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benzoyl chloride
2,2-Dimethyl-1,3-propanediol
O,O'-bisbenzoyl-2,2-dimethyl-1,3-propylenediol
Conditions | Yield |
---|---|
With pyridine at 20℃; for 1h; | 84% |
With pyridine for 12h; | 81% |
With pyridine | |
With sodium hydroxide |
2,2-Dimethyl-1,3-propanediol
benzoic acid
O,O'-bisbenzoyl-2,2-dimethyl-1,3-propylenediol
Conditions | Yield |
---|---|
With xylene |
2-Ethylhexanoic acid
2,2-Dimethyl-1,3-propanediol
benzoic acid
C
benzoic acid 3-(2-ethyl-hexanoyloxy)-2,2-dimethyl-propyl ester
D
benzoic acid 3-[3-(benzoyloxy)-2,2-dimethyl-propionyloxy]-2,2-dimethyl-propyl ester
E
benzoic acid 3-{3-[3-(benzoyloxy)-2,2-dimethyl-propionyloxy]-2,2-dimethyl-propionyloxy}-2,2-dimethyl-propyl ester
F
2-ethyl-hexanoic acid 2-[3-(2-ethyl-hexanoyloxy)-2,2-dimethyl-propoxycarbonyl]-2-methyl-propyl ester
G
benzoic acid 3-{3-[3-(2-ethyl-hexanoyloxy)-2,2-dimethyl-propionyloxy]-2,2-dimethyl-propionyloxy}-2,2-dimethyl-propyl ester
H
2-ethyl-hexanoic acid 2-{2-[3-(2-ethyl-hexanoyloxy)-2,2-dimethyl-propoxycarbonyl]-2-methyl-propoxycarbonyl}-2-methyl-propyl ester
I
bis(2-ethylhexanoic acid) 2,2-dimethylpropane-1,3-diyl ester
J
O,O'-bisbenzoyl-2,2-dimethyl-1,3-propylenediol
Conditions | Yield |
---|---|
Stage #1: hydroxypivalyl hydroxypivalate; 2-Ethylhexanoic acid; 2,2-Dimethyl-1,3-propanediol; benzoic acid; titanium(IV) isopropylate at 220℃; for 8h; Stage #2: With sodium hydroxide In water Product distribution / selectivity; |
2-Ethylhexanoic acid
benzoic acid
C
benzoic acid 3-(2-ethyl-hexanoyloxy)-2,2-dimethyl-propyl ester
D
benzoic acid 3-[3-(benzoyloxy)-2,2-dimethyl-propionyloxy]-2,2-dimethyl-propyl ester
E
benzoic acid 3-{3-[3-(benzoyloxy)-2,2-dimethyl-propionyloxy]-2,2-dimethyl-propionyloxy}-2,2-dimethyl-propyl ester
F
2-ethyl-hexanoic acid 2-[3-(2-ethyl-hexanoyloxy)-2,2-dimethyl-propoxycarbonyl]-2-methyl-propyl ester
G
benzoic acid 3-{3-[3-(2-ethyl-hexanoyloxy)-2,2-dimethyl-propionyloxy]-2,2-dimethyl-propionyloxy}-2,2-dimethyl-propyl ester
H
2-ethyl-hexanoic acid 2-{2-[3-(2-ethyl-hexanoyloxy)-2,2-dimethyl-propoxycarbonyl]-2-methyl-propoxycarbonyl}-2-methyl-propyl ester
I
bis(2-ethylhexanoic acid) 2,2-dimethylpropane-1,3-diyl ester
J
O,O'-bisbenzoyl-2,2-dimethyl-1,3-propylenediol
Conditions | Yield |
---|---|
Stage #1: hydroxypivalyl hydroxypivalate; 2-Ethylhexanoic acid; benzoic acid; titanium(IV) isopropylate In xylene at 220℃; for 8h; Stage #2: With sodium hydroxide In water Product distribution / selectivity; | |
Stage #1: hydroxypivalyl hydroxypivalate; 2-Ethylhexanoic acid; benzoic acid; titanium(IV) isopropylate at 220℃; for 8h; Stage #2: With sodium hydroxide In water Product distribution / selectivity; |
benzoic acid
A
benzoic acid 3-[3-(benzoyloxy)-2,2-dimethyl-propionyloxy]-2,2-dimethyl-propyl ester
B
benzoic acid 3-{3-[3-(benzoyloxy)-2,2-dimethyl-propionyloxy]-2,2-dimethyl-propionyloxy}-2,2-dimethyl-propyl ester
C
O,O'-bisbenzoyl-2,2-dimethyl-1,3-propylenediol
Conditions | Yield |
---|---|
Stage #1: hydroxypivalyl hydroxypivalate; benzoic acid; titanium(IV) isopropylate In xylene at 220℃; for 8h; Stage #2: With sodium hydroxide In water Product distribution / selectivity; |
O,O'-bisbenzoyl-2,2-dimethyl-1,3-propylenediol
β‐cyclodextrin
β-cyclodextrin O,O'-dibenzoyl-2,2-dimethyl-1,3-propylendiol
Conditions | Yield |
---|---|
In water at 70℃; for 1h; | 47% |
In water at 70℃; for 1h; | 47% |
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