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inquiryIt can be used as a reactive monomer to introduce amino groups into the polymer. The prepared amino group can make the polymer alkaline and cationic, which can improve its cohesiveness. It can be used for dyes; flocculants, paper additives ( For exam
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inquiryName: N,N-Dimethyl Aminopropyl Methacrylamide Synonyms: Dimethylamino propyl methacrylamide CAS: 5205-93-6 MF: C9H18N2O Appearance:Colorless clear liquid Storage:Preserve in well-closed, light-resistant and airtight containers. Package:25kg/drum A
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inquiryBeluga chemical professional supply Dimethylamino propyl methacrylamide CAS 5205-93-6 Why choose Beluga chemical 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and resear
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inquiryProduct Name: Dimethylamino propyl methacrylamide Synonyms: 3-DIMETHYLAMINOPROPYL METHACRYLAMIDE;3-DIMETHYLAMINOPROPYL-METHYLACRYLAMIDE;N-[3-(N,N-DIMETHYLAMINO)PROPYL]METHACRYLAMIDE;N-(3-Dimethylaminopropyl)methacrylamide (stabilized with MEHQ);
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryProduct name: Dimethylaminopropyl Methacrylamide CAS No.:5205-93-6 Molecule Formula:C9H18N2O Molecule Weight:170.25 Purity: 99.0% Package: 200kg/drum Description:Colorless to light yellow liquid Manufacture Standards:Enterprise Standard
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inquiryDimethylamino propyl methacrylamide Basic information Product Name: Dimethylamino propyl methacrylamide Synonyms: 3-DIMETHYLAMINOPROPYL METHACRYLAMIDE;3-DIMETHYLAMINOPROPYL-METHYLACRYLAMIDE;N-[3-(N,N-DIMETHYLAMINO)PROPYL]METHACRYLAMIDE;N-(3-Di
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiry2-(N,N-dimethylamino)ethanol
1-amino-3-(dimethylamino)propane
methacrylic acid methyl ester
A
2-(dimethylamino)ethyl methacrylate
B
2-methyl-acrylic acid 3-dimethylamino-propyl amide
Conditions | Yield |
---|---|
Stage #1: methacrylic acid methyl ester With 10H-phenothiazine; 4-methoxy-phenol Heating / reflux; Neat (no solvent); Stage #2: di(n-butyl)tin oxide at 70 - 101℃; Heating / reflux; Neat (no solvent); Stage #3: 2-(N,N-dimethylamino)ethanol; 1-amino-3-(dimethylamino)propane; titanium(IV) isopropylate Product distribution / selectivity; more than 3 stages; | A 87% B 99.2% |
Stage #1: methacrylic acid methyl ester With 10H-phenothiazine; 4-methoxy-phenol In hexane Heating / reflux; Stage #2: di(n-butyl)tin oxide In hexane at 70 - 101℃; Heating / reflux; Stage #3: 2-(N,N-dimethylamino)ethanol; 1-amino-3-(dimethylamino)propane; titanium(IV) isopropylate Product distribution / selectivity; more than 3 stages; | A 92.3% B 99.6% |
Stage #1: methacrylic acid methyl ester With 10H-phenothiazine; 4-methoxy-phenol Heating / reflux; Neat (no solvent); Stage #2: dioctyltin(IV) oxide at 70 - 101℃; Heating / reflux; Neat (no solvent); Stage #3: 2-(N,N-dimethylamino)ethanol; 1-amino-3-(dimethylamino)propane Product distribution / selectivity; more than 3 stages; | A 86.1% B 84.4% |
Stage #1: methacrylic acid methyl ester With 10H-phenothiazine Heating / reflux; Neat (no solvent); Stage #2: di(n-butyl)tin oxide at 70 - 101℃; Heating / reflux; Neat (no solvent); Stage #3: 2-(N,N-dimethylamino)ethanol; 1-amino-3-(dimethylamino)propane; titanium(IV) isopropylate Product distribution / selectivity; more than 3 stages; | A 82.5% B 90 %Chromat. - 100 % |
p-toluenesulfonic acid 3-dimethylamino-n-propyl ester
2-propenamide
2-methyl-acrylic acid 3-dimethylamino-propyl amide
Conditions | Yield |
---|---|
Stage #1: 2-propenamide With potassium hydroxide In N,N-dimethyl-formamide at 60℃; for 1h; Stage #2: p-toluenesulfonic acid 3-dimethylamino-n-propyl ester In N,N-dimethyl-formamide at 100℃; for 6h; | 95% |
1-amino-3-(dimethylamino)propane
methacrylic acid methyl ester
2-methyl-acrylic acid 3-dimethylamino-propyl amide
Conditions | Yield |
---|---|
Stage #1: methacrylic acid methyl ester With 10H-phenothiazine; 4-methoxy-phenol In xylene at 70℃; Heating / reflux; Stage #2: titanium(IV) isopropylate; di(n-butyl)tin oxide In xylene at 70 - 103℃; Heating / reflux; Stage #3: 1-amino-3-(dimethylamino)propane In xylene at 103 - 150℃; for 4h; Product distribution / selectivity; Heating / reflux; | 93% |
Stage #1: methacrylic acid methyl ester With 10H-phenothiazine In xylene Heating / reflux; Stage #2: di(n-butyl)tin oxide In xylene at 70 - 103℃; Heating / reflux; Stage #3: 1-amino-3-(dimethylamino)propane In xylene at 103 - 150℃; for 5.5h; Product distribution / selectivity; Heating / reflux; | 96.9 - 97.4 %Chromat. |
Stage #1: methacrylic acid methyl ester With 10H-phenothiazine Heating / reflux; Neat (no solvent); Stage #2: di(n-butyl)tin oxide at 70 - 103℃; Heating / reflux; Neat (no solvent); Stage #3: 1-amino-3-(dimethylamino)propane at 103 - 150℃; for 5.5h; Product distribution / selectivity; Heating / reflux; Neat (no solvent); | 95.2 %Chromat. |
3-(Dimethylamino)propyl chloride
2-propenamide
2-methyl-acrylic acid 3-dimethylamino-propyl amide
Conditions | Yield |
---|---|
Stage #1: 2-propenamide With sodium hydride In N,N-dimethyl-formamide; mineral oil at 60℃; for 1h; Stage #2: 3-(Dimethylamino)propyl chloride In N,N-dimethyl-formamide; mineral oil at 80℃; for 4h; | 90% |
β-methoxy-isobutyric acid amide
1-amino-3-(dimethylamino)propane
2-methyl-acrylic acid 3-dimethylamino-propyl amide
Conditions | Yield |
---|---|
With sodium hydroxide | 72% |
Conditions | Yield |
---|---|
With carbon dioxide | 7% |
1-amino-3-(dimethylamino)propane
methacrylic acid methyl ester
A
2-methyl-acrylic acid 3-dimethylamino-propyl amide
Conditions | Yield |
---|---|
at 200℃; Product distribution; also with methyl acrylate; var. temp. and reaction time; also in the presence of amidation catalysts; |
1,2-propanediene
carbon monoxide
1-amino-3-(dimethylamino)propane
2-methyl-acrylic acid 3-dimethylamino-propyl amide
Conditions | Yield |
---|---|
dodecacarbonyl-triangulo-triruthenium In 1,4-dioxane at 100℃; under 9880 Torr; for 18h; | 10 % Chromat. |
β-alaninamide
poly(methacrylic acid)
B
2-methyl-acrylic acid 3-dimethylamino-propyl amide
Conditions | Yield |
---|---|
In water |
poly(methacrylic acid)
1-amino-3-(dimethylamino)propane
2-methyl-acrylic acid 3-dimethylamino-propyl amide
Conditions | Yield |
---|---|
at 150℃; under 7500.75 Torr; Microwave irradiation; | |
Stage #1: poly(methacrylic acid); 1-amino-3-(dimethylamino)propane With 10H-phenothiazine In toluene at 35℃; Cooling with ice; Industry scale; Stage #2: at 253℃; under 15001.5 Torr; for 0.0208333h; Microwave irradiation; Industry scale; |
1-amino-3-(dimethylamino)propane
2-methyl-acrylic acid 3-dimethylamino-propyl amide
Conditions | Yield |
---|---|
With 10H-phenothiazine In toluene at 175 - 185℃; for 0.0333333h; Microwave irradiation; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: N,N-dimethyl-formamide / 6 h / 20 - 50 °C 2.1: potassium hydroxide / N,N-dimethyl-formamide / 1 h / 60 °C 2.2: 6 h / 100 °C View Scheme |
1,3-propanesultone
2-methyl-acrylic acid 3-dimethylamino-propyl amide
N,N-dimethyl-N-(3-sulfopropyl)-3'-methacrylamidopropanaminium inner salt
Conditions | Yield |
---|---|
In acetone at 20℃; for 48h; | 98% |
With oxygen; 4-methoxy-phenol In methanol; acetone at 40 - 45℃; for 2h; Temperature; Reagent/catalyst; | 97.41% |
at 25℃; for 3h; Temperature; Heating; | 93.4% |
In diethyl ether at 20℃; for 24h; | 86% |
Conditions | Yield |
---|---|
With nitrobenzene In acetonitrile at 50℃; for 24h; Schlenk technique; Inert atmosphere; | 95.6% |
Conditions | Yield |
---|---|
In acetonitrile at 65℃; for 144h; Schlenk technique; | 95% |
4-methyl-2-oxo-1,3,2-dioxathiolane
2-methyl-acrylic acid 3-dimethylamino-propyl amide
Conditions | Yield |
---|---|
With hydroquinone In 1,4-dioxane at 97℃; for 2.5h; | 94% |
Conditions | Yield |
---|---|
In acetone at 60℃; for 30h; Inert atmosphere; | 89.6% |
2-methyl-acrylic acid 3-dimethylamino-propyl amide
1,3,2-dioxathiane 2,2-dioxide
Conditions | Yield |
---|---|
With nitrobenzene In acetonitrile at 50℃; for 24h; Schlenk technique; Inert atmosphere; | 88.8% |
N,N'-Methylenebisacrylamide
2-methyl-acrylic acid 3-dimethylamino-propyl amide
2-propenamide
(3-acrylamidophenyl)boronic acid
Conditions | Yield |
---|---|
With α,α'-azodiizobutyramidine-dihydrochloride In water; dimethyl sulfoxide at 60℃; for 20h; | 83.7% |
Conditions | Yield |
---|---|
In dichloromethane at 40℃; for 24h; Inert atmosphere; | 81.1% |
β-Propiolactone
2-methyl-acrylic acid 3-dimethylamino-propyl amide
N,N-dimethyl-N-(3-methacrylamidopropyl)propiobetaine
Conditions | Yield |
---|---|
With 2,2-diphenyl-1-picrylhydrazyl In tetrahydrofuran at 0 - 4℃; for 27h; Inert atmosphere; | 80% |
2-methyl-acrylic acid 3-dimethylamino-propyl amide
4-cyano-4-(thiobenzoylthio)pentanoic acid
poly(N-[3-(dimethylamino)propyl]methacrylamide), terminated with 4-carboxy-2-cyanobutyl-2-yl and thiobenzoylsulfanyl units, product of RAFT polymerization; monomer(s): N-[3-(dimethylamino)propyl]methacrylamide; 4-carboxy-2-cyanobutyl-2-yl dithiobenzoate
Conditions | Yield |
---|---|
With hydrogenchloride; 4,4'-dicyano-4,4'-azo-di-valeric acid In acetate buffer at 70℃; for 1h; pH=5; | 78.77% |
Conditions | Yield |
---|---|
In acetone at 4 - 60℃; for 42h; Inert atmosphere; | 73.9% |
2-acrylamido-2-methylpropanesulfonic acid
2-methyl-acrylic acid 3-dimethylamino-propyl amide
Conditions | Yield |
---|---|
With hydroquinone In water at 20℃; for 72h; Addition; | 71% |
With hydroquinone In water at 70℃; Kinetics; Concentration; |
2-methyl-acrylic acid 3-dimethylamino-propyl amide
acrylic acid
N,N-dimethyl-N-(3-methacrylamidopropyl)propiobetaine
Conditions | Yield |
---|---|
With radical inhibitor at 0 - 20℃; for 5h; Cooling with ice; | 70% |
In water at 70℃; Product distribution; Further Variations:; Reaction partners; Temperatures; Addition; | |
In water Addition; | |
In water-d2 Kinetics; Solvent; | |
With hydroquinone In water at 50℃; Kinetics; Concentration; |
Conditions | Yield |
---|---|
In diethyl ether at 20℃; for 16h; | 39% |
2-methyl-acrylic acid 3-dimethylamino-propyl amide
Conditions | Yield |
---|---|
With sulfuric acid In water at 70℃; for 4h; | 35% |
With sulfuric acid In water Activation energy; | |
With sulfuric acid In water Kinetics; Further Variations:; pH-values; |
methyl 2-iodopropionate
2-methyl-acrylic acid 3-dimethylamino-propyl amide
(3-methacryloylamino-propyl)-(1-methoxycarbonyl-ethyl)-dimethyl-ammonium; iodide
Conditions | Yield |
---|---|
With acetone |
2-methyl-acrylic acid 3-dimethylamino-propyl amide
Ethyl 2-bromopropionate
(1-ethoxycarbonyl-ethyl)-(3-methacryloylamino-propyl)-dimethyl-ammonium; bromide
Conditions | Yield |
---|---|
With acetone |
Conditions | Yield |
---|---|
In water at 70℃; Rate constant; |
Conditions | Yield |
---|---|
With hydrogenchloride In water at 20℃; for 0.5h; quaternization; | 76 % Chromat. |
2-methyl-acrylic acid 3-dimethylamino-propyl amide
(3-methacryloylamino-propyl)-methoxycarbonylmethyl-dimethyl-ammonium; iodide
2-methyl-acrylic acid 3-dimethylamino-propyl amide
ethoxycarbonylmethyl-(3-methacryloylamino-propyl)-dimethyl-ammonium; iodide
2-methyl-acrylic acid 3-dimethylamino-propyl amide
(3-methacryloylamino-propyl)-methoxycarbonylmethyl-dimethyl-ammonium; bromide
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