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Cas:3144-74-9
Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Min.Order:5 Kiloliter
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Type:Manufacturers
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Min.Order:1 Kilogram
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Type:Trading Company
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Cas:3144-74-9
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Chloromethyl(dimethyl)silaneAppearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:Used in Synthesis, Pharmaceuticals and other fields Transportation:Sea/air/courier
Cas:3144-74-9
Min.Order:0
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Type:Lab/Research institutions
inquiryChloromethyl(dimethyl)silane cas 3144-74-9Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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Min.Order:0
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Type:Lab/Research institutions
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Type:Trading Company
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Cas:3144-74-9
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryWith certain technical reserves, high quality, preferential price and excellent service Application:high-purity organosilicone products have been developed, covering almost all fields of new material
Cas:3144-74-9
Min.Order:0
Negotiable
Type:Lab/Research institutions
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CFTC?PharmaChem?is?a?service?based?company?in?China,?a?pharmachem?division?of?Changzhou?Foreign?Trade?Corp.,supplying?raw?materials,?intermediates,?APIs?and?fine?chemicals?for?the?pharmaceutical?and?specialty?chemical?industries?worldwide. Applicatio
High purity Application:Pharmaceutical intermediates, Material synthesis and analyzing the expectant ingredients
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In dibutyl ether under 0.8 - 3.8 Torr; | 92% |
Stage #1: Chloro(chloromethyl)dimethylsilane With lithium aluminium tetrahydride; diethylene glycol dibutyl ether at 2 - 45℃; Inert atmosphere; Stage #2: With hydrogenchloride In water at 2 - 10℃; pH=< 2; | 86% |
With lithium aluminium tetrahydride In diethyl ether at 0℃; | 78% |
Conditions | Yield |
---|---|
With platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex In toluene at 40℃; for 16h; Inert atmosphere; Schlenk technique; | 99% |
chloromethyldimethylsilane
1,3,5-Tris-(1,1-diallyl-but-3-enyl)-benzene
Conditions | Yield |
---|---|
With bis(η2:η2-1,3-divinyltetramethyl)platinum(0) In diethyl ether; xylene at 20℃; for 72h; | 98% |
chloroplatinic acid 1,1,3,3-tetramethyl-1,3-divinyldisiloxane complex at 20℃; for 24h; | |
Kartsted catalyst In diethyl ether at 20℃; for 13h; |
chloromethyldimethylsilane
Conditions | Yield |
---|---|
With platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex In toluene at 25 - 40℃; for 16h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
dihydrogen hexachloroplatinate In toluene at 20℃; | 94% |
chloromethyldimethylsilane
5-benzyloxy-1-pentyne
(5-(benzyloxy)pent-1-en-2-yl)(chloromethyl)dimethylsilane
Conditions | Yield |
---|---|
With cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate In acetone at 5℃; for 2h; Inert atmosphere; Cooling; | 94% |
chloromethyldimethylsilane
4-triallylmethylphenol
4-{4-(chloromethyl-dimethyl-silanyl)-1,1-bis-[3-(chloromethyl-dimethyl-silanyl)-propyl]-butyl}-phenol
Conditions | Yield |
---|---|
In diethyl ether at 20℃; for 48h; | 91% |
chloroplatinic acid 1,1,3,3-tetramethyl-1,3-divinyldisiloxane complex In diethyl ether at 20 - 35℃; for 48h; | 85% |
chloroplatinic acid 1,1,3,3-tetramethyl-1,3-divinyldisiloxane complex In diethyl ether at 20 - 50℃; for 48h; | 85% |
With chloroplatinic acid 1,1,3,3-tetramethyl-1,3-divinyldisiloxane complex In tetrahydrofuran at 40℃; for 24h; Inert atmosphere; | |
With platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex In diethyl ether at 20℃; for 24h; |
chloromethyldimethylsilane
carbon dioxide
diethylamine
(chloromethyl)dimethylsilyl diethylcarbamate
Conditions | Yield |
---|---|
at 50℃; for 5h; N-siloxycarbonylation; | 90.8% |
Conditions | Yield |
---|---|
In hexane for 10h; amination; Heating; | 90.7% |
chloromethyldimethylsilane
Conditions | Yield |
---|---|
With platinum divinyltetramethyldisiloxane In tetrahydrofuran at 54℃; for 22h; | 90% |
chloromethyldimethylsilane
1-(1,1-diallyl-but-3-enyl)-4-methylsulfanyl-benzene
1-{4-(chloromethyl-dimethyl-silanyl)-1,1-bis-[3-(chloromethyl-dimethyl-silanyl)-propyl]-butyl}-4-methylsulfanyl-benzene
Conditions | Yield |
---|---|
In diethyl ether at 20℃; for 48h; | 90% |
chloromethyldimethylsilane
Allyl acetate
3-(chloromethyldimethylsilanyl)propyl ethanoate
Conditions | Yield |
---|---|
With dihydrogen hexachloroplatinate In tetrahydrofuran; isopropyl alcohol for 2h; Heating; | 88% |
chloromethyldimethylsilane
tetraallylsilane
1-(chloromethyl-dimethyl-silanyl)-3-{tris-[3-(chloromethyl-dimethyl-silanyl)-propyl]-silanyl}-propane
Conditions | Yield |
---|---|
With Speier's catalyst In toluene at 60℃; for 5h; Inert atmosphere; | 87% |
With dihydrogen hexachloroplatinate In tetrahydrofuran at 70℃; for 12h; | 76% |
bis(tetrabutylammonium) hexachloroplatinate(IV) In dichloromethane at 45℃; |
chloromethyldimethylsilane
allyl-trimethyl-silane
(chloromethyl)dimethyl(3-(trimethylsilyl)propyl)silane
Conditions | Yield |
---|---|
platinum In tetrahydrofuran; toluene for 72h; Heating; | 87% |
With 1,3-di(η2-vinyl)-1.1.3.3-tetramethyldisiloxane platinum(0) In tetrahydrofuran; toluene Cooling with ice; Reflux; Inert atmosphere; | 87% |
chloromethyldimethylsilane
carbon dioxide
diethyl amine hydrochloride
(chloromethyl)dimethylsilyl diethylcarbamate
Conditions | Yield |
---|---|
at 60℃; for 10h; N-siloxycarbonylation; | 86.9% |
chloromethyldimethylsilane
Conditions | Yield |
---|---|
at 110 - 120℃; Substitution; | 86% |
Conditions | Yield |
---|---|
HRh(PPh3)4 for 1.5h; Ambient temperature; | 85% |
chloromethyldimethylsilane
carbon dioxide
diethylammonium diethylcarbamate
(chloromethyl)dimethylsilyl diethylcarbamate
Conditions | Yield |
---|---|
for 5h; dehydrocondensation; Heating; | 84.6% |
chloromethyldimethylsilane
(n-butylaminomethyl)dimethylmethoxysilane
Conditions | Yield |
---|---|
at 65℃; for 3h; dehydrocondensation; | 84.6% |
chloromethyldimethylsilane
carbon dioxide
(n-butylaminomethyl)dimethylmethoxysilane
Conditions | Yield |
---|---|
at 55℃; for 5h; N-siloxycarbonylation; | 83.9% |
Conditions | Yield |
---|---|
HRh(PPh3)4 for 0.5h; Ambient temperature; | 83% |
chloromethyldimethylsilane
Conditions | Yield |
---|---|
HRh(PPh3)4 for 10h; Ambient temperature; | 83% |
chloromethyldimethylsilane
diphenylphosphane
((dimethylsilyl)methyl)diphenylphosphane
Conditions | Yield |
---|---|
Stage #1: diphenylphosphane With n-butyllithium In tetrahydrofuran; hexane at -80 - 20℃; for 3.5h; Inert atmosphere; Schlenk technique; Stage #2: chloromethyldimethylsilane In tetrahydrofuran; hexane at -40 - 20℃; Schlenk technique; Inert atmosphere; | 83% |
chloromethyldimethylsilane
Conditions | Yield |
---|---|
Stage #1: chloromethyldimethylsilane With magnesium In tetrahydrofuran for 2h; Inert atmosphere; Reflux; Stage #2: ethyl (R)-3-(benzyloxy)hexanoate With cerium(III) chloride In tetrahydrofuran at -78 - 20℃; for 17h; Inert atmosphere; | 83% |
Conditions | Yield |
---|---|
With platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex In toluene at 40℃; for 16h; Inert atmosphere; Schlenk technique; | 81% |
diazoacetic acid ethyl ester
chloromethyldimethylsilane
ethyl <(chloromethyl)dimethylsilyl>acetate
Conditions | Yield |
---|---|
Product distribution; multistep reaction; new method for synthesis of ethyl silylacetates; | 80% |
copper 1) 90 deg C, 2) 90 deg C; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
HRh(PPh3)4 for 4h; Ambient temperature; | 80% |
chloromethyldimethylsilane
4-pentenyl acetate
5-(chloromethyldimethylsilanyl)pentyl ethanoate
Conditions | Yield |
---|---|
With dihydrogen hexachloroplatinate In tetrahydrofuran; isopropyl alcohol for 2h; Heating; | 80% |
chloromethyldimethylsilane
3-[Allyl-methyl-(3-{tris-[3-(diallyl-methyl-silanyl)-propyl]-silanyl}-propyl)-silanyl]-propene
Conditions | Yield |
---|---|
With Speier's catalyst In toluene at 60℃; for 5h; Inert atmosphere; | 80% |
With dihydrogen hexachloroplatinate In tetrahydrofuran Heating; | 70% |
Conditions | Yield |
---|---|
In hexane at 40℃; for 5h; Alkylation; | 79.6% |
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