CAS No.51-05-8,Procaine hydrochloride Suppliers,MSDS download

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Synthetic route

: 7732-18-5
water

: 4-β-D-glucopyranosylamino-benzoic acid-(2-diethylamino-ethyl ester); hydrochloride

A: 50-99-7
D-glucose

B: 51-05-8
procaine hydrochloride

Conditions

Conditions	Yield
at 20 - 100℃; Equilibrium constant;

...Expand

: 54-21-7
sodium salicylate

: 51-05-8
procaine hydrochloride

: 4344-99-4
procainium salicylate

Conditions

Conditions	Yield
In water; acetone at 20℃;	98%

: 124-38-9
carbon dioxide

: 51-05-8
procaine hydrochloride

: procainium hydrocarbonate

Conditions

Conditions	Yield
With sodium hydrogencarbonate In water at -4 - 0℃; under 760.051 Torr; Product distribution / selectivity;	97.7%

: 529-44-2
myricetin

: 51-05-8
procaine hydrochloride

: 6,8-bis{p-[2-(diethylamino)ethoxycarbonyl]benzeneazo}-3,3',4',5,5',7-hexahydroxyflavone

Conditions

Conditions	Yield
Stage #1: procaine hydrochloride With hydrogenchloride; sodium acetate; sodium nitrite In water Diazotization; Stage #2: myricetin In ethanol; water at 25℃; Substitution;	95%

: 51-05-8
procaine hydrochloride

: 2-diethylaminoethyl 4-amino-3-chlorobenzoate

Conditions

Conditions	Yield
With N-chloro-succinimide; 2,2,6,6-tetramethylpiperidin-1-oxoammonium trifluoromethanesulfonate In chloroform at 25℃; for 12h; Reagent/catalyst; Schlenk technique;	95%

: 51-05-8
procaine hydrochloride

: 996-50-9
N,N-diethyl-1,1,1-trimethylsilanamine

: 76064-19-2
N,N'-Diethylaminoethyl-p-aminobenzoxytrimethylsilane

Conditions

Conditions	Yield
With triethylamine for 2h; Heating;	82%

: 51-05-8
procaine hydrochloride

: 31121-93-4
sodium 2-(4-isobutylphenyl)propionate

: C13H20N2O2*C13H18O2

Conditions

Conditions	Yield
In water at 20℃; for 2h;	79.1%

: 13156-10-0
3-Acetyl-4,5,5-trimethyl-Δ3-butenolide

: 51-05-8
procaine hydrochloride

: 82814-30-0
4-[1-(4,5,5-Trimethyl-2-oxo-2,5-dihydro-furan-3-yl)-eth-(E)-ylideneamino]-benzoic acid 2-diethylamino-ethyl ester

Conditions

Conditions	Yield
With sodium In ethanol for 4h; Heating;	54.4%

: 517-23-7
3-acetyl-2-oxo-4,5-dihydrofuran

: 51-05-8
procaine hydrochloride

: 4-[1-(2-oxo-tetrahydro-[3]furyl)-ethylLiDenamino]-benzoic acid-(2-diethylamino-ethyl ester)

Conditions

Conditions	Yield
at 150℃;

: 50-99-7
D-glucose

: 51-05-8
procaine hydrochloride

: 47593-05-5
4-β-D-glucopyranosylamino-benzoic acid-(2-diethylamino-ethyl ester)

Conditions

Conditions	Yield
With ethanol
With water

: 1835-02-5
2-Bromo-1-(3,4-dimethoxyphenyl)ethanone

: 51-05-8
procaine hydrochloride

: 4-(3,4-dimethoxy-phenacylamino)-benzoic acid-(2-diethylamino-ethyl ester)

Conditions

Conditions	Yield
With water

: 6305-04-0
p-hydroxyphenacyl chloride

: 51-05-8
procaine hydrochloride

: 4-(4-hydroxy-phenacylamino)-benzoic acid-(2-diethylamino-ethyl ester)

Conditions

Conditions	Yield
With water

: 51-05-8
procaine hydrochloride

: 4-amino-3-bromo-benzoic acid-(2-diethylamino-ethyl ester)

Conditions

Conditions	Yield
With water; bromine

: 51-05-8
procaine hydrochloride

: 79-22-1
methyl chloroformate

: 97441-57-1
4-methoxycarbonylamino-benzoic acid-(2-diethylamino-ethyl ester); hydrochloride

: 51-05-8
procaine hydrochloride

: 70-11-1
α-bromoacetophenone

: 4-phenacylamino-benzoic acid-(2-diethylamino-ethyl ester)

Conditions

Conditions	Yield
With water

: 42021-85-2
2,5,8,11,14-pentaoxa-pentadecanedioyl chloride

: 51-05-8
procaine hydrochloride

: 41562-67-8
C36H54N4O11

Conditions

Conditions	Yield
With triethylamine In chloroform

: 87385-94-2
benzaldehyde (4-phenyl-selenazol-2-yl)-hydrazone

: 51-05-8
procaine hydrochloride

: 109054-36-6
4-(4-Phenyl-2-{N'-[1-phenyl-meth-(Z)-ylidene]-hydrazino}-selenazol-5-ylazo)-benzoic acid 2-diethylamino-ethyl ester

Conditions

Conditions	Yield
With hydrogenchloride; sodium nitrite 1.) 0 deg C, 2.) EtOH, 0-5 deg C; Yield given. Multistep reaction;

: 3042-01-1
thiazolo[3,2-a]benzimidazol-3(2H)-one

: 51-05-8
procaine hydrochloride

: 107106-86-5
4-(3-Oxo-2,3-dihydro-benzo[4,5]imidazo[2,1-b]thiazol-2-ylazo)-benzoic acid 2-diethylamino-ethyl ester; hydrochloride

Conditions

Conditions	Yield
With sodium nitrite 1) glacial acetic acid, H2O, 0 deg C, 2) dioxane, 2 h, 5 deg C; Yield given. Multistep reaction;

: 51-05-8
procaine hydrochloride

: 20432-36-4
s-trans-((2trans-4trans)-5-(4-dimethylaminophenyl)phenyl)penta-2,4-dienal

: C26H33N3O2*H(1+)

Conditions

Conditions	Yield
With hydrogenchloride In methanol for 0.166667h;

: 51-05-8
procaine hydrochloride

: 109054-52-6
2-hydroxy-benzaldehyde (4-phenyl-selenazol-2-yl)-hydrazone

: 109081-52-9
4-(2-{N'-[1-(2-Hydroxy-phenyl)-meth-(Z)-ylidene]-hydrazino}-4-phenyl-selenazol-5-ylazo)-benzoic acid 2-diethylamino-ethyl ester

Conditions

Conditions	Yield
With hydrogenchloride; sodium nitrite 1.) 0 deg C, 2.) EtOH, 0-5 deg C; Yield given. Multistep reaction;

: 51-05-8
procaine hydrochloride

: 109054-53-7
4-phenyl-[2-(4-metoxy-benzyliden)-hydrazinyl]-1,3-selenazole

: 109054-37-7
4-(2-{N'-[1-(4-Methoxy-phenyl)-meth-(Z)-ylidene]-hydrazino}-4-phenyl-selenazol-5-ylazo)-benzoic acid 2-diethylamino-ethyl ester

Conditions

Conditions	Yield
With hydrogenchloride; sodium nitrite 1.) 0 deg C, 2.) EtOH, 0-5 deg C; Yield given. Multistep reaction;

: 51-05-8
procaine hydrochloride

: 109054-54-8
4-hydroxy-3-methoxy-benzaldehyde (4-phenyl-selenazol-2-yl)-hydrazone

: 4-(2-{N'-[1-(3-Hydroxy-4-methoxy-phenyl)-meth-(Z)-ylidene]-hydrazino}-4-phenyl-selenazol-5-ylazo)-benzoic acid 2-diethylamino-ethyl ester

Conditions

Conditions	Yield
With hydrogenchloride; sodium nitrite 1.) 0 deg C, 2.) EtOH, 0-5 deg C; Yield given. Multistep reaction;

: 51-05-8
procaine hydrochloride

: 95213-81-3
3-Benzylthiazolidin-2-one-4-thione

: 117014-20-7
4-(3-Benzyl-2-oxo-4-thioxo-thiazolidin-5-ylazo)-benzoic acid 2-diethylamino-ethyl ester; hydrochloride

Conditions

Conditions	Yield
With sodium nitrite 1.) acetic acid, water, 0-5 deg C, 10 min, 2.) dioxane, 0 deg C, 2 h; Yield given. Multistep reaction;

: 51-05-8
procaine hydrochloride

: 60795-47-3
5-Carbamoyl-2-methoxy-benzoyl chloride

: 89366-52-9
4-(5-Carbamoyl-2-methoxy-benzoylamino)-benzoic acid 2-diethylamino-ethyl ester

Conditions

Conditions	Yield
With triethylamine In tetrahydrofuran for 3h; Heating; Yield given;

: 51-05-8
procaine hydrochloride

: 5-Carbamoyl-2-octyloxy-benzoyl chloride

: 89366-50-7
4-(5-Carbamoyl-2-octyloxy-benzoylamino)-benzoic acid 2-diethylamino-ethyl ester

Conditions

Conditions	Yield
With triethylamine In tetrahydrofuran for 3h; Heating; Yield given;

: 51-05-8
procaine hydrochloride

: 2-Methoxy-5-octylcarbamoyl-benzoyl chloride

: 89366-60-9
4-(2-Methoxy-5-octylcarbamoyl-benzoylamino)-benzoic acid 2-diethylamino-ethyl ester

Conditions

Conditions	Yield
With triethylamine In tetrahydrofuran for 3h; Heating; Yield given;

: 51-05-8
procaine hydrochloride

: 5-Isopropylcarbamoyl-2-octyloxy-benzoyl chloride

: 89366-57-4
4-(5-Isopropylcarbamoyl-2-octyloxy-benzoylamino)-benzoic acid 2-diethylamino-ethyl ester

Conditions

Conditions	Yield
With triethylamine In tetrahydrofuran for 3h; Heating; Yield given;

: 51-05-8
procaine hydrochloride

: 5-Isobutylcarbamoyl-2-octyloxy-benzoyl chloride

: 89366-51-8
4-(5-Isobutylcarbamoyl-2-octyloxy-benzoylamino)-benzoic acid 2-diethylamino-ethyl ester

Conditions

Conditions	Yield
With triethylamine In tetrahydrofuran for 3h; Heating; Yield given;

: 51-05-8
procaine hydrochloride

: 5-Cyclohexylcarbamoyl-2-octyloxy-benzoyl chloride

: 89366-53-0
4-(5-Cyclohexylcarbamoyl-2-octyloxy-benzoylamino)-benzoic acid 2-diethylamino-ethyl ester

Conditions

Conditions	Yield
With triethylamine In tetrahydrofuran for 3h; Heating; Yield given;

: 51-05-8
procaine hydrochloride

: 5-Octylcarbamoyl-2-octyloxy-benzoyl chloride

: 89366-59-6
4-(5-Octylcarbamoyl-2-octyloxy-benzoylamino)-benzoic acid 2-diethylamino-ethyl ester

Conditions

Conditions	Yield
With triethylamine In tetrahydrofuran for 3h; Heating; Yield given;

: 51-05-8
procaine hydrochloride

: Procainperiodid

Conditions

Conditions	Yield
With iodine; potassium iodide In ethanol

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