CAS No.53623-10-2,3,11-dimethylnonacosan-2-one Suppliers

Shanghai Upbio Tech Co.,Ltd

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Zibo Hangyu Biotechnology Development Co., Ltd

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Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

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Golden Pharma Co., Limited

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Wuhan Circle Star Chem-medical Technology co.,Ltd.

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Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

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Hangzhou Fandachem Co.,Ltd

3,11-DIMETHYLNONACOSAN-2-ONEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

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HuBei Ipure Biotech CO.,ltd

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Nanjing Raymon Biotech Co., Ltd.

2-Nonacosanone,3,11-dimethyl-Appearance:Off white to slight yellow solid Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By

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Synthetic route

: 83165-94-0
3,11-dimethyl-3-nonacosen-2-one

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
With hydrogen; platinum(IV) oxide In ethanol	90%

: 944153-92-8
3,11-dimethyl 3-ethylcarbonylcosan-2-one

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
With sodium hydroxide; tetra(n-butyl)ammonium hydroxide In tetrahydrofuran; water at 20℃; for 2h;	73%

: 204848-20-4
1-methyl-2-(8-methylhexacosyl)-1-cyclopropanol

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
With potassium hydroxide In tetrahydrofuran for 12h; Ambient temperature;	57%

: 57998-45-5
5-methyl-6-oxoheptanoic acid

: 73087-74-8
6-Methyltetracosansaeure

A: 53623-10-2
3,11-dimethylnonacosan-2-one

B: 73087-78-2
3,10-Dimethyl-2,11-dodecandion

C: 73087-79-3
19,28-Dimethylhexatetracontan

Conditions

Conditions	Yield
With potassium hydroxide In methanol coelectroylsis up to pH 9;	A 42.5% B 50% C n/a
With potassium hydroxide In methanol coelectroylsis up to pH 9; Yield given;	A 42.5% B 50% C n/a

...Expand

: 55590-34-6
1-bromo-8-methylhexacosane

: 19753-66-3
triphenylphosphoranylidene-2-butanone

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
(i) nBuLi, THF, hexane, (ii) /BRN= 1818630/, THF; Multistep reaction;

: 56599-07-6
2,10-dimethyl-octacosanoic acid

: 917-54-4
methyllithium

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
In diethyl ether

: 64245-77-8
2-acetyl-2,10-dimethyl-octacos-10-enoic acid benzyl ester

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
With hydrogen; palladium on activated charcoal

: 59410-40-1
3,11-dimethyl-nonacosan-2-ol

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
With chromium(VI) oxide; sulfuric acid In acetone

: 1072-21-5
hexanedial

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 7 steps 1: 65 percent / benzene / 10 h / Heating 2: 80 percent / ammonium nitrate / ethanol / 15 h / 20 - 23 °C 3: 1) Bu-Li / 1) ether, hexane, 0 deg C, 1 h; 2) 20-23 deg C, 2 h 4: 90 percent / H2 / PtO2 / ethanol 5: 50percent H2SO4 / dioxane / 2 h / 40 - 50 °C 6: 1) NaH / 1) THF , t<20 deg C; 2) ether, 35 deg C, 8 h 7: 90 percent / H2 / PtO2 / ethanol View Scheme

: 85110-98-1
8-oxo-non-6-enal

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 6 steps 1: 80 percent / ammonium nitrate / ethanol / 15 h / 20 - 23 °C 2: 1) Bu-Li / 1) ether, hexane, 0 deg C, 1 h; 2) 20-23 deg C, 2 h 3: 90 percent / H2 / PtO2 / ethanol 4: 50percent H2SO4 / dioxane / 2 h / 40 - 50 °C 5: 1) NaH / 1) THF , t<20 deg C; 2) ether, 35 deg C, 8 h 6: 90 percent / H2 / PtO2 / ethanol View Scheme

: 83165-91-7
1,1-diethoxy-6-nonen-8-one

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1: 1) Bu-Li / 1) ether, hexane, 0 deg C, 1 h; 2) 20-23 deg C, 2 h 2: 90 percent / H2 / PtO2 / ethanol 3: 50percent H2SO4 / dioxane / 2 h / 40 - 50 °C 4: 1) NaH / 1) THF , t<20 deg C; 2) ether, 35 deg C, 8 h 5: 90 percent / H2 / PtO2 / ethanol View Scheme

: 944153-91-7
1-bromomethylhexacosan-8-ol

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 93 percent / triethylsilane; BF3*OEt2 / CH2Cl2 / 2 h / 0 °C 2: 93 percent / K2CO3; KI / acetone / 20 h / Heating 3: 73 percent / NaOH; tetrabutylammonium hydroxide / tetrahydrofuran; H2O / 2 h / 20 °C View Scheme

: 112-92-5
1-octadecanol

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1.1: 95 percent / phosphorus tribromide / diethyl ether / 2 h / Heating 2.1: Li / diethyl ether / -10 - 10 °C 2.2: 60 percent / diethyl ether / 3 h / 0 °C 3.1: 93 percent / triethylsilane; BF3*OEt2 / CH2Cl2 / 2 h / 0 °C 4.1: 93 percent / K2CO3; KI / acetone / 20 h / Heating 5.1: 73 percent / NaOH; tetrabutylammonium hydroxide / tetrahydrofuran; H2O / 2 h / 20 °C View Scheme

Yield

Multi-step reaction with 5 steps
1.1: 95 percent / phosphorus tribromide / diethyl ether / 2 h / Heating
2.1: Li / diethyl ether / -10 - 10 °C
2.2: 60 percent / diethyl ether / 3 h / 0 °C
3.1: 93 percent / triethylsilane; BF3*OEt2 / CH2Cl2 / 2 h / 0 °C
4.1: 93 percent / K2CO3; KI / acetone / 20 h / Heating
5.1: 73 percent / NaOH; tetrabutylammonium hydroxide / tetrahydrofuran; H2O / 2 h / 20 °C
View Scheme

: 629-41-4
1,8-Octanediol

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 7 steps 1.1: 72 percent / HBr / benzene / 18 h / Heating 2.1: 80 percent / Jones reagent / acetone / 1 h / 0 - 20 °C 3.1: 64 percent / tetrahydrofuran; diethyl ether / 1 h / -78 - 0 °C 4.1: Li / diethyl ether / -10 - 10 °C 4.2: 60 percent / diethyl ether / 3 h / 0 °C 5.1: 93 percent / triethylsilane; BF3*OEt2 / CH2Cl2 / 2 h / 0 °C 6.1: 93 percent / K2CO3; KI / acetone / 20 h / Heating 7.1: 73 percent / NaOH; tetrabutylammonium hydroxide / tetrahydrofuran; H2O / 2 h / 20 °C View Scheme

Yield

Multi-step reaction with 7 steps
1.1: 72 percent / HBr / benzene / 18 h / Heating
2.1: 80 percent / Jones reagent / acetone / 1 h / 0 - 20 °C
3.1: 64 percent / tetrahydrofuran; diethyl ether / 1 h / -78 - 0 °C
4.1: Li / diethyl ether / -10 - 10 °C
4.2: 60 percent / diethyl ether / 3 h / 0 °C
5.1: 93 percent / triethylsilane; BF3*OEt2 / CH2Cl2 / 2 h / 0 °C
6.1: 93 percent / K2CO3; KI / acetone / 20 h / Heating
7.1: 73 percent / NaOH; tetrabutylammonium hydroxide / tetrahydrofuran; H2O / 2 h / 20 °C
View Scheme

: 17696-11-6
8-bromooctanoic acid

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1.1: 64 percent / tetrahydrofuran; diethyl ether / 1 h / -78 - 0 °C 2.1: Li / diethyl ether / -10 - 10 °C 2.2: 60 percent / diethyl ether / 3 h / 0 °C 3.1: 93 percent / triethylsilane; BF3*OEt2 / CH2Cl2 / 2 h / 0 °C 4.1: 93 percent / K2CO3; KI / acetone / 20 h / Heating 5.1: 73 percent / NaOH; tetrabutylammonium hydroxide / tetrahydrofuran; H2O / 2 h / 20 °C View Scheme

Yield

Multi-step reaction with 5 steps
1.1: 64 percent / tetrahydrofuran; diethyl ether / 1 h / -78 - 0 °C
2.1: Li / diethyl ether / -10 - 10 °C
2.2: 60 percent / diethyl ether / 3 h / 0 °C
3.1: 93 percent / triethylsilane; BF3*OEt2 / CH2Cl2 / 2 h / 0 °C
4.1: 93 percent / K2CO3; KI / acetone / 20 h / Heating
5.1: 73 percent / NaOH; tetrabutylammonium hydroxide / tetrahydrofuran; H2O / 2 h / 20 °C
View Scheme

: 55590-34-6
1-bromo-8-methylhexacosane

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 93 percent / K2CO3; KI / acetone / 20 h / Heating 2: 73 percent / NaOH; tetrabutylammonium hydroxide / tetrahydrofuran; H2O / 2 h / 20 °C View Scheme
Multi-step reaction with 2 steps 1: KOH / ethanol / 0.75 h / 180 - 185 °C 2: diethyl ether View Scheme

: 50816-19-8
8-bromooctanol

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 6 steps 1.1: 80 percent / Jones reagent / acetone / 1 h / 0 - 20 °C 2.1: 64 percent / tetrahydrofuran; diethyl ether / 1 h / -78 - 0 °C 3.1: Li / diethyl ether / -10 - 10 °C 3.2: 60 percent / diethyl ether / 3 h / 0 °C 4.1: 93 percent / triethylsilane; BF3*OEt2 / CH2Cl2 / 2 h / 0 °C 5.1: 93 percent / K2CO3; KI / acetone / 20 h / Heating 6.1: 73 percent / NaOH; tetrabutylammonium hydroxide / tetrahydrofuran; H2O / 2 h / 20 °C View Scheme

Yield

Multi-step reaction with 6 steps
1.1: 80 percent / Jones reagent / acetone / 1 h / 0 - 20 °C
2.1: 64 percent / tetrahydrofuran; diethyl ether / 1 h / -78 - 0 °C
3.1: Li / diethyl ether / -10 - 10 °C
3.2: 60 percent / diethyl ether / 3 h / 0 °C
4.1: 93 percent / triethylsilane; BF3*OEt2 / CH2Cl2 / 2 h / 0 °C
5.1: 93 percent / K2CO3; KI / acetone / 20 h / Heating
6.1: 73 percent / NaOH; tetrabutylammonium hydroxide / tetrahydrofuran; H2O / 2 h / 20 °C
View Scheme

: 52330-02-6
8-bromononan-2-one

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1.1: Li / diethyl ether / -10 - 10 °C 1.2: 60 percent / diethyl ether / 3 h / 0 °C 2.1: 93 percent / triethylsilane; BF3*OEt2 / CH2Cl2 / 2 h / 0 °C 3.1: 93 percent / K2CO3; KI / acetone / 20 h / Heating 4.1: 73 percent / NaOH; tetrabutylammonium hydroxide / tetrahydrofuran; H2O / 2 h / 20 °C View Scheme

: 112-89-0
1-Bromooctadecane

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1.1: Li / diethyl ether / -10 - 10 °C 1.2: 60 percent / diethyl ether / 3 h / 0 °C 2.1: 93 percent / triethylsilane; BF3*OEt2 / CH2Cl2 / 2 h / 0 °C 3.1: 93 percent / K2CO3; KI / acetone / 20 h / Heating 4.1: 73 percent / NaOH; tetrabutylammonium hydroxide / tetrahydrofuran; H2O / 2 h / 20 °C View Scheme

: 66344-19-2
3-Methylheneicosansaeure

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 66 percent / KOH (neutralisation to 2.8percent) / methanol / coelectrolysis up to pH 8 2: 80 percent / NaOH / methanol; H2O / 10 h / Heating 3: 42.5 percent / KOH (neutralisation to 6percent) / methanol / coelectroylsis up to pH 9 View Scheme

: 92206-73-0
1-octadecylmagnesium bromide

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1: CuCl / diethyl ether / 3 h / 0 °C 2: KOH / methanol / 20 h 3: 66 percent / KOH (neutralisation to 2.8percent) / methanol / coelectrolysis up to pH 8 4: 80 percent / NaOH / methanol; H2O / 10 h / Heating 5: 42.5 percent / KOH (neutralisation to 6percent) / methanol / coelectroylsis up to pH 9 View Scheme

: 73087-75-9
2-Acetyl-2-methyladipinsaeure-diethylester

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 80 percent / aq. HCl, 50percent HAc / 24 h / Heating 2: 42.5 percent / KOH (neutralisation to 6percent) / methanol / coelectroylsis up to pH 9 View Scheme

: 3-Methylheneicosansaeure-sek-butylester

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: KOH / methanol / 20 h 2: 66 percent / KOH (neutralisation to 2.8percent) / methanol / coelectrolysis up to pH 8 3: 80 percent / NaOH / methanol; H2O / 10 h / Heating 4: 42.5 percent / KOH (neutralisation to 6percent) / methanol / coelectroylsis up to pH 9 View Scheme

: 73087-76-0
6-Methyltetracosansaeure-methylester

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 80 percent / NaOH / methanol; H2O / 10 h / Heating 2: 42.5 percent / KOH (neutralisation to 6percent) / methanol / coelectroylsis up to pH 9 View Scheme

: 25542-64-7
8-oxononanoic acid

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 7 steps 1: diethyl ether / 5 °C 2: dimethylformamide; tetrahydrofuran / 36 h / 25 °C 3: H2 / PtO2 4: LiAlH4 / diethyl ether / 6 h / 25 °C 5: aq. HBr, H2SO4 / 5 h / Heating 6: KOH / ethanol / 0.75 h / 180 - 185 °C 7: diethyl ether View Scheme

: 56599-05-4
8-methyl-hexacosan-1-ol

: 53623-10-2
3,11-dimethylnonacosan-2-one

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: aq. HBr, H2SO4 / 5 h / Heating 2: KOH / ethanol / 0.75 h / 180 - 185 °C 3: diethyl ether View Scheme

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