage #1: N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylpropionamide With n-butyllithium; lithium chloride; lithium diisopropyl amide In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere; Stage #2: (S)-1-iodo-2-methyl-butane In tetrahydrofuran; hexane at 0 - 20℃; for 18h; Inert atmosphere;	74%

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 2385-77-5
(R)-Citronellal

: (3S,5RS,7R)-(+)-3,7,11-trimethyldodec-10-en-5-ol

Conditions

Conditions	Yield
Stage #1: (S)-1-iodo-2-methyl-butane With tert.-butyl lithium In diethyl ether; pentane at -78 - 20℃; for 0.333333h; Inert atmosphere; Stage #2: (R)-Citronellal In diethyl ether; pentane at -78℃; for 1.5h; Inert atmosphere; Stage #3: With hydrogenchloride; ammonium chloride In diethyl ether; water; pentane Cooling with ice;	86%

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 5949-05-3
(S)-Citronellal

: 1262552-53-3
(3S,5RS,7S)-3,7,11-trimethyl-10-dodecen-5-ol

Conditions

Conditions	Yield
Stage #1: (S)-1-iodo-2-methyl-butane With tert.-butyl lithium In diethyl ether; pentane at -78 - 20℃; for 0.333333h; Inert atmosphere; Stage #2: (S)-Citronellal In diethyl ether; pentane at -78℃; for 1.5h; Inert atmosphere; Stage #3: With hydrogenchloride; ammonium chloride In diethyl ether; water; pentane Cooling with ice;	84%

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 603-35-0
triphenylphosphine

: 93119-12-1
(S)-(2-methyl-butyl)triphenylphosphonium iodide

Conditions

Conditions	Yield
In toluene at 105℃; for 63h; Inert atmosphere;	82%

: 6007-26-7
2-methyl-1,3-dithian

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 136024-50-5
(S)-(+)-2-(2-methylbutyl)-2-methyl-1,3-dithiane

Conditions

Conditions	Yield
With n-butyllithium 1.) hexane, THF, -70 degC to 0 degC, 3 h, 2a.) THF, -78 degC, 1 h, 2b.) room temp., 12 h;	81%

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: Lithium 2-lithiopropionate

: 42329-90-8, 42330-37-0, 70621-82-8, 130248-45-2
(2RS,4S)-(+)-2,4-Dimethylhexansaeure

Conditions

Conditions	Yield
With N,N,N,N,N,N-hexamethylphosphoric triamide In tetrahydrofuran at -15℃; for 2h;	80%

: 103-82-2
phenylacetic acid

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 1314887-10-9
(2R,4S)-4-methyl-2-phenylhexanoic acid

Conditions

Conditions	Yield
Stage #1: phenylacetic acid With n-butyllithium; C29H44N4 In tetrahydrofuran; hexanes at 0℃; Inert atmosphere; Stage #2: (S)-1-iodo-2-methyl-butane In tetrahydrofuran; hexanes at -78℃; for 10h; Inert atmosphere; optical yield given as %de; diastereoselective reaction;	79%

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 192060-67-6
(1R,2R)-(-)-pseudoephedrinepropionamide

: 192060-48-3
(2S,4S)-N-[(1'R,2'R)-2'-hydroxy-1'-methyl-2'-phenylethyl]-N-methyl-2,4-dimethylhexanamide

Conditions

Conditions	Yield
Stage #1: (1R,2R)-(-)-pseudoephedrinepropionamide With n-butyllithium; lithium chloride; lithium diisopropyl amide In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere; Stage #2: (S)-1-iodo-2-methyl-butane In tetrahydrofuran; hexane at 0 - 20℃; for 18h; Inert atmosphere;	79%
Stage #1: (1R,2R)-(-)-pseudoephedrinepropionamide With n-butyllithium; diisopropylamine; lithium chloride In tetrahydrofuran; hexane at -78 - 25℃; for 1.33333h; Stage #2: (S)-1-iodo-2-methyl-butane In tetrahydrofuran; hexane at 0 - 25℃; for 24h;

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 105-53-3
diethyl malonate

: 6210-82-8
diethyl S-(+)-2-methyl-1-butyl malonate

Conditions

Conditions	Yield
With ethanol; sodium In ethanol at 0 - 20℃;	76.5%

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 185745-70-4
((R)-9-Methyl-tridecane-1-sulfonyl)-benzene

: 185745-71-5
((3S,13R)-3,13-Dimethyl-heptadecane-5-sulfonyl)-benzene

Conditions

Conditions	Yield
With n-butyllithium In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane 1.) -78 deg C to -30 deg C, 2.) -78 deg C to r.t., 5 h;	72%

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 128143-88-4
2,2':6',2''-Terpyridin-4'(1'H)-one

: 1171117-90-0
C20H21N3O

Conditions

Conditions	Yield
With potassium carbonate In N,N-dimethyl-formamide at 100℃; for 12h; Inert atmosphere;	71%

: 580-18-7
3-hydroxyquinoline

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 1607440-41-4
(5)-3-(2-methylbutyloxy)quinoline

Conditions

Conditions	Yield
With potassium carbonate In dimethyl sulfoxide at 80℃; for 4h;	68%

: 103-82-2
phenylacetic acid

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 1314887-07-4
(2S,4S)-4-methyl-2-phenylhexanoic acid

Conditions

Conditions	Yield
Stage #1: phenylacetic acid With n-butyllithium; N1,N3-bis((R)-1-phenyl-2-(piperidin-1-yl)ethyl)propane-1,3-diamine In tetrahydrofuran; hexanes at 0℃; Inert atmosphere; Stage #2: (S)-1-iodo-2-methyl-butane In tetrahydrofuran; hexanes at -78℃; for 10h; Inert atmosphere; optical yield given as %de; diastereoselective reaction;	67%

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 177841-46-2
(5,10,15,20-tetraphenyl-2-aza-21-carbaporphyrinato)nickel(II)

: (5,10,15,20-tetraphenyl-21-(S-2'-methylbutyl)-2-aza-21-carbaporphyrinato)nickel(II)

Conditions

Conditions	Yield
With potassium carbonate In ethanol; dichloromethane under N2; mixt. of Ni complex and S-2-(methyliodo)butane (7 equiv.) in CH2Cl2-EtOH contg. suspn. of K2CO3 refluxed for 3 h; solvent evapd. under reduced pressure; dissolved in CH2Cl2; chromd. (silica gel, CH2Cl2); second brown-reddish band collected; crystd. from CH2Cl2-hexane; mixt. of two diastereomers (1:1) obtained;	66%

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 1419569-71-3
diethyl 5,5′,6,6′,9,9′,10,10′-octamethoxy-2H,2′H-[1,1′-bidibenzo[e,g]isoindole]-3,3′-dicarboxylate

: 1419569-83-7
diethyl 5,5′,6,6′,9,9′,10,10′-octamethoxy-2,2′-bis((S)-2-methylbutyl)-2H,2′H-[1,1′-bidibenzo[e,g]isoindole]-3,3′-dicarboxylate

Conditions

Conditions	Yield
Stage #1: diethyl 5,5′,6,6′,9,9′,10,10′-octamethoxy-2H,2′H-[1,1′-bidibenzo[e,g]isoindole]-3,3′-dicarboxylate With 18-crown-6 ether; potassium carbonate In tetrahydrofuran for 0.5h; Inert atmosphere; Stage #2: (S)-1-iodo-2-methyl-butane In tetrahydrofuran at 90℃; for 48h; Inert atmosphere;	64%

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 947383-55-3
(-)-(S)-2-methyl-1-nitrobutane

Conditions

Conditions	Yield
With silver(I) nitrite In diethyl ether 1.) 0 deg C, 24 h; 2.) RT, 48 h;	62%

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 142235-67-4
(S)-1,3-benzodithiole-1-oxide

: 142181-72-4, 142235-74-3
2-<(S)-2'-methylbutyl>-2-<(S)-2"-methylbutyl>-1,3-benzodithiole 1-oxide

Conditions

Conditions	Yield
With potassium hexamethylsilazane In tetrahydrofuran; toluene for 72h; Ambient temperature;	54%

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 153782-37-7
benzo-1,3-dithiolane-1-oxide

A: 142181-72-4, 142235-74-3
2-<(S)-2'-methylbutyl>-2-<(S)-2"-methylbutyl>-1,3-benzodithiole 1-oxide

B: 142181-72-4, 142235-74-3
2-<(S)-2'-methylbutyl>-2-<(S)-2"-methylbutyl>-1,3-benzodithiole 1-oxide

Conditions

Conditions	Yield
With potassium hexamethylsilazane In tetrahydrofuran; toluene Ambient temperature;	A 47% B 40%

...Expand

: 1202-34-2
di(pyridin-2-yl)amine

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 790666-71-6
N-(S)-2-methylbutyldipyridylamine

Conditions

Conditions	Yield
Stage #1: di(pyridin-2-yl)amine With sodium hydride In dimethyl sulfoxide at 60℃; for 12h; Stage #2: (S)-1-iodo-2-methyl-butane In dimethyl sulfoxide at 60℃; for 24h;	34%

: 13869-38-0, 21264-32-4, 13869-42-6
bis(acetonitrile)dichloroplatinum(II)

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: diiodo-tetra-tert-butylhexaphosphapentaprismane

: di-(S)-2-methylbutyl-hexaphosphapentaprismane-platin(II)-dichloride

Conditions

Conditions	Yield
Stage #1: (S)-1-iodo-2-methyl-butane With potassium; magnesium chloride In tetrahydrofuran for 3h; Stage #2: diiodo-tetra-tert-butylhexaphosphapentaprismane In tetrahydrofuran at -80℃; Stage #3: bis(acetonitrile)dichloroplatinum(II) In tetrahydrofuran for 28h; diastereoselective reaction;	31%

...Expand

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 153782-37-7
benzo-1,3-dithiolane-1-oxide

A: 142181-71-3
2-(2'-methylbutyl)-1,3-benzodithiole 1-oxide

B: 142235-73-2
2-(2'-methylbutyl)-1,3-benzodithiole 1-oxide

C: 142235-72-1
2-(2'-methylbutyl)-1,3-benzodithiole 1-oxide

D: 142235-71-0
2-(2'-methylbutyl)-1,3-benzodithiole 1-oxide

Conditions

Conditions	Yield
With potassium hexamethylsilazane In tetrahydrofuran; toluene for 72h; Ambient temperature;	A 30% B 8% C 8% D 24%

...Expand

: 3,6-dithiophen-2-yl-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: 1386439-79-7
2,5-dimethylbutyl-3,6-dithiophen-2-ylpyrrolo[3,4-c]pyrrole-1,4-dione

Conditions

Conditions	Yield
Stage #1: 3,6-dithiophen-2-yl-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione With potassium carbonate In N,N-dimethyl-formamide at 120℃; Inert atmosphere; Stage #2: (S)-1-iodo-2-methyl-butane In N,N-dimethyl-formamide at 125℃; for 15h;	30%

: 6825-20-3
3,6-dibromo-9H-carbazole

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: (S)-3,6-dibromo-9-(2-methylbutyl)-9H-carbazole

Conditions

Conditions	Yield
With potassium carbonate In N,N-dimethyl-formamide at 100℃; for 24h;	26%

: 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)

: 29394-58-9
(S)-1-iodo-2-methyl-butane

: diiodo-tetra-tert-butylhexaphosphapentaprismane

: di-(S)-2-methylbutyl-hexaphosphapentaprismane-palladium(II)-dichloride

Conditions

Conditions	Yield
Stage #1: (S)-1-iodo-2-methyl-butane With potassium; magnesium chloride In tetrahydrofuran for 3h; Stage #2: diiodo-tetra-tert-butylhexaphosphapentaprismane In tetrahydrofuran at -80℃; Stage #3: dichloro(1,5-cyclooctadiene)palladium(II) In tetrahydrofuran for 20.5h; diastereoselective reaction;	23%

...Expand

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