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inquiryProduct Name: 1-BUTOXY-2-PROPANOL Synonyms: PROPYLENE GLYCOL 1-MONOBUTYL ETHER;PROPYLENE GLYCOL MONOBUTYL ETHER;PROPYLENE GLYCOL NORMAL BUTYL ETHER;PNB;ARCOSOLV(R) PNB;1-BUTOXY-2-PROPANOL;1,2-PROPYLENE GLYCOL 1-MONOBUTYL ETHER;1-butoxy
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Conditions | Yield |
---|---|
With Al2O3/MgO composite at 120℃; Inert atmosphere; | 38.5% |
With sodium hydroxide | |
With hematite at 160℃; for 8h; Autoclave; | |
With 1-ethyl-3-methyl-1H-imidazol-3-ium methylcarbonate at 50℃; for 0.166667h; Reagent/catalyst; Microwave irradiation; Green chemistry; |
methyloxirane
butan-1-ol
A
(R)-2-butoxy-1propanol
B
1-butoxy-2-propanol
Conditions | Yield |
---|---|
With sulfuric acid bei Siedetemperatur; | |
With H+-Zeolite X at 35℃; for 24h; Yield given. Yields of byproduct given; | |
With aluminum oxide Yield given. Yields of byproduct given; |
propylene glycol
n-Butyl chloride
A
(R)-2-butoxy-1propanol
B
1-butoxy-2-propanol
C
1,2-dibutoxy-propane
Conditions | Yield |
---|---|
(i) DMSO, NaOH, (ii) /BRN= 1730909/; Multistep reaction; |
Conditions | Yield |
---|---|
In butan-1-ol |
1-bromo-butane
propylene glycol
A
(R)-2-butoxy-1propanol
B
1-butoxy-2-propanol
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydrogensulfate In sodium hydroxide at 80 - 90℃; for 3h; Title compound not separated from byproducts; |
propylene glycol
butyraldehyde
A
cis/trans 2-propyl-4-methyl-1,3-dioxolane
B
(R)-2-butoxy-1propanol
C
1-butoxy-2-propanol
D
butan-1-ol
Conditions | Yield |
---|---|
With hydrogen; palladium 10% on activated carbon at 180℃; under 51716.2 Torr; for 3h; Inert atmosphere; | A 11.9 %Chromat. B n/a C n/a D 5.8 %Chromat. |
With palladium 10% on activated carbon; hydrogen at 180℃; under 51755.2 Torr; for 3h; | A n/a B n/a C n/a D 5.8 %Chromat. |
cis/trans 2-propyl-4-methyl-1,3-dioxolane
A
(R)-2-butoxy-1propanol
B
1-butoxy-2-propanol
Conditions | Yield |
---|---|
With hydrogen; 5%-palladium/activated carbon In propylene glycol at 150℃; under 51680.2 Torr; for 1h; Product distribution / selectivity; Autoclave; |
propylene glycol
butan-1-ol
A
(R)-2-butoxy-1propanol
B
1-butoxy-2-propanol
Conditions | Yield |
---|---|
With bismuth(lll) trifluoromethanesulfonate at 150℃; for 24h; Overall yield = 46 %Chromat.; |
1-butoxy-2-propanol
1-(butoxy)-2-propanone
Conditions | Yield |
---|---|
With oxygen; LnPd(II) at 100℃; for 10h; | 100% |
With 2-chloro-1,3-dimethylimidazolinium chloride; dimethyl sulfoxide; triethylamine In dichloromethane at 20℃; for 47h; Oxidation; | 80% |
With pyridinium chlorochromate; dichloro-acetic acid In nitrobenzene; chlorobenzene at 35℃; Rate constant; Mechanism; different reagent, substrate and catalyst concentrations, catalyst and solvent ratios; | |
With 2,2,6,6-tetramethyl-piperidine-N-oxyl; trichloroisocyanuric acid In dichloromethane at 0 - 20℃; for 4h; |
1-butoxy-2-propanol
acetonitrile
propylene glycol n-butyl ether acetate
Conditions | Yield |
---|---|
With Bromotrichloromethane; [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate at 20℃; for 15h; Irradiation; Inert atmosphere; | 67% |
1-butoxy-2-propanol
bis(pinacol)diborane
Conditions | Yield |
---|---|
With tris(triphenylphosphine)ruthenium(II) chloride; 1,3-bis(dicyclohexylphosphino)propane bis(tetrafluoroborate) salt; pivalaldehyde; iron(II) bromide; sodium t-butanolate In toluene at 100℃; for 6h; Glovebox; Schlenk technique; Inert atmosphere; Sealed tube; | 30% |
1-butoxy-2-propanol
1,7-dibromo-N,N'-bis(2,6-diisopropylphenyl)perylene-3,4:9,10-tetracarboxylic acid diimide
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 3h; Inert atmosphere; | 16% |
1-butoxy-2-propanol
butyl 2-fluoropropyl ether
Conditions | Yield |
---|---|
With diethylamino-sulfur trifluoride | 9% |
1-butoxy-2-propanol
A
formaldehyd
B
n-butyl formate
C
acetaldehyde
D
propionaldehyde
Conditions | Yield |
---|---|
With air; hydroxide at 22.85℃; under 740 Torr; Kinetics; Irradiation; |
Conditions | Yield |
---|---|
With sodium methylate In hexane; water at 53℃; Dean-Stark; |
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