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inquirydi-tert-butyl dicarbonate
(S)-(+)-(adamant-1-yl)aminoacetic acid hydrochloride
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 20℃; for 19h; | 92% |
With triethylamine In methanol | 80% |
Stage #1: (S)-(+)-(adamant-1-yl)aminoacetic acid hydrochloride With sodium hydroxide In water at 0 - 5℃; for 0.25h; Stage #2: di-tert-butyl dicarbonate In tetrahydrofuran; water at 0 - 5℃; | 80 g |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 19h; Inert atmosphere; | 4.07 g |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
With sodium chlorite; potassium dihydrogenphosphate; 2-methyl-but-2-ene In tert-butyl alcohol at 0 - 10℃; for 19.5h; | 82% |
di-tert-butyl dicarbonate
(S)-(+)-β-amino-1-adamantaneacetic acid
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide for 19h; | 4.07 g |
(S)-2-(adamantan-1-yl)-2-(((R)-2-hydroxy-1-phenylethyl)amino)acetonitrile
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 78 percent / aq. HCl; AcOH / 18 h / 80 °C 2: H2; AcOH / Pd(OH)2/C / methanol / 18 h / 2585.74 Torr 3: 4.07 g / K2CO3 / dimethylformamide / 19 h View Scheme | |
Multi-step reaction with 3 steps 1: hydrogenchloride; water / acetic acid / 80 °C 2: hydrogen; palladium 10% on activated carbon / acetic acid 3: triethylamine / methanol View Scheme | |
Multi-step reaction with 3 steps 1.1: hydrogenchloride; acetic acid; water / 20 - 95 °C 2.1: acetic acid; hydrogen; 10% palladium hydroxide on charcoal / methanol / 20 °C 3.1: sodium hydroxide / water / 0.25 h / 0 - 5 °C 3.2: 0 - 5 °C View Scheme | |
Multi-step reaction with 3 steps 1: hydrogenchloride; water / acetic acid / 18 h / 80 °C 2: hydrogen; 20% palladium hydroxide-activated charcoal / methanol; acetic acid / 18 h / 2585.81 Torr 3: potassium carbonate / N,N-dimethyl-formamide / 19 h / 20 °C / Inert atmosphere View Scheme |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: H2; AcOH / Pd(OH)2/C / methanol / 18 h / 2585.74 Torr 2: 4.07 g / K2CO3 / dimethylformamide / 19 h View Scheme | |
Multi-step reaction with 2 steps 1: hydrogen; palladium 10% on activated carbon / acetic acid 2: triethylamine / methanol View Scheme | |
Multi-step reaction with 2 steps 1.1: acetic acid; hydrogen; 10% palladium hydroxide on charcoal / methanol / 20 °C 2.1: sodium hydroxide / water / 0.25 h / 0 - 5 °C 2.2: 0 - 5 °C View Scheme | |
Multi-step reaction with 2 steps 1: hydrogen; 20% palladium hydroxide-activated charcoal / methanol; acetic acid / 18 h / 2585.81 Torr 2: potassium carbonate / N,N-dimethyl-formamide / 19 h / 20 °C / Inert atmosphere View Scheme |
1-adamantanemethanol
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 98 percent / oxalyl chloride; DMSO; Et3N / CH2Cl2 / 1 h / -78 °C 2: 65 percent / NaHSO3 / H2O; methanol / 16 h / Heating 3: 78 percent / aq. HCl; AcOH / 18 h / 80 °C 4: H2; AcOH / Pd(OH)2/C / methanol / 18 h / 2585.74 Torr 5: 4.07 g / K2CO3 / dimethylformamide / 19 h View Scheme | |
Multi-step reaction with 5 steps 1.1: potassium bromide; sodium hydrogencarbonate / dichloromethane / 0.25 h / 0 - 5 °C 1.2: 0 - 5 °C 2.1: sodium hydrogensulfite / methanol; water / 0 - 55 °C 3.1: hydrogenchloride; acetic acid; water / 20 - 95 °C 4.1: acetic acid; hydrogen; 10% palladium hydroxide on charcoal / methanol / 20 °C 5.1: sodium hydroxide / water / 0.25 h / 0 - 5 °C 5.2: 0 - 5 °C View Scheme | |
Multi-step reaction with 5 steps 1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere 1.2: 0.5 h / -78 °C / Inert atmosphere 2.1: sodium hydrogensulfite / methanol; water / 18 h / 0 - 20 °C / Reflux 3.1: hydrogenchloride; water / acetic acid / 18 h / 80 °C 4.1: hydrogen; 20% palladium hydroxide-activated charcoal / methanol; acetic acid / 18 h / 2585.81 Torr 5.1: potassium carbonate / N,N-dimethyl-formamide / 19 h / 20 °C / Inert atmosphere View Scheme |
1-Adamantanecarboxylic acid
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: 100 percent / diethyl ether; hexane; methanol / 3 h / 20 °C 2: 96 percent / LiAlH4 / tetrahydrofuran / 1.5 h / 0 - 20 °C 3: 98 percent / oxalyl chloride; DMSO; Et3N / CH2Cl2 / 1 h / -78 °C 4: 65 percent / NaHSO3 / H2O; methanol / 16 h / Heating 5: 78 percent / aq. HCl; AcOH / 18 h / 80 °C 6: H2; AcOH / Pd(OH)2/C / methanol / 18 h / 2585.74 Torr 7: 4.07 g / K2CO3 / dimethylformamide / 19 h View Scheme | |
Multi-step reaction with 7 steps 1.1: thionyl chloride / 3 h / 20 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere 3.1: potassium bromide; sodium hydrogencarbonate / dichloromethane / 0.25 h / 0 - 5 °C 3.2: 0 - 5 °C 4.1: sodium hydrogensulfite / methanol; water / 0 - 55 °C 5.1: hydrogenchloride; acetic acid; water / 20 - 95 °C 6.1: acetic acid; hydrogen; 10% palladium hydroxide on charcoal / methanol / 20 °C 7.1: sodium hydroxide / water / 0.25 h / 0 - 5 °C 7.2: 0 - 5 °C View Scheme | |
Multi-step reaction with 7 steps 1.1: methanol; diethyl ether; hexane / 3 h / 20 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere 3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere 3.2: 0.5 h / -78 °C / Inert atmosphere 4.1: sodium hydrogensulfite / methanol; water / 18 h / 0 - 20 °C / Reflux 5.1: hydrogenchloride; water / acetic acid / 18 h / 80 °C 6.1: hydrogen; 20% palladium hydroxide-activated charcoal / methanol; acetic acid / 18 h / 2585.81 Torr 7.1: potassium carbonate / N,N-dimethyl-formamide / 19 h / 20 °C / Inert atmosphere View Scheme |
1-Adamantanecarbaldehyde
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 65 percent / NaHSO3 / H2O; methanol / 16 h / Heating 2: 78 percent / aq. HCl; AcOH / 18 h / 80 °C 3: H2; AcOH / Pd(OH)2/C / methanol / 18 h / 2585.74 Torr 4: 4.07 g / K2CO3 / dimethylformamide / 19 h View Scheme | |
Multi-step reaction with 4 steps 1: sodium hydrogensulfite / 0 - 60 °C 2: hydrogenchloride; water / acetic acid / 80 °C 3: hydrogen; palladium 10% on activated carbon / acetic acid 4: triethylamine / methanol View Scheme | |
Multi-step reaction with 4 steps 1.1: sodium hydrogensulfite / methanol; water / 0 - 55 °C 2.1: hydrogenchloride; acetic acid; water / 20 - 95 °C 3.1: acetic acid; hydrogen; 10% palladium hydroxide on charcoal / methanol / 20 °C 4.1: sodium hydroxide / water / 0.25 h / 0 - 5 °C 4.2: 0 - 5 °C View Scheme | |
Multi-step reaction with 4 steps 1: sodium hydrogensulfite / methanol; water / 18 h / 0 - 20 °C / Reflux 2: hydrogenchloride; water / acetic acid / 18 h / 80 °C 3: hydrogen; 20% palladium hydroxide-activated charcoal / methanol; acetic acid / 18 h / 2585.81 Torr 4: potassium carbonate / N,N-dimethyl-formamide / 19 h / 20 °C / Inert atmosphere View Scheme |
methyl adamantane-1-carboxylate
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 96 percent / LiAlH4 / tetrahydrofuran / 1.5 h / 0 - 20 °C 2: 98 percent / oxalyl chloride; DMSO; Et3N / CH2Cl2 / 1 h / -78 °C 3: 65 percent / NaHSO3 / H2O; methanol / 16 h / Heating 4: 78 percent / aq. HCl; AcOH / 18 h / 80 °C 5: H2; AcOH / Pd(OH)2/C / methanol / 18 h / 2585.74 Torr 6: 4.07 g / K2CO3 / dimethylformamide / 19 h View Scheme | |
Multi-step reaction with 6 steps 1.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere 2.1: potassium bromide; sodium hydrogencarbonate / dichloromethane / 0.25 h / 0 - 5 °C 2.2: 0 - 5 °C 3.1: sodium hydrogensulfite / methanol; water / 0 - 55 °C 4.1: hydrogenchloride; acetic acid; water / 20 - 95 °C 5.1: acetic acid; hydrogen; 10% palladium hydroxide on charcoal / methanol / 20 °C 6.1: sodium hydroxide / water / 0.25 h / 0 - 5 °C 6.2: 0 - 5 °C View Scheme | |
Multi-step reaction with 6 steps 1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere 2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere 2.2: 0.5 h / -78 °C / Inert atmosphere 3.1: sodium hydrogensulfite / methanol; water / 18 h / 0 - 20 °C / Reflux 4.1: hydrogenchloride; water / acetic acid / 18 h / 80 °C 5.1: hydrogen; 20% palladium hydroxide-activated charcoal / methanol; acetic acid / 18 h / 2585.81 Torr 6.1: potassium carbonate / N,N-dimethyl-formamide / 19 h / 20 °C / Inert atmosphere View Scheme |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 0 - 20℃; | 93% |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
[(S)-1-Adamantan-1-yl-2-((1S,3S,5S)-3-carbamoyl-2-aza-bicyclo[3.1.0]hex-2-yl)-2-oxo-ethyl]-carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With TEA; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; | 90% |
(S)-1-(((R)-1-amino-5-(benzyloxy)-1,5-dioxopentan-2-yl)amino)-1-oxopropan-2-aminium 2,2,2-trifluoroacetate
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Stage #1: (alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0℃; for 0.5h; Stage #2: (S)-1-(((R)-1-amino-5-(benzyloxy)-1,5-dioxopentan-2-yl)amino)-1-oxopropan-2-aminium 2,2,2-trifluoroacetate With triethylamine In 1,4-dioxane; dichloromethane at 0 - 20℃; for 49h; | 82% |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
A
(αS)-α-[[(1,1-dimethylethoxy)carbonyl]-amino]-3-hydroxytricyclo[3.3.1.13,7]decane-1-acetic acid
B
(S)-2-((tert-butoxycarbonyl)amino)-2-(3,5-dihydroxyadamantan-1-yl)acetic acid
Conditions | Yield |
---|---|
With potassium hydroxide; potassium permanganate at 60 - 90℃; for 1.5h; | A 51% B 17% |
With potassium hydroxide; potassium permanganate In water at 60 - 90℃; for 1.5h; | A 51% B 17% |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
(αS)-α-[[(1,1-dimethylethoxy)carbonyl]-amino]-3-hydroxytricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
With potassium permanganate; water; potassium hydroxide at 60 - 90℃; for 1.5h; | 51% |
With potassium permanganate; potassium hydroxide at 90℃; | 49% |
With potassium permanganate; tetrabutylammomium bromide; potassium hydroxide In water at 20 - 25℃; | 18.6 g |
C20-O-trityl-prostratin-ol
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 14h; | 24.8% |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane for 2.5h; |
L-Alanine methyl ester
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
(S)-2-((S)-2-Adamantan-1-yl-2-tert-butoxycarbonylamino-acetylamino)-propionic acid methyl ester
Conditions | Yield |
---|---|
With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane |
N-(cyanomethyl)ethylamine
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane |
N-propene-2 aminoacetonitrile
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane |
propylamino acetonitrile
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane |
2-amino-2-methylpropionic acid methyl ester
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
2-(2-adamantan-1-yl-2-tert-butoxycarbonylamino-acetylamino)-2-methyl-propionic acid methyl ester
Conditions | Yield |
---|---|
With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane |
benzylaminoacetonitrile
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane |
(cyclopropylamino)acetonitrile
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane |
2-aminoacetonitrile
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane |
(methylamino)acetonitrile
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: EDAC; HOAt; Et3N / CH2Cl2 2: TFA / CH2Cl2 View Scheme |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: EDAC; HOAt; Et3N / CH2Cl2 2: TFA / CH2Cl2 View Scheme |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: EDAC; HOAt; Et3N / CH2Cl2 2: aq. NaOH / methanol / 50 °C 3: NMO; i-BuOCOCl; NH3 / -15 °C 4: TFAA / CH2Cl2 5: TFA / CH2Cl2 View Scheme |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: EDAC; HOAt; Et3N / CH2Cl2 2: aq. NaOH / methanol / 50 °C 3: NMO; i-BuOCOCl; NH3 / -15 °C 4: TFAA / CH2Cl2 5: TFA / CH2Cl2 View Scheme |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: EDAC; HOAt; Et3N / CH2Cl2 2: TFA / CH2Cl2 View Scheme |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: EDAC; HOAt; Et3N / CH2Cl2 2: TFA / CH2Cl2 View Scheme |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: EDAC; HOAt; Et3N / CH2Cl2 2: TFA / CH2Cl2 View Scheme |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: EDAC; HOAt; Et3N / CH2Cl2 2: TFA / CH2Cl2 View Scheme |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: EDAC; HOAt; Et3N / CH2Cl2 2: TFA / CH2Cl2 View Scheme |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: EDAC; HOAt; Et3N / CH2Cl2 2: aq. NaOH / methanol / 50 °C 3: NMO; i-BuOCOCl; NH3 / -15 °C 4: TFAA / CH2Cl2 View Scheme |
(alpha S)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]tricyclo[3.3.1.13,7]decane-1-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: EDAC; HOAt; Et3N / CH2Cl2 2: aq. NaOH / methanol / 50 °C 3: NMO; i-BuOCOCl; NH3 / -15 °C 4: TFAA / CH2Cl2 View Scheme |
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