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Cas:33184-16-6
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inquiryOur Services 1. Certificate Of Analysis (COA) 2. Material Safety Data Sheet (MSDS) 3. Route of synthesis (ROS) 4. Method of Aanlysis (MOA)
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inquiry5-Fluoro-2-methylbenzoic acid CAS No.:33184-16-6 Name: 5-Fluoro-2-methylbenzoic acid Synonyms: 5-Fluoro-o-toluic acid Molecular Structure: Molecular Formula: C8H7FO2 Molecular Weight:
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inquiryName 5-Fluoro-2-methylbenzoic acid Synonyms 5-Fluoro-o-toluic acid Molecular Structure Molecular Formula
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inquiryHigh quality. Factory supply. In stock. Best price.1.Quick response within 24 hours;2.Best quality in your requirement;?3.We pay more attention on delivery time, and usually ship on time;4.Under the premise of safety and effectiveness, we can produce
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiryProduct Name: 5-Fluoro-2-methylbenzoic acid Synonyms: RARECHEM AL BO 0443;2-METHYL-5-FLUOROBENZOIC ACID;5-FLUORO-2-METHYLBENZOIC ACID;5-FLUORO-O-TOLUIC ACID;5-Fluoro-2-Methyl Benzoic Acid 2-Me
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:33184-16-6
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inquiry5-Fluoro-2-methylbenzoic acid CAS:33184-16-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality org
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:33184-16-6
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inquiryWe are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to provide excellence in researching, manufacturing and drug discovery process. Our
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:33184-16-6
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:33184-16-6
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:33184-16-6
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inquiryProduct name: 5-Fluoro-2-Methylbenzoic Acid CAS No.:33184-16-6 Molecule Formula:C8H6FO2 Molecule Weight:153.13 Purity: 98.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TES
Cas:33184-16-6
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:33184-16-6
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:33184-16-6
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Cas:33184-16-6
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:33184-16-6
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:33184-16-6
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inquiryProduct Name: 5-Fluoro-2-methylbenzoic acid Synonyms: 2-METHYL-5-FLUOROBENZOIC ACID;RARECHEM AL BO 0443;5-Fluoro-2-Methyl Benzoic Acid 2-Methyl-5-Fluorobenzoic Acid;5-Fluoro-2-methylbenzoic acid 99%;5-Fluoro-2-methylbenzoicacid99%;5-FLUORO-2-ME
Cas:33184-16-6
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquirycarbon dioxide
5-fluoro-2-methylbenzoic acid
Conditions | Yield |
---|---|
Stage #1: 2-bromo-4-fluorotoluene With magnesium In diethyl ether for 2h; Grignard Reaction; Heating / reflux; Stage #2: carbon dioxide In diethyl ether Grignard Reaction; Stage #3: With hydrogenchloride In water; ethyl acetate Grignard Reaction; | 59% |
Conditions | Yield |
---|---|
Stage #1: 2-chloro-4-fluorotoluene With magnesium at 55℃; for 11h; Inert atmosphere; Stage #2: carbon dioxide With hydrogenchloride In water at 0 - 10℃; pH=1 - 2; |
Conditions | Yield |
---|---|
Stage #1: 2-bromo-4-fluorotoluene With magnesium In tetrahydrofuran at 25℃; for 4h; Inert atmosphere; Reflux; Stage #2: carbon dioxide With hydrogenchloride In water at 0 - 10℃; pH=1 - 2; |
Conditions | Yield |
---|---|
Stage #1: 4-fluoro-2-iodotoluene With magnesium In tetrahydrofuran at 25 - 50℃; for 4h; Inert atmosphere; Reflux; Stage #2: carbon dioxide With hydrogenchloride In water at 0 - 10℃; pH=1 - 2; |
5-fluoro-2-methylbenzoic acid
methyl iodide
5-fluoro-2-methylbenzoic acid methyl ester
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 16h; | 99% |
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃; for 2h; | 90% |
5-fluoro-2-methylbenzoic acid
1-bromo-2-(triisopropylsilyl)acetylene
Conditions | Yield |
---|---|
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; potassium hydrogencarbonate In tert-Amyl alcohol at 30℃; for 24h; | 96% |
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; potassium carbonate In tert-Amyl alcohol at 80℃; for 24h; Sealed tube; Schlenk technique; | 86% |
5-fluoro-2-methylbenzoic acid
3-fluoro-2-iodo-6-methylbenzoic acid
Conditions | Yield |
---|---|
With N-iodo-succinimide; palladium diacetate In N,N-dimethyl-formamide | 89.7% |
With [bis(acetoxy)iodo]benzene; iodine; palladium diacetate In N,N-dimethyl-formamide at 100℃; for 18h; Inert atmosphere; | |
With [bis(acetoxy)iodo]benzene; iodine; palladium diacetate In N,N-dimethyl-formamide at 100℃; for 16h; | 80 g |
With N-iodo-succinimide; palladium diacetate In N,N-dimethyl-formamide at 110℃; for 15h; | 25 g |
methanol
5-fluoro-2-methylbenzoic acid
5-fluoro-2-methylbenzoic acid methyl ester
Conditions | Yield |
---|---|
With sulfuric acid at 60℃; | 89% |
With sulfuric acid for 24h; Heating; | |
With thionyl chloride for 4h; Heating; |
5-fluoro-2-methylbenzoic acid
5-fluoro-2-methylbenzaldehyde
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; fac-tris(2-phenylpyridinato-N,C2')iridium(III); tris-(trimethylsilyl)silane; dimethyl dicarbonate In acetonitrile at 20℃; for 6h; Schlenk technique; Inert atmosphere; Sealed tube; Irradiation; | 85% |
oct-1-en-3-one
5-fluoro-2-methylbenzoic acid
Conditions | Yield |
---|---|
With manganese(II)carbonate; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In water; acetonitrile at 150℃; for 20h; Inert atmosphere; | 83% |
5-fluoro-2-methylbenzoic acid
methylamine
5-fluoro-N,2-dimethylbenzamide
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃; for 6.5h; Inert atmosphere; | 82% |
2-methyl-4-(2-(2R)-methyl-[1,3'(3'S)]bipyrrolidinyl-1'-yl)-phenylamine
5-fluoro-2-methylbenzoic acid
(2R,3'S)-5-fluoro-2-methyl-N-[2-methyl-4-(2-methyl[1,3']bipyrrolidinyl-1'-yl) phenyl]benzamide
Conditions | Yield |
---|---|
With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; | 82% |
2-methyl-4-(2-(2S)-methyl-[1,3'(3'R)]bipyrrolidinyl-1'-yl)-phenylamine
5-fluoro-2-methylbenzoic acid
Conditions | Yield |
---|---|
With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; | 82% |
2-methyl-4-(2-(2S)-methyl-[1,3'(3'S)]bipyrrolidinyl-1'-yl)-phenylamine
5-fluoro-2-methylbenzoic acid
(2S,3'S)-5-fluoro-2-methyl-N-[2-methyl-4-(2-methyl[1,3']bipyrrolidinyl-1'-yl) phenyl]benzamide
Conditions | Yield |
---|---|
With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; | 82% |
2-methyl-4-(2(2R)-methyl-[1,3'(3'R)]bipyrrolidinyl-1'-yl)-phenylamine
5-fluoro-2-methylbenzoic acid
(2R,3'R)-5-fluoro-2-methyl-N-[2-methyl-4-(2-methyl[1,3']bipyrrolidinyl-1'-yl) phenyl]benzamide
Conditions | Yield |
---|---|
With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; | 82% |
5-fluoro-2-methylbenzoic acid
5-phenyl-1-penten-3-one
Conditions | Yield |
---|---|
With manganese(II)carbonate; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In water; acetonitrile at 150℃; for 20h; Inert atmosphere; | 82% |
5-fluoro-2-methylbenzoic acid
triphenylantimony dichloride
Conditions | Yield |
---|---|
With sodium ethoxide In methanol under N2, Schlenk techniques; soln. of benzoic acid deriv. and EtONa in MeOH stirred for 30 min, Ph3SbCl2 added, mixt. stirred at room temp. for12 h; evapn. under vac., recrystd. from CH2Cl2/ether (1/1); elem. anal.; | 80% |
5-fluoro-2-methylbenzoic acid
tetraphenylantimony(V) bromide
Conditions | Yield |
---|---|
With sodium ethoxide In methanol under N2, Schlenk techniques; soln. of benzoic acid deriv. and EtONa in MeOH stirred for 30 min, Ph4SbBr added, mixt. stirred at room temp. for 12 h; evapn. under vac., recrystd. from CH2Cl2/petroleum ether (1/1); elem. anal.; | 80% |
Conditions | Yield |
---|---|
With sulfuric acid at 100℃; for 12h; Sealed tube; | 80% |
5-fluoro-2-methylbenzoic acid
5-fluoro-2-methylbenzoic acid methyl ester
Conditions | Yield |
---|---|
With sulfuric acid In methanol | 78% |
4-penten-3-one
5-fluoro-2-methylbenzoic acid
Conditions | Yield |
---|---|
With [RhCl2(p-cymene)]2 In water at 95℃; for 12h; Sealed tube; | 78% |
dec-1-en-3-one
5-fluoro-2-methylbenzoic acid
Conditions | Yield |
---|---|
With manganese(II)carbonate; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In water; acetonitrile at 150℃; for 20h; Inert atmosphere; | 78% |
5-fluoro-2-methylbenzoic acid
1,1'-carbonyldiimidazole
Conditions | Yield |
---|---|
Stage #1: 5-fluoro-2-methylbenzoic acid; 1,1'-carbonyldiimidazole In dichloromethane at 35℃; for 1h; Stage #2: With ammonia In dichloromethane at 35℃; for 2h; | 77.6% |
5-fluoro-2-methylbenzoic acid
5-fluoro-2-methylbenzoyl chloride
Conditions | Yield |
---|---|
With thionyl chloride for 3h; Reflux; | 77% |
With thionyl chloride | |
With thionyl chloride In toluene |
non-1-en-3-one
5-fluoro-2-methylbenzoic acid
Conditions | Yield |
---|---|
With manganese(II)carbonate; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In water; acetonitrile at 150℃; for 20h; Inert atmosphere; | 77% |
dodec-1-en-3-one
5-fluoro-2-methylbenzoic acid
Conditions | Yield |
---|---|
With manganese(II)carbonate; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In water; acetonitrile at 150℃; for 20h; Inert atmosphere; | 77% |
5-fluoro-2-methylbenzoic acid
Phenyl vinyl ketone
Conditions | Yield |
---|---|
With manganese(II)carbonate; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In water; acetonitrile at 150℃; for 20h; Inert atmosphere; | 76% |
octyl vinyl ketone
5-fluoro-2-methylbenzoic acid
Conditions | Yield |
---|---|
With manganese(II)carbonate; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In water; acetonitrile at 150℃; for 20h; Inert atmosphere; | 74% |
tetradec-1-en-3-one
5-fluoro-2-methylbenzoic acid
Conditions | Yield |
---|---|
With manganese(II)carbonate; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In water; acetonitrile at 150℃; for 20h; Inert atmosphere; | 72% |
5-fluoro-2-methylbenzoic acid
2-methyl-3-nitro-5-fluorobenzoic acid
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid In dichloromethane at 30 - 40℃; for 3h; Temperature; Reagent/catalyst; | 70.5% |
With sulfuric acid; nitric acid at -110 - -15℃; for 4.5h; | 45.1% |
With sulfuric acid; nitric acid at 0℃; for 0.5h; Nitration; |
Conditions | Yield |
---|---|
With iron(III)-acetylacetonate; copper(II) nitrate; Selectfluor at 80℃; for 8h; Schlenk technique; Inert atmosphere; | 70% |
Conditions | Yield |
---|---|
With sodium dihydrogenphosphate; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; water at 85℃; for 16h; Green chemistry; chemoselective reaction; | 70% |
5-fluoro-2-methylbenzoic acid
2-bromo-5-fluorobenzamide
Conditions | Yield |
---|---|
Stage #1: 5-fluoro-2-methylbenzoic acid With thionyl chloride at 70℃; for 20h; Stage #2: With ammonium hydroxide In water at 20℃; for 1h; | 69% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; | 68% |
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