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Cas:438226-89-2
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:438226-89-2
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryOur own factory produces direct sales with absolute price advantage Application:Pharmaceutical industry Transportation:By sea Port:Shanghai/tianjin
Cas:438226-89-2
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?sale Application:Fine chemical intermediates, used as the main raw material for the synthesis of various pesticides, medicines, surfactants, polymer monomers, and antifungal agents
Cas:438226-89-2
Min.Order:0
Negotiable
Type:Other
inquiryhome-produced Application:medicine
Cas:438226-89-2
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryethane-1,2-dithiol
4,5-bis(1,3,2-dithioarsolan-2-yl) resorufin
Conditions | Yield |
---|---|
Stage #1: 4,5-bis(mercurictrifluoroacetate) With palladium diacetate; arsenic trichloride; N-ethyl-N,N-diisopropylamine In 1-methyl-pyrrolidin-2-one at 70℃; for 3h; Stage #2: ethane-1,2-dithiol In 1-methyl-pyrrolidin-2-one; aq. phosphate buffer; acetone pH=7; Cooling; | 97% |
Conditions | Yield |
---|---|
In phosphate buffer; acetone pH=7; |
7-hydroxy-3H-phenoxazin-3-one sodium salt
4,5-bis(1,3,2-dithioarsolan-2-yl) resorufin
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: HgO / 20 °C 1.2: AsCl3; DIEA; Pd(OAc)2 / 2 h / 60 - 70 °C 2.1: acetone; aq. phosphate buffer / pH 7 View Scheme |
resorufin
4,5-bis(1,3,2-dithioarsolan-2-yl) resorufin
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 4 h / 25 °C 2.1: palladium diacetate; N-ethyl-N,N-diisopropylamine; arsenic trichloride / 1-methyl-pyrrolidin-2-one / 3 h / 70 °C 2.2: pH 7 / Cooling View Scheme |
4,5-bis(1,3,2-dithioarsolan-2-yl) resorufin
Conditions | Yield |
---|---|
With mercury(II) diacetate; trifluoroacetic acid In tetrahydrofuran |
Conditions | Yield |
---|---|
With 4-methyl-morpholine In dimethyl sulfoxide at 20℃; for 1h; |
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