CAS No.33125-97-2,Etomidate Suppliers,MSDS download

This product is a nationally controlled contraband, and the Lookchem platform doesn't provide relevant sales information.

Synthetic route

: 64-17-5
ethanol

: 1-[(1R)-1-phenylethyl]-5-hydroxymethylimidazole

: 33125-97-2
etomidate

Conditions

Conditions	Yield
With sodium cyanide; manganese(IV) oxide; acetic acid at 80℃; for 12h;	85%

: 1445-91-6
(S)-1-phenylethanol

: 23785-21-9
1H-imidazole-5-carboxylic acid ethyl ester

: 33125-97-2
etomidate

Conditions

Conditions	Yield
With di-tert-butyl-diazodicarboxylate; triphenylphosphine In tetrahydrofuran at -40℃; Mitsunobu reaction; Inert atmosphere;	70%

: 97849-55-3
[1-11C]ethyl iodide

: 56649-48-0
(R)-(+)-1-(1-phenylethyl)-1H-imidazole-5-carboxylic acid

: 33125-97-2
etomidate

Conditions

Conditions	Yield
With tetra(n-butyl)ammonium hydroxide In N,N-dimethyl-formamide at 120℃; for 0.0833333h;

: [Ru(2,2′-bipyridine)2(etomidate)2](PF6)2

: 7732-18-5
water

A: [Ru(2,2′-bipyridine)2(etomidate)(H2O)](PF6)2

B: 33125-97-2
etomidate

Conditions

Conditions	Yield
for 0.0166667h; Kinetics; Time; UV-irradiation;

...Expand

: [Ru(2,2′-bipyridine)2(etomidate)2]Cl2

: 75-05-8
acetonitrile

A: 55124-54-4
bis(acetonitrile)bis(2,2'-bipyridine)ruthenium(II) hexafluorophosphate

B: 33125-97-2
etomidate

Conditions

Conditions	Yield
for 1h; Kinetics; Time; UV-irradiation;

...Expand

: C12H14N2OS

: 33125-97-2
etomidate

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: acetic acid; sodium nitrite / tetrahydrofuran; water / 0.5 h / Flow reactor 2: manganese(IV) oxide; sodium cyanide; acetic acid / 12 h / 80 °C View Scheme

: 33125-97-2
etomidate

: 56649-48-0
(R)-(+)-1-(1-phenylethyl)-1H-imidazole-5-carboxylic acid

Conditions

Conditions	Yield
With methanol; lithium hydroxide In tetrahydrofuran; water at 20℃;	93%
With sodium hydroxide In methanol at 20℃; for 6h;	91.5%
With methanol; sodium hydroxide at 20℃; for 6h;	90.1%

: 67-63-0
isopropyl alcohol

: 33125-97-2
etomidate

: 771422-77-6
C15H18N2O2

Conditions

Conditions	Yield
With sodium isopropylate at 20℃; for 5h;	80%

: 71-23-8
propan-1-ol

: 33125-97-2
etomidate

: 61045-93-0
C15H18N2O2

Conditions

Conditions	Yield
With sodium n-propoxide at 20℃; for 5h;	78%

: 67-56-1
methanol

: 33125-97-2
etomidate

: 61045-91-8
(R)-Metomidate

Conditions

Conditions	Yield
With sodium methylate at 20℃; for 5h;	71%

: 33125-97-2
etomidate

: 74-89-5
methylamine

A: 1016274-81-9
C13H15N3O

B: 844658-92-0
(R)-(-)-[1-phenylethyl]-1H-imidazole

Conditions

Conditions	Yield
In ethanol at 180℃; for 18h; Inert atmosphere; Sealed tube;	A 19% B 65%

...Expand

: 17084-13-8
potassium hexafluorophosphate

: trans-[Ru(2,2'-bipyridyl)2(H2O)2](CF3SO3)2

: 33125-97-2
etomidate

: [Ru(2,2′-bipyridine)2(etomidate)2](PF6)2

Conditions

Conditions	Yield
Stage #1: trans-[Ru(2,2'-bipyridyl)2(H2O)2](CF3SO3)2; etomidate In ethanol; water at 85℃; for 24h; Inert atmosphere; Stage #2: potassium hexafluorophosphate In ethanol; water	47%

...Expand

: 33125-97-2
etomidate

A: (R)-(+)-ethyl 1-[1-(4-iodophenyl)ethyl]-1H-imidazole-5-carboxylate

B: (R)-(+)-ethyl 1-[1-(3-iodophenyl)ethyl]-1H-imidazole-5-carboxylate

Conditions

Conditions	Yield
With iodine; silver trifluoroacetate; acetic acid In tetrachloromethane at 80℃; for 16h; in the dark;

: 33125-97-2
etomidate

: (+)-Azietomidate

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: aq. NaOH / 1 h / 100 °C 2: 76 percent / p-(dimethylamino)pyridine; dicyclohexylcarbodiimide / CH2Cl2 / 15 h / 20 °C View Scheme

: 33125-97-2
etomidate

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: lithium hydroxide / tetrahydrofuran; methanol / 20 °C 2: phosgene / dichloromethane / 0 - 20 °C View Scheme
Multi-step reaction with 2 steps 1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C 2: oxalyl dichloride / dichloromethane / 0 - 20 °C View Scheme
Multi-step reaction with 2 steps 1: sodium hydroxide / water 2: oxalyl dichloride / dichloromethane View Scheme
Multi-step reaction with 2 steps 1: lithium hydroxide; methanol / tetrahydrofuran; water / 20 °C 2: oxalyl dichloride / dichloromethane / 1 h / 0 - 20 °C View Scheme

: 33125-97-2
etomidate

: 1446482-53-6
C18H20N2O4

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: lithium hydroxide / tetrahydrofuran; methanol / 20 °C 2: phosgene / dichloromethane / 0 - 20 °C 3: triethylamine / dichloromethane / 48 h / 0 - 20 °C View Scheme
Multi-step reaction with 3 steps 1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C 2: oxalyl dichloride / dichloromethane / 0 - 20 °C 3: triethylamine / dichloromethane / 48 h / 0 - 20 °C View Scheme

: 33125-97-2
etomidate

: 1446482-57-0
C19H22N2O4

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: lithium hydroxide / tetrahydrofuran; methanol / 20 °C 2: phosgene / dichloromethane / 0 - 20 °C 3: dichloromethane; pyridine / 1 h / 80 °C View Scheme
Multi-step reaction with 3 steps 1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C 2: oxalyl dichloride / dichloromethane / 0 - 20 °C 3: pyridine / dichloromethane / 1 h / 80 °C View Scheme

: 33125-97-2
etomidate

: C21H26N2O3

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: lithium hydroxide / tetrahydrofuran; methanol / 20 °C 2: phosgene / dichloromethane / 0 - 20 °C 3: pyridine / dichloromethane / 1 h / 80 °C View Scheme

: 33125-97-2
etomidate

: 1446482-69-4
C18H20N2O4

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: lithium hydroxide / tetrahydrofuran; methanol / 20 °C 2: phosgene / dichloromethane / 0 - 20 °C 3: triethylamine / dichloromethane / 0 - 20 °C View Scheme
Multi-step reaction with 3 steps 1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C 2: oxalyl dichloride / dichloromethane / 0 - 20 °C 3: triethylamine / dichloromethane / 0 - 20 °C View Scheme

: 33125-97-2
etomidate

: C20H25N3O3*2ClH

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: lithium hydroxide / tetrahydrofuran; methanol / 20 °C 2.1: phosgene / dichloromethane / 0 - 20 °C 3.1: pyridine / dichloromethane / 2 h / 80 °C 3.2: 1 h / 20 °C View Scheme

: 33125-97-2
etomidate

: C21H27N3O3

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1.1: lithium hydroxide / tetrahydrofuran; methanol / 20 °C 2.1: phosgene / dichloromethane / 0 - 20 °C 3.1: pyridine / dichloromethane / 2 h / 80 °C 3.2: 1 h / 20 °C 4.1: acetonitrile / 0.5 h 4.2: 2 h View Scheme

: 33125-97-2
etomidate

: C20H24N2O4

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: lithium hydroxide / tetrahydrofuran; methanol / 20 °C 2: phosgene / dichloromethane / 0 - 20 °C 3: pyridine / dichloromethane / 1 h / 80 °C View Scheme

: 33125-97-2
etomidate

: 1446482-52-5
C20H18N2O4

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: lithium hydroxide / tetrahydrofuran; methanol / 20 °C 2: phosgene / dichloromethane / 0 - 20 °C 3: triethylamine / dichloromethane / 0 - 20 °C View Scheme
Multi-step reaction with 3 steps 1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C 2: oxalyl dichloride / dichloromethane / 0 - 20 °C 3: triethylamine / dichloromethane / 0 - 20 °C View Scheme

: 33125-97-2
etomidate

: 1198154-78-7
methoxycarbonyl etomidate

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: lithium hydroxide / tetrahydrofuran; methanol / 20 °C 2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 48 h / 20 °C View Scheme
Multi-step reaction with 2 steps 1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C 2: dicyclohexyl-carbodiimide; dmap / dichloromethane / 48 h / 20 °C View Scheme

: 33125-97-2
etomidate

: C20H24N2O4

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C 2: oxalyl dichloride / dichloromethane / 0 - 20 °C 3: pyridine / dichloromethane / 1 h / 80 °C View Scheme

: 33125-97-2
etomidate

: C24H31N3O6

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C 2: oxalyl dichloride / dichloromethane / 0 - 20 °C 3: pyridine / dichloromethane / 2 h / 80 °C View Scheme

: 33125-97-2
etomidate

: C19H23N3O4*2ClH

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C 2: oxalyl dichloride / dichloromethane / 0 - 20 °C 3: pyridine / dichloromethane / 2 h / 80 °C 4: hydrogenchloride / ethyl acetate; 1,4-dioxane / 1 h / 20 °C View Scheme

: 33125-97-2
etomidate

: C20H25N3O4

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1.1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C 2.1: oxalyl dichloride / dichloromethane / 0 - 20 °C 3.1: pyridine / dichloromethane / 2 h / 80 °C 4.1: hydrogenchloride / ethyl acetate; 1,4-dioxane / 1 h / 20 °C 5.1: acetonitrile / 0.5 h 5.2: 2 h View Scheme

: 33125-97-2
etomidate

: C20H25N3O4*2ClH

Conditions

Conditions	Yield
Multi-step reaction with 6 steps 1.1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C 2.1: oxalyl dichloride / dichloromethane / 0 - 20 °C 3.1: pyridine / dichloromethane / 2 h / 80 °C 4.1: hydrogenchloride / ethyl acetate; 1,4-dioxane / 1 h / 20 °C 5.1: acetonitrile / 0.5 h 5.2: 2 h 6.1: hydrogenchloride / ethyl acetate; 1,4-dioxane / 1 h View Scheme

: 33125-97-2
etomidate

: C19H22N2O5

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C 2: oxalyl dichloride / dichloromethane / 0 - 20 °C 3: pyridine / dichloromethane / 1 h / 80 °C View Scheme

: 33125-97-2
etomidate

: 1446482-73-0
C16H16N2O4

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C 2: oxalyl dichloride / dichloromethane / 0 - 20 °C 3: triethylamine / dichloromethane / 0 - 20 °C View Scheme

: 33125-97-2
etomidate

: 1446482-74-1
C16H15ClN2O3

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C 2: oxalyl dichloride / dichloromethane / 0 - 20 °C 3: triethylamine / dichloromethane / 0 - 20 °C 4: oxalyl dichloride / dichloromethane / 0 - 20 °C View Scheme

: 33125-97-2
etomidate

: 1446482-75-2
C19H20N2O5

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C 2: oxalyl dichloride / dichloromethane / 0 - 20 °C 3: triethylamine / dichloromethane / 0 - 20 °C 4: oxalyl dichloride / dichloromethane / 0 - 20 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme

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