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Cas:30438-74-5
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inquiryOur company engages in Sodium Tripolyphosphate (STPP) and Sodium Hexametabphosphate (SHMP) production; development of noble metal catalysts, synthesis of electronic chemical materials and general chemicals Imp&Exp trading business. The company
Cas:30438-74-5
Min.Order:1 Kilogram
FOB Price: $1000.0
Type:Lab/Research institutions
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:30438-74-5
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inquirybulk productiongoods in stockswe have the best competitive price in the marketmeantime,we are committed to service to our every customer Chemsigma International Co.,Ltd. is a chemical manufacturer, specialize in custom synthesis and organic chemical
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inquiryfactory?direct?sale Application:Fine chemical intermediates, used as the main raw material for the synthesis of various pesticides, medicines, surfactants, polymer monomers, and antifungal agents
Cas:30438-74-5
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inquiryMethanamine,1-chloro-N,N-dimethyl- (9CI) cas 30438-74-5Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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Cas:30438-74-5
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inquiry1 good quality, better price and bettter service;2 Timely delivery;3 100% refunded if parcel is t delivered or poor quality.We will try to satisfy you upon receipt of your reply. I hope that we can become a long-term cooperative partner. Application:
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inquiryMethanamine,1-chloro-N,N-dimethyl- (9CI) Application:intermediates
Cas:30438-74-5
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inquiryN-<(trimethylsiloxy)methyl>dimethylamine
A
Hexamethyldisiloxane
B
N-(chloromethyl)dimethylamine
Conditions | Yield |
---|---|
With chloro-trimethyl-silane In diethyl ether at 20 - 40℃; | A 97% B 95% |
bis-(dimethylamino)methane
N-(chloromethyl)dimethylamine
Conditions | Yield |
---|---|
With acetyl chloride In diethyl ether for 2h; Ambient temperature; | 95% |
With hydrogenchloride; N,N-dimethyl-formamide | |
With tetrachloromethane; chlorine | |
With benzoyl chloride In diethyl ether | |
With chloromethyl methyl ether In acetonitrile |
chloro-trimethyl-silane
C10H28N2O3Si2
A
decamethyltetrasiloxane
B
N-(chloromethyl)dimethylamine
Conditions | Yield |
---|---|
In benzene at 40℃; for 20h; Inert atmosphere; Schlenk technique; | A 86% B n/a |
C10H28N2O3Si2
chlorotrimethylgermane
A
C10H30Ge2O3Si2
B
N-(chloromethyl)dimethylamine
Conditions | Yield |
---|---|
In benzene at 40℃; for 15h; Inert atmosphere; Schlenk technique; | A 57% B n/a |
Triphenylsilyl chloride
C10H28N2O3Si2
A
3,3,5,5-tetramethyl-1,1,1,7,7,7-hexaphenyl-tetrasiloxane
B
N-(chloromethyl)dimethylamine
Conditions | Yield |
---|---|
In benzene at 40℃; for 20h; Inert atmosphere; Schlenk technique; | A 45% B n/a |
C10H28N2O3Si2
chlorotriphenylgermane
A
C40H42Ge2O3Si2
B
N-(chloromethyl)dimethylamine
Conditions | Yield |
---|---|
In benzene at 40℃; for 20h; Inert atmosphere; Schlenk technique; | A 33% B n/a |
N-(chloromethyl)dimethylamine
Methacrylamide
Conditions | Yield |
---|---|
In dichloromethane at 20 - 25℃; Product distribution; Further Variations:; Solvents; Alkylation; | 98% |
Conditions | Yield |
---|---|
In acetic acid | 96% |
2-isobutyl-3-(diethoxyphosphorylmethyl)furan
N-(chloromethyl)dimethylamine
Conditions | Yield |
---|---|
In acetonitrile at 80℃; for 6h; | 95% |
N-(chloromethyl)dimethylamine
hexaphenylcarbodiphosphorane
Conditions | Yield |
---|---|
In benzene for 2h; | 90% |
julolidine
N-(chloromethyl)dimethylamine
Conditions | Yield |
---|---|
With acetyl chloride In acetonitrile; benzene for 1h; Substitution; | 90% |
N-(chloromethyl)dimethylamine
O,O-bis(trimethylsilyl)-2,4-diphenylbutylphosphonite
trimethylsilyl (dimethylaminomethyl)(2,4-diphenylbutyl)phosphinate
Conditions | Yield |
---|---|
In dichloromethane Substitution; Heating; | 89% |
In dichloromethane Arbuzuv reaction; Heating; | 89% |
N-(chloromethyl)dimethylamine
[2,3-bis (methoxycarbonyl)propyl]phosphonous acid bis(trimethylsilyl) ester
Conditions | Yield |
---|---|
In dichloromethane for 0.25h; Heating; | 89% |
In dichloromethane Heating; | 89% |
1,3-dithiacyclohexan-5-one
N-(chloromethyl)dimethylamine
4-Dimethylaminomethyl-1,3-dithian-5-one Hydrogen Chloride
Conditions | Yield |
---|---|
In acetonitrile for 20h; Ambient temperature; | 86% |
[2-phenylethyl]phosphonous acid bis(trimethylsilyl) ester
N-(chloromethyl)dimethylamine
Conditions | Yield |
---|---|
In dichloromethane Heating; | 86% |
In dichloromethane Arbuzuv reaction; Heating; | 86% |
N-(chloromethyl)dimethylamine
O,O-bis(trimethylsilyl) (N-methanesulfonyl)-N-methylaminomethylphosphonite
Conditions | Yield |
---|---|
In dichloromethane Heating; | 86% |
In dichloromethane at 5℃; | 86% |
In dichloromethane at 5℃; Inert atmosphere; | 86% |
In dichloromethane at 5℃; Arbuzov Reaction; Inert atmosphere; Reflux; | 86% |
bis(trimethylsilyl)phosphonite
N-(chloromethyl)dimethylamine
Trimethylsilyl Bis<(dimethylamino)methyl>phosphinate
Conditions | Yield |
---|---|
With triethylamine In diethyl ether; dichloromethane for 1h; Ambient temperature; | 85% |
With triethylamine In dichloromethane at 20℃; for 1h; | 7.7 g |
With triethylamine In diethyl ether; dichloromethane at 20℃; for 1h; Inert atmosphere; | 7.7 g |
tetraisopropyl methylenebis
N-(chloromethyl)dimethylamine
diisopropyl methylenebis<<(dimethylamino)methyl>phosphinate>
Conditions | Yield |
---|---|
In dichloromethane 0 deg C to RT; | 85% |
2-isobutyl-4-(diethoxyphosphorylmethyl)furan
N-(chloromethyl)dimethylamine
Conditions | Yield |
---|---|
In acetonitrile at 80℃; for 6h; | 83% |
N-(chloromethyl)dimethylamine
bis(trimethylsilyl) (N-methyl-N-formylaminomethyl)phosphonite
Conditions | Yield |
---|---|
In dichloromethane | 82% |
N-(chloromethyl)dimethylamine
bis(trimethylsilyl) [2-(triethylsilyl)ethyl]phosphonite
Conditions | Yield |
---|---|
In dichloromethane Substitution; Heating; | 81% |
N-(chloromethyl)dimethylamine
bis(trimethylsilyl) 2,3-bis(trimethylsiloxycarbonyl)propylphosphonite
Conditions | Yield |
---|---|
In dichloromethane Heating; | 81% |
Ethyl diphenylphosphinite
N-(chloromethyl)dimethylamine
<(dimethylamino)methyl>diphenylphosphine oxide
Conditions | Yield |
---|---|
In toluene for 1h; Heating; | 78% |
1,4,6,9-tetraoxa-5λ5-phosphaspiro[4,4]nonane
N-(chloromethyl)dimethylamine
5-<(dimethylamino)methyl>-1,4,6,9-tetraoxa-5λ5-phosphaspiro<4.4>nonane
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; | 75% |
With triethylamine In dichloromethane | |
With triethylamine In dichloromethane at 20℃; Inert atmosphere; | 14.4 g |
N-(chloromethyl)dimethylamine
bis(trimethylsilyl) [(2-diethylaminosulfonyl)ethyl]phosphonite
Conditions | Yield |
---|---|
In dichloromethane Heating; | 73% |
In dichloromethane at 10℃; | 73% |
In dichloromethane at 10℃; | 73% |
N-(chloromethyl)dimethylamine
bis(trimethylsilyl) 2-[N-(2-oxopyrrolidino)]ethylphosphonite
trimethylsilyl (dimethylaminomethyl){2-[N-(2-oxopyrrolidino)]ethyl}phosphinate
Conditions | Yield |
---|---|
In dichloromethane Heating; | 71% |
In dichloromethane Arbuzuv reaction; Heating; | 71% |
norbornane-2,5-dione
N-(chloromethyl)dimethylamine
3-endo-6-endo-bis(dimethylaminomethyl)bicyclo<2.2.1.>heptane-2,5-dione
Conditions | Yield |
---|---|
In acetonitrile 1.) reflux, 10 min, 2.) RT, 2 d; | 70% |
N-(chloromethyl)dimethylamine
bis(trimethylsilyl) dimethylcarbamoylphosphonite
Conditions | Yield |
---|---|
In diethyl ether Heating; | 69% |
In dichloromethane Reflux; | 69% |
N-(chloromethyl)dimethylamine
lithium diphenylphosphide
[(N,N-dimethylamino)methyl]diphenylphosphine
Conditions | Yield |
---|---|
In tetrahydrofuran | 66% |
In tetrahydrofuran |
tetraisopropyl methylenebis
N-(chloromethyl)dimethylamine
isopropyl <(diisopropoxyphosphino)methyl><(dimethylamino)methyl>phosphinate
Conditions | Yield |
---|---|
In dichloromethane 0 deg C to RT; | 66% |
dimethylsulfite
N-(chloromethyl)dimethylamine
A
methylene chloride
B
dimethylaminomethylsulfonic acid
C
N-methoxymethyl-N,N-dimethylamine
Conditions | Yield |
---|---|
at 80℃; for 5h; Product distribution; other temperatures, time; reaction of dimethyl sulfite with dimethylammonium derivatives Me2NCH2X (X = Cl, CF3CO2, CCl3CO2, MeCO2); | A n/a B n/a C n/a D 64% |
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