CAS No.4316-33-0,1-methoxy-4-(trimethoxymethyl)benzene Suppliers

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Ortho-p-anisic acid, trimethyl ester

Cas:4316-33-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

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Ortho-p-anisic acid, trimethyl ester

Cas:4316-33-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Antimex Chemical Limied

hight degree of purity Application:Fine chemical intermediates, used as the main raw material for he synthesis of various pesticides, medicines, surfactants, polymer monomers, Ond Ontifungal agents

Ortho-p-anisic acid, trimethyl ester

Cas:4316-33-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

: 67-56-1
methanol

: 2186-92-7
p-Anisaldehyde dimethyl acetal

A: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

B: 121-98-2
methyl 4-methoxybenzoate

Conditions

Conditions	Yield
With sodium methylate; lithium perchlorate; Tris(2,4-dibromophenyl)amine In dichloromethane indirect electrochemical oxidation;	A 78.3% B 13.2%
With sodium methylate; potassium benzenesulfonate; Tris(2,4-dibromophenyl)amine	A 53% B 18.4%

...Expand

: C10H12OS2(1+)*ClO4(1-)

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

Conditions

Conditions	Yield
With silver nitrate; triethylamine In methanol; acetonitrile for 10h; Ambient temperature;	53%

: 5874-09-9
methyl (4-methoxyphenyl)carbodithioate

: 1067-55-6
dibutyldimethoxytin

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

: 67-56-1
methanol

: 140-67-0
Estragole

A: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

B: 126501-50-6
1-(1,1-Dimethoxy-allyl)-4-methoxy-benzene

Conditions

Conditions	Yield
With sodium methylate at 30℃; for 0.5h; electrolysis;	A 3 % Chromat. B 34 % Chromat.

...Expand

: 67-56-1
methanol

: 79431-14-4
[Dimethoxy-(4-methoxy-phenyl)-methyl]-methyl-phenyl-amine

A: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

B: 100-61-8
N-methylaniline

Conditions

Conditions	Yield
With acetic acid for 0.166667h; Yield given;

...Expand

: 67-56-1
methanol

: 104-46-1
anethole

A: 2186-92-7
p-Anisaldehyde dimethyl acetal

B: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

Conditions

Conditions	Yield
With sodium 2,2,2-trifluoroacetate electrooxidation: current 0.8 A, current density 150 mA/cm2, 5F/mole;	A 76 % Chromat. B 11 % Chromat.

...Expand

: 67-56-1
methanol

: 104-46-1
anethole

A: 2186-92-7
p-Anisaldehyde dimethyl acetal

B: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

: 126501-48-2, 126501-49-3, 138169-72-9
1-(1,2-Dimethoxy-propyl)-4-methoxy-benzene

: 126501-48-2, 126501-49-3, 138169-72-9
1-(1,2-Dimethoxy-propyl)-4-methoxy-benzene

Conditions

Conditions	Yield
With sodium methylate at 30℃; for 0.75h; Product distribution; electrolysis; other time, other alkenyl phenol ethers;

...Expand

: 67-56-1
methanol

: 104-46-1
anethole

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

Conditions

Conditions	Yield
With sodium methylate at 30℃; for 0.75h; electrolysis;	11 % Chromat.

: 33672-81-0
4-methoxy-N-methyl-N-phenylbenzamide.

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 2: 1.) sodium / 1.) - 2.) CH2Cl2, 30 min 3: glacial acetic acid / 0.17 h View Scheme

: Trifluoro-methanesulfonate[1-methoxy-1-(4-methoxy-phenyl)-meth-(Z)-ylidene]-methyl-phenyl-ammonium;

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 1.) sodium / 1.) - 2.) CH2Cl2, 30 min 2: glacial acetic acid / 0.17 h View Scheme

: 67-56-1
methanol

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

Conditions

Conditions	Yield
With potassium fluoride Electrochemical reaction; Continuous flow conditions;

: 67-56-1
methanol

: 33672-81-0
4-methoxy-N-methyl-N-phenylbenzamide.

: 333-27-7
methyl trifluoromethanesulfonate

A: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

B: 100-61-8
N-methylaniline

Conditions

Conditions	Yield
Stage #1: 4-methoxy-N-methyl-N-phenylbenzamide.; methyl trifluoromethanesulfonate In dichloromethane at 20℃; Stage #2: methanol With sodium In dichloromethane for 0.166667h; Overall yield = 4.35 g; Further stages;

...Expand

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

: 16053-52-4
threothymidine

: (R)-1-[2-deoxy-3,5-O-(4-methoxy-methoxybenzylidene)-β-D-threo-pentofuranosyl]thymine

Conditions

Conditions	Yield
With pyridinium p-toluenesulfonate In N,N-dimethyl-formamide at 20℃; Inert atmosphere;	70%

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

: 50409-12-6
cis,cis-1,3,5-trihydroxycyclohexane

: 3-(4-methoxyphenyl)-2,4,10-trioxaadamantane

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at 20℃; Inert atmosphere;	58%

: 870-46-2
t-butoxycarbonylhydrazine

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

: 137256-74-7
N'-[(tert-Butoxycarbonyl-hydrazono)-(4-methoxy-phenyl)-methyl]-hydrazinecarboxylic acid tert-butyl ester

Conditions

Conditions	Yield
With toluene-4-sulfonic acid a) r.t., 16 h, b) reflux, 6 h;	54%

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

: 68430-14-8, 72121-06-3, 139628-84-5
1,3,3-trimethyl-2-oxa-bicyclo[2.2.2]octane-5,6-dione 6-hydrazone 5-oxime

: 73083-57-5
3-(4-methoxy-phenyl)-6,6,8-trimethyl-5,8-dihydro-6H-5,8-ethano-pyrano[4,3-e][1,2,4]triazine

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

: 121-98-2
methyl 4-methoxybenzoate

Conditions

Conditions	Yield
With water In acetonitrile at 30℃; Rate constant; ionic strength 0.50 M;

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

A: 67-56-1
methanol

B: 100-09-4
4-methoxybenzoic acid

Conditions

Conditions	Yield
With hydrogenchloride; potassium chloride In acetonitrile at 30℃; Rate constant; also in biphosphate buffer solution; kinetic isotope effect;

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

: 2-amino-5-(3-tert-butyl-4,4-dimethyl-4,5-dihydro-furan-2-yl)-3-methoxy-phenol

6-(3-tert-butyl-4,4-dimethyl-4,5-dihydro-furan-2-yl)-4-methoxy-2-(4-methoxy-phenyl)-benzooxazole: 6-(3-tert-butyl-4,4-dimethyl-4,5-dihydro-furan-2-yl)-4-methoxy-2-(4-methoxy-phenyl)-benzooxazole

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

: 244124-51-4
6-(3-tert-butyl-4,4-dimethyl-4,5-dihydro-furan-2-yl)-2-(4-methoxy-phenyl)-benzooxazol-4-ol

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: EtSNa / dimethylformamide View Scheme

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

: 6-(5-tert-butyl-4,4-dimethyl-2,6,7-trioxa-bicyclo[3.2.0]hept-1-yl)-2-(4-methoxy-phenyl)-benzooxazol-4-ol

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: EtSNa / dimethylformamide 2: 93.2 percent / tetraphenylporphin; O2 / CH2Cl2 / 0.67 h / 0 °C / Irradiation View Scheme

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

: 137257-07-9
4-Amino-3-(4-methoxy-phenyl)-4H-[1,2,4]triazin-5-one

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 54 percent / p-TsOH / a) r.t., 16 h, b) reflux, 6 h 2: 78 percent / conc. aq. HCl / methanol / 0.5 h / Ambient temperature 3: 49 percent / Et3N / methanol / 15 h / Ambient temperature View Scheme

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

: 137257-10-4
4-Amino-3-(4-methoxy-phenyl)-6-methyl-4H-[1,2,4]triazin-5-one

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 54 percent / p-TsOH / a) r.t., 16 h, b) reflux, 6 h 2: 78 percent / conc. aq. HCl / methanol / 0.5 h / Ambient temperature 3: 55 percent / Et3N / methanol / 2 h / Heating View Scheme

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

: 137257-13-7
4-Amino-3-(4-methoxy-phenyl)-5-oxo-4,5-dihydro-[1,2,4]triazine-6-carboxylic acid methyl ester

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 54 percent / p-TsOH / a) r.t., 16 h, b) reflux, 6 h 2: 78 percent / conc. aq. HCl / methanol / 0.5 h / Ambient temperature 3: 87 percent / Et3N / methanol / 24 h / Ambient temperature View Scheme

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

C8H12N4O*2ClH: C8H12N4O*2ClH

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 54 percent / p-TsOH / a) r.t., 16 h, b) reflux, 6 h 2: 78 percent / conc. aq. HCl / methanol / 0.5 h / Ambient temperature View Scheme

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: pyridinium p-toluenesulfonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere 2: acetonitrile / -40 - 0 °C / Inert atmosphere View Scheme

(S)-1-[2-deoxy-3,5-O-(4-methoxy-phosphonobenzylidene)-β-D-threo-pentofuranosyl]thymine disodium salt: (S)-1-[2-deoxy-3,5-O-(4-methoxy-phosphonobenzylidene)-β-D-threo-pentofuranosyl]thymine disodium salt

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: pyridinium p-toluenesulfonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere 2.1: acetonitrile / -40 - 0 °C / Inert atmosphere 3.1: trimethylsilyl bromide; 2,6-dimethylpyridine / acetonitrile / 20 °C / Inert atmosphere 3.2: Dowex resin 50 Na+ form / Inert atmosphere View Scheme

: 4316-33-0
p-Methoxybenzoic acid methyl orthoester

: 3-(p-methoxyphenyl)-2,4-dioxabicyclo[3.3.1]nonan-7-ol

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: boron trifluoride diethyl etherate / dichloromethane / 20 °C / Inert atmosphere 2: borane-THF; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / 0 °C / Inert atmosphere View Scheme

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Shandong Mopai Biotechnology Co., LTD

Antimex Chemical Limied

Synthetic route

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