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inquiryName: Sodium diethyl dithiophosphate Synonyms: sodium O,O-diethyl dithiophosphate CAS:3338-24-7 MF: C4H10NaO2PS2 Appearance: white powder Storage:Store in cool and dry place, away from sun light. Package: 25kgs/drum Application:Mining Collec
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inquiryProduct Name: sodium O,O-diethyl dithiophosphate Synonyms: sodium O,O-diethyl dithiophosphate;Phosphorodithioic acid, O,O-diethyl ester, sodium salt;O,O-DIETHYLPHOSPHORODITHIOATE,SODIUMSALT;Natrium-O,O-diethyldithiophosphat;ethyl sodium phosphorod
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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Specifications Classification: Chemical Auxiliary Agent CAS No.: 3338-24-7 Other Names: sodium O O-diethyl dithiophosphate MF: C4H10NaO2PS2 EINECS No.: 222-079-2 Purity: 95% Min Place of Origin: Hunan, China (Mainland) Type: Beneficia
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiryThe collectivity of Ethyl Thiocarbamate is similar with xanthates and dithiophosphates. Ethyl Thiocarbamate displays strong collective power and rapid flotation, low dosage in comparison with xanthates and dithiophosphates. Because its collectivit
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inquirysub/micron to mesh powders (near/spheres, whiskers, flake, fiber, porous) and grain/ball, thin/ thick metal / alloys pieces / parts, thin and thick (particle) film materials /target, and custom-made crystals, substrates/parts. In the industries and a
antimony(III) tris(O,O-diethylphosphorodithioate)
sodium O,O-diethyl phosphorodithioate
Conditions | Yield |
---|---|
With sodium pyrrolide In tetrahydrofuran for 2h; Ambient temperature; | 70% |
Conditions | Yield |
---|---|
Stage #1: ethanol With tetraphosphorus decasulfide In benzene at 60℃; for 1h; Stage #2: With sodium hydroxide |
Conditions | Yield |
---|---|
With sodium hydroxide In water at 26 - 32℃; for 5.33333h; pH=9; | |
With sodium hydroxide In water; toluene |
[RuCl(η(5)-C5H4Me)(PPh3)2]
sodium O,O-diethyl phosphorodithioate
Conditions | Yield |
---|---|
In methanol byproducts: NaCl, P(C6H5)3; refluxing under N2, 10-20 min; immediate pptn.; filtration; washing (methanol, water, methanol); drying (vac.); elem. anal.; | 100% |
chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II)
sodium O,O-diethyl phosphorodithioate
Conditions | Yield |
---|---|
In methanol byproducts: NaCl, P(C6H5)3; refluxing under N2, 10-20 min; immediate pptn.; filtration; washing (methanol, water, methanol); drying (vac.); elem. anal.; | 100% |
Conditions | Yield |
---|---|
Ambient temperature; | 98.7% |
sodium O,O-diethyl phosphorodithioate
titanium tetrachloride
ClTi(S2P(OEt)2)3
Conditions | Yield |
---|---|
In benzene byproducts: sodium chloride; TiCl4 in benzene added to suspn. NaS2P(OEt)2 in benzene (molar ratio 1:3), react. mixt. refluxed for 3 h; ppt. filtered, solvent removed under reduced pressure, product washed with n-hexane and dried; elem. anal.; | 98% |
1,3,5-trichloro-2,4,6-triazine
sodium O,O-diethyl phosphorodithioate
2,4,6-tris-diethoxythiophosphorylsulfanyl-[1,3,5]triazine
Conditions | Yield |
---|---|
In acetone for 24h; Ambient temperature; | 95% |
sodium O,O-diethyl phosphorodithioate
Conditions | Yield |
---|---|
In ethanol molar ratio Ln : P = 1 : 4, boiling and stirring (10 min); hot filtration, evapn. to dryness, extn. into hot C6H6, filtration, concn., crystn. on cooling, collection, washing (C6H6), drying (vac.); | 95% |
In diethyl ether molar ratio Ln : P = 1 : 4, boiling and stirring (10 min); hot filtration, evapn. to dryness, extn. into Et2O, filtration, concn., crystn. on cooling, collection, washing (C6H6), drying (vac.); |
sodium O,O-diethyl phosphorodithioate
Conditions | Yield |
---|---|
In ethanol molar ratio of chloride:phosphinate=1:4, boiling for 10 min, manipulations were carried out rapidly in air; filtration, drying, extraction with hot benzene, filtration, concentration, cooling, crystallization, washing with benzene, drying in vac.; | 95% |
In ethanol molar ratio of chloride:phosphinate=1:4, boiling for 10 min, manipulations were carried out rapidly in air; filtration, drying, extraction with hot benzene, filtration, concentration, cooling, crystallization, washing with benzene, drying in vac.; | 95% |
Conditions | Yield |
---|---|
In benzene for 5h; Reflux; | 95% |
sodium O,O-diethyl phosphorodithioate
bis(O,O-diethyldithiophosphato)cadmium(II)
Conditions | Yield |
---|---|
In ethanol adding of educts to ethanol, refluxing for 1 h; cooling, filtration, recrystn. (ethanol); | 93% |
sodium O,O-diethyl phosphorodithioate
titanium tetrachloride
Cl2Ti(S2P(OEt)2)2
Conditions | Yield |
---|---|
In benzene byproducts: sodium chloride; TiCl4 in benzene added to suspn. NaS2P(OEt)2 in benzene (molar ratio 1:2), react. mixt. refluxed for 3 h; ppt. filtered, solvent removed under reduced pressure, product washed with n-hexane and dried; elem. anal.; | 93% |
Conditions | Yield |
---|---|
In benzene byproducts: sodium chloride; TiCl4 in benzene added to suspn. NaS2P(OEt)2 in benzene (molar ratio 1:4 , react. mixt. refluxed for 3 h; ppt. filtered, solvent removed under reduced pressure, product washed with n-hexane and dried; elem. anal.; | 93% |
sodium O,O-diethyl phosphorodithioate
tri-n-butylchlorogermane
tributylgermanium(IV) diethyldithiophosphate
Conditions | Yield |
---|---|
In benzene Ge compd. added to suspn. of Na salt in C6H6, mixture refluxed for 2 h; filtration, concg., distn.; elem. anal.; | 93% |
sodium O,O-diethyl phosphorodithioate
1,3-dibromotetra-n-butyldistannoxane
Conditions | Yield |
---|---|
In benzene byproducts: NaBr; moisture free atmosphere; addn. of suspn. of dithiophosphate to soln. ofstannoxane, refluxing with stirring (4 h); filtration, solvent removal (vac.), washing (n-hexane); elem. anal.; | 92% |
sodium O,O-diethyl phosphorodithioate
Chloroarsenic(III)
Conditions | Yield |
---|---|
In benzene for 4h; Heating; | 91% |
Conditions | Yield |
---|---|
In benzene Heating; | 91% |
sodium O,O-diethyl phosphorodithioate
diphenylantimony(III) chloride
diphenylantimony(III) O,O-(C2H5)2-dithiophosphate
Conditions | Yield |
---|---|
In benzene byproducts: NaCl; addn. of Na-salt in benzene to Ph2SbCl, refluxing for 2 h; filtn. of NaCl, removing of the volatile fraction under vac. gives a liquid, dissoln. in petroleum ether and keeping in a deep freezer overnight, solvent removal in vac., elem. anal.; | 91% |
Conditions | Yield |
---|---|
In ethanol dissolving LaCl3*7H2O, Na(Et2dtp) and dibenzyl sulfoxide in warm ethanol; filtn., removal of the solvent in a vacuum evaporator at 80°C, dissolving the residue in warm benzene, cooling, standing in contact with petroleum ether vapour at room temp. for several days, filtn.; | 90% |
sodium O,O-diethyl phosphorodithioate
Gallium trichloride
gallium(III) diethyldithiophosphate
Conditions | Yield |
---|---|
In benzene byproducts: NaCl; Na salt was added to the soln. of Ga salt in molar ratio 3:1, the mixt.was refluxed for 2 h; NaCl was filtered, the solvent was removed in vac., elem. anal.; | 89% |
sodium O,O-diethyl phosphorodithioate
triethylchlorogermane
triethylgermanium(IV) diethyldithiophosphate
Conditions | Yield |
---|---|
In benzene Ge compd. added to suspn. of Na salt in C6H6, mixture refluxed for 2 h; filtration, concg., distn.; elem. anal.; | 89% |
sodium O,O-diethyl phosphorodithioate
phenyltin trichloride
PhSn(S2P(OEt)2)3
Conditions | Yield |
---|---|
In benzene byproducts: sodium chloride; PhSnCl3 in benzene added to suspn. (EtO)2PS2Na in benzene (molar ratio 1:3) and mixt. refluxed for 3 h; NaCl filtered off, solvent removed under reduced pressure; elem. anal.; | 88% |
Ni[(OCNHC6H4SCO)C6H4]2(NO3)2
sodium O,O-diethyl phosphorodithioate
Ni[(OCNHC6H4SCO)C6H4]2[S2P(OC2H5)2]2
Conditions | Yield |
---|---|
In tetrahydrofuran; methanol byproducts: NaNO3; mixed Ni-compd. in THF and Na-compd. in CH3OH in 1:2 molar ratio, refluxed for ca. 2 h; filtered, washed with CH3OH, dried in vac., crystallized with a THF/EtOHmixture (1:1), elem. anal.; | 88% |
Conditions | Yield |
---|---|
In acetone for 24h; | 87% |
Ni[(OCNHC6H4SCO)(CH2)3]2(NO3)2
sodium O,O-diethyl phosphorodithioate
Ni[(OCNHC6H4SCO)(CH2)3]2[S2P(OC2H5)2]2
Conditions | Yield |
---|---|
In tetrahydrofuran; methanol byproducts: NaNO3; mixed Ni-compd. in THF and Na-compd. in CH3OH in 1:2 molar ratio, refluxed for ca. 2 h; filtered, washed with CH3OH, dried in vac., crystallized with a THF/EtOHmixture (1:1), elem. anal.; | 87% |
Ni[(OCNHC6H4SCO)(CH2)4]2(NO3)2
sodium O,O-diethyl phosphorodithioate
Ni[(OCNHC6H4SCO)(CH2)4]2[S2P(OC2H5)2]2
Conditions | Yield |
---|---|
In tetrahydrofuran; methanol byproducts: NaNO3; mixed Ni-compd. in THF and Na-compd. in CH3OH in 1:2 molar ratio, refluxed for ca. 2 h; filtered, washed with CH3OH, dried in vac., crystallized with a THF/EtOHmixture (1:1), elem. anal.; | 87% |
Ni[(OCNHC6H4SCO)CH2]2(NO3)2
sodium O,O-diethyl phosphorodithioate
Ni[(OCNHC6H4SCO)CH2]2[S2P(OC2H5)2]2
Conditions | Yield |
---|---|
In tetrahydrofuran; methanol byproducts: NaNO3; mixed Ni-compd. in THF and Na-compd. in CH3OH in 1:2 molar ratio, refluxed for ca. 2 h; filtered, washed with CH3OH, dried in vac., crystallized with a THF/EtOHmixture (1:1), elem. anal.; | 86% |
sodium O,O-diethyl phosphorodithioate
Conditions | Yield |
---|---|
In benzene for 4h; Heating; | 85% |
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium
sodium O,O-diethyl phosphorodithioate
{(η-cycloocta-1,5-diene)-rhodium(I)-(S2P(OC2H5)2)}
Conditions | Yield |
---|---|
In benzene byproducts: NaCl; addition of a solution of the Rh(I) compound (0.51 mmol) in benzene to a suspension of the sodium salt (1.02 mmol) in benzene, stirring (2 - 3 hours), filtration and evaporation;; drying, recrystallization from benzene-hexane; elem. anal.;; | 85% |
Conditions | Yield |
---|---|
In water aq. soln. of ligand was added to aq. soln. of TlOCOCH3; ppt. was filtered, dried under reduced pressure, crystd. from toluene; elem. anal.; | 85% |
Conditions | Yield |
---|---|
In benzene Ge compd. added to suspn. of Na salt in C6H6, mixture refluxed for 2 h; filtration, concg., distn.; elem. anal.; | 85% |
Ni[(OCNHC6H4SCO)(CH2)2]2(CH3COO)2
sodium O,O-diethyl phosphorodithioate
Ni[(OCNHC6H4SCO)(CH2)2]2[S2P(OC2H5)2]2
Conditions | Yield |
---|---|
In tetrahydrofuran; methanol byproducts: CH3COONa; mixed Ni-compd. in THF and Na-compd. in CH3OH in 1:2 molar ratio, refluxed for ca. 2 h; filtered, washed with CH3OH, dried in vac., crystallized with a THF/EtOHmixture (1:1), elem. anal.; | 85% |
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