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Cas:53-94-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:53-94-1
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:53-94-1
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:53-94-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryhight degree of purity Application:Fine chemical intermediates, used as the main raw material for he synthesis of various pesticides, medicines, surfactants, polymer monomers, Ond Ontifungal agents
Cas:53-94-1
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Conditions | Yield |
---|---|
With ammonium chloride; D,L-histidine; zinc at 20 - 30℃; for 0.75h; pH=7.4 - 7.5; | 91% |
With hydrazine hydrate In ethanol; 1,2-dichloro-ethane for 1h; | 66% |
With hydrazine hydrate; palladium on activated charcoal In tetrahydrofuran at 0℃; for 1h; |
N-(9H-fluoren-2-yl)hydroxylamine
benzaldehyde
α-phenyl-N-(2-aminofluorenyl)nitrone
Conditions | Yield |
---|---|
In ethanol at 0 - 15℃; | 95% |
N-(9H-fluoren-2-yl)hydroxylamine
acetyl chloride
N-Hydroxy-2-acetylaminofluoren
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In diethyl ether at 20℃; for 1h; | 78% |
With sodium hydrogencarbonate; triethylamine 1) THF, rt, 30 min, 2) 30 min, rt; Yield given. Multistep reaction; | |
With sodium hydrogencarbonate In diethyl ether at 0℃; |
Acetyl cyanide
N-(9H-fluoren-2-yl)hydroxylamine
O-Acetyl-N-(2-fluorenyl)hydroxylamin
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at -40℃; for 2h; all steps at -40 deg C (at least); | 60% |
N-(9H-fluoren-2-yl)hydroxylamine
Conditions | Yield |
---|---|
Stage #1: N-(9H-fluoren-2-yl)hydroxylamine With 3-chloro-benzenecarboperoxoic acid In toluene at 20℃; for 0.166667h; Inert atmosphere; Stage #2: With (S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate In toluene at -65℃; for 0.0833333h; Inert atmosphere; Stage #3: With benzyl ((1E,3E)-penta-1,3-dien-1-yl)carbamate In toluene at -65℃; for 72h; Diels-Alder Cycloaddition; Inert atmosphere; stereoselective reaction; | 59% |
Methoxyacetyl chloride
N-(9H-fluoren-2-yl)hydroxylamine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In diethyl ether Ambient temperature; Yield given; |
Conditions | Yield |
---|---|
In water for 3h; Heating; Yield given; |
N-(9H-fluoren-2-yl)hydroxylamine
Conditions | Yield |
---|---|
With 4-nitrophenol acetate In ethanol-d6 at 22℃; for 48h; |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In diethyl ether Ambient temperature; Yield given; |
N-(9H-fluoren-2-yl)hydroxylamine
acetic anhydride
N-Hydroxy-2-acetylaminofluoren
Conditions | Yield |
---|---|
In chloroform-d1 at 22℃; | |
With triethylamine In ethyl acetate at 20℃; for 0.5h; |
N-(9H-fluoren-2-yl)hydroxylamine
benzoyl chloride
N-hydroxy-N-2-fluorenylbenzamide
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In diethyl ether Ambient temperature; Yield given; |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In diethyl ether Ambient temperature; Yield given; |
Conditions | Yield |
---|---|
In benzene Ambient temperature; Yield given; |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In diethyl ether Ambient temperature; Yield given; |
Conditions | Yield |
---|---|
In diethyl ether Ambient temperature; Yield given; |
Conditions | Yield |
---|---|
In diethyl ether Yield given; |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In diethyl ether Ambient temperature; Yield given; |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In diethyl ether Ambient temperature; Yield given; |
N-(9H-fluoren-2-yl)hydroxylamine
[8-13C]Guo
Conditions | Yield |
---|---|
With ethylene diamine tetraacetic acid tetrasodium salt; aspirin In phosphate buffer at 23℃; for 0.283333h; pH=7.0; Product distribution; Further Variations:; Reaction partners; reaction time; |
N-(9H-fluoren-2-yl)hydroxylamine
2-fluoren
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 95 percent / ethanol / 0 - 15 °C 2: 87 percent / benzene / 0.17 h / 0 °C 3: 22 percent / ethanol; various solvent(s) / 12 h / 60 °C / pH 7.0 4: 96 percent / Na2CO3; MeOH / 8 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: 60 percent / Et3N / tetrahydrofuran / 2 h / -40 °C / all steps at -40 deg C (at least) 2: 14 percent / tetrahydrofuran; H2O / 1. -40 deg C 2. room temperature View Scheme |
N-(9H-fluoren-2-yl)hydroxylamine
N-acetoxy-N-benzoyl-2-fluorenylamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 95 percent / ethanol / 0 - 15 °C 2: 87 percent / benzene / 0.17 h / 0 °C View Scheme |
N-(9H-fluoren-2-yl)hydroxylamine
N-(benzoyl)-N-(deoxyguanosin-8-yl)-2-aminofluorene
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 95 percent / ethanol / 0 - 15 °C 2: 87 percent / benzene / 0.17 h / 0 °C 3: 22 percent / ethanol; various solvent(s) / 12 h / 60 °C / pH 7.0 View Scheme |
N-(9H-fluoren-2-yl)hydroxylamine
>-2-aminofluorene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1) NEt3, 2) aq. NaHCO3 / 1) THF, rt, 30 min, 2) 30 min, rt 2: 1) N-methylmorpholine, ClCOOiBu / 1) DMF, 15 min, -20 deg C, 2) -20 deg C, 5 min, then rt, 15 min View Scheme |
N-(9H-fluoren-2-yl)hydroxylamine
8-[acetyl(9H-fluoren-2-yl)amino]-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium hydrogencarbonate / diethyl ether / 0 °C 2: caesium carbonate / 1,2-dimethoxyethane / 20 °C / Inert atmosphere View Scheme |
N-(9H-fluoren-2-yl)hydroxylamine
fluorene
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sodium hydrogencarbonate / diethyl ether / 0 °C 2: caesium carbonate / 1,2-dimethoxyethane / 20 °C / Inert atmosphere 3: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran View Scheme |
N-(9H-fluoren-2-yl)hydroxylamine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: sodium hydrogencarbonate / diethyl ether / 0 °C 2: caesium carbonate / 1,2-dimethoxyethane / 20 °C / Inert atmosphere 3: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran 4: pyridine / 20 °C / Inert atmosphere View Scheme |
N-(9H-fluoren-2-yl)hydroxylamine
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: sodium hydrogencarbonate / diethyl ether / 0 °C 2: caesium carbonate / 1,2-dimethoxyethane / 20 °C / Inert atmosphere 3: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran 4: pyridine / 20 °C / Inert atmosphere 5: pyridine / 20 °C / Inert atmosphere View Scheme |
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