As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1699.html Product Name 10,10-Dimethylanthrone CAS No. 5447-86-9
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inquiry10,10-Dimethylanthrone 10,10-Dimethylanthrone Basic information Product Name: 10,10-Dimethylanthrone Synonyms: 10,10-dimethylanthracen-9(10H)-one;10,10-Dimethylanthrone;10,10-D
With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiry1,In No Less five years exporting experience. 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Appearance:white-off solid or colorless liquid
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inquiry10,10-Dimethylanthrone CAS:5447-86-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic int
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Appearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By
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inquiry10-10-DIMETHYLANTHRONE (5447-86-9) Information The produce is Meritroxine intermediate. Quality Advanced technology Supper quality Effective & safety package
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:5447-86-9
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Hot sale Top quality 5447-86-9 low price 10,10-Dimethylanthrone Molecular Formula C16H14O Molar Mass 222.28 Density 1.105±0.06 g/cm3(Predicted) Melting Point 101-103°C Boling Point
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inquiryOur Advantages Production: Advanced chemical equipment with years of experience.Staffs for producing various extract products. Quality Control:A complete set of Testing Professional and Analysis Equipment ensures the Quality Requirements and Speci
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Cas:5447-86-9
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inquiryProduct name: 10,10-Dimethylanthracen-9(10)-One CAS No.: 5447-86-9 Molecule Formula:C16H14O Molecule Weight:222.28 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:5447-86-9
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inquiry9,9-Dimethyl-10-(trimethylsilyl)-9,10-dihydroanthracene
10,10-dimethyl-9,10-dihydroanthracen-9-one
Conditions | Yield |
---|---|
With sodium dichromate; acetic acid for 12h; Ambient temperature; | 90% |
With sodium dichromate; acetic acid for 12h; Ambient temperature; other 9,9-dialkyl-10-(trimethylsilyl)- and 9,9-dialkyl-9,10-dihydroanthracenes; | 90% |
9-diazo-10,10-dimethyl-9,10-dihydroanthracene
A
10,10-dimethyl-9,10-dihydroanthracen-9-one
B
10-[10,10-dimethyl-9(10H)-anthracenyl]-9,10-dihydro-9,9-dimethylanthracene
Conditions | Yield |
---|---|
With (Z)-2-Butene Irradiation; | A 8% B 80% |
9,10-Dihydro-10,10-dimethylanthracen
10,10-dimethyl-9,10-dihydroanthracen-9-one
Conditions | Yield |
---|---|
With bromine In tetrachloromethane for 6h; Heating; Irradiation; | 70% |
With chromium(VI) oxide In acetic acid |
(8aR,9R)-8a,9-Dimethyl-8a,9-dihydro-anthracen-9-ol
A
10,10-dimethyl-9,10-dihydroanthracen-9-one
B
9,10-Dihydro-10,10-dimethylanthracen
Conditions | Yield |
---|---|
With sulfuric acid; acetic anhydride In acetic acid | A 25% B 53% |
9,9a-dihydro-9,9a-dimethyl-9-anthracenol
A
10,10-dimethyl-9,10-dihydroanthracen-9-one
B
9,10-Dihydro-10,10-dimethylanthracen
Conditions | Yield |
---|---|
With sulfuric acid; acetic anhydride In acetic acid at 23℃; for 2.25h; | A 25% B 53% |
acetic anhydride
9,9a-dihydro-9,9a-dimethyl-9-anthracenol
A
10,10-dimethyl-9,10-dihydroanthracen-9-one
B
9,10-Dihydro-10,10-dimethylanthracen
C
10,10-dimethyl-9,10-dihydroanthranylacetic acid
Conditions | Yield |
---|---|
With sulfuric acid for 2h; Yields of byproduct given; | A n/a B n/a C 45% |
dimethylketene
N-(10,10-dimethyl-9,10-dihydroanthracen-9-ylidene)phenylamine N-oxide
A
10,10-dimethyl-9,10-dihydroanthracen-9-one
B
4',4',10,10-tetramethyl-3'-phenyl-9,10-dihydroanthracene-9-spiro-2'-oxazolidin-5'-one
Conditions | Yield |
---|---|
In ethyl acetate Ambient temperature; | A 150 mg B 24% |
2-(1-hydroxy-1-methyl-ethyl)-benzophenone cyclohemiacetal
10,10-dimethyl-9,10-dihydroanthracen-9-one
Conditions | Yield |
---|---|
With sulfuric acid at 150℃; for 1.5h; | 20% |
With PPA | |
With sulfuric acid at 150 - 155℃; for 5h; | 105 g |
(8aR,9R)-8a,9-Dimethyl-8a,9-dihydro-anthracen-9-ol
A
10,10-dimethyl-9,10-dihydroanthracen-9-one
B
9,10-Dihydro-10,10-dimethylanthracen
C
10,10-dimethyl-9,10-dihydroanthranylacetic acid
Conditions | Yield |
---|---|
A 10% B 15% C 75 % Spectr. |
anthracen-9(10H)-one
methyl iodide
10,10-dimethyl-9,10-dihydroanthracen-9-one
Conditions | Yield |
---|---|
12% | |
With potassium hydroxide | |
(i) Li, MeOH, toluene, (ii) /BRN= 969135/, tBuOH; Multistep reaction; | |
With lithium methanolate 1) toluene, 100-120 deg C; 140 deg C 2) tBuOH, 24 h, 140-150 deg C; Yield given. Multistep reaction; | |
With sodium hydroxide In dichloromethane at 20℃; for 15h; | 100 % Spectr. |
Conditions | Yield |
---|---|
Lithium-Verbindung; | |
With water; potassium carbonate |
anthracen-9(10H)-one
methyl iodide
A
10,10-dimethyl-9,10-dihydroanthracen-9-one
B
methyl-9-methoxy-10-anthracene
Conditions | Yield |
---|---|
With potassium hydroxide |
o-Isopropylbenzophenon-oxim
chloroacetic acid
10,10-dimethyl-9,10-dihydroanthracen-9-one
Conditions | Yield |
---|---|
(i) NaOH, aq. EtOH, (ii) K2S2O8, aq. NaOH; Multistep reaction; |
9,10-dihydro-10,10-dimethyl-9-anthracenol
A
10,10-dimethyl-9,10-dihydroanthracen-9-one
B
9,10-Dihydro-10,10-dimethylanthracen
Conditions | Yield |
---|---|
With sulfuric acid In acetic acid for 3h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
methylene chloride
10-nitro-9-methylanthracene
10,10-dimethyl-9,10-dihydroanthracen-9-one
Conditions | Yield |
---|---|
Yield given. Multistep reaction; |
9,10-dihydro-10,10-dimethyl-9-anthracenol
acetic anhydride
A
10,10-dimethyl-9,10-dihydroanthracen-9-one
B
9,10-Dihydro-10,10-dimethylanthracen
C
10,10-dimethyl-9,10-dihydroanthranylacetic acid
Conditions | Yield |
---|---|
With sulfuric acid for 2h; Yields of byproduct given; |
anthracen-9(10H)-one
methyl iodide
A
10,10-dimethyl-9,10-dihydroanthracen-9-one
B
methyl-9-methoxy-10-anthracene
C
9-methoxyanthracene
D
9,10-phenanthrenequinone
Conditions | Yield |
---|---|
With potassium hydroxide; 18-crown-6 ether 1.) toluene, 70 deg C, 2.) toluene, 70 deg C, 3.5 h; r.t. 12 h; Yield given. Multistep reaction. Yields of byproduct given; | |
With potassium hydroxide; 18-crown-6 ether 1.) toluene, 70 deg C, 2.) toluene, 70 deg C, 3.5 h; r.t. 12 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
With toluene Erhitzen des Reaktionsprodukts mit CH3I und wenig tert-Butylalkohol; |
anthracen-9(10H)-one
methyl iodide
10,10-dimethyl-9,10-dihydroanthracen-9-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 83 percent / diethyl ether / 0 °C 2: 20 percent / H2SO4 / 1.5 h / 150 °C View Scheme | |
Multi-step reaction with 2 steps 2: polyphosphoric acid View Scheme | |
Multi-step reaction with 2 steps 1.1: magnesium; iodine / tetrahydrofuran / 2 h / Reflux 1.2: 5 h / 20 °C 2.1: sulfuric acid / 5 h / 150 - 155 °C View Scheme |
9a-hydro-9a-methyl-9-anthracenone
10,10-dimethyl-9,10-dihydroanthracen-9-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 71 percent / diethyl ether / 1.) -70 deg C -> 0 deg C, 1 h, 2.) 23 deg C, 1 h 2: 25 percent / conc. sulfuric acid, acetic anhydride / acetic acid / 2.25 h / 23 °C View Scheme | |
Multi-step reaction with 2 steps 1: 71 percent 2: 25 percent / sulfuric acid, Ac2O / acetic acid View Scheme | |
Multi-step reaction with 2 steps 1: 71 percent 2: 10 percent View Scheme |
C23H22N2O2S
10,10-dimethyl-9,10-dihydroanthracen-9-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 77 percent / sodium methoxide / pyridine / 70 °C 2: 8 percent / cis-2-butene / Irradiation View Scheme |
1,4,9a-trihydro-9a-methyl-9-anthracenone
10,10-dimethyl-9,10-dihydroanthracen-9-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1.)Bromine 2.)DBU / 2.)benzene 2: 71 percent 3: 25 percent / sulfuric acid, Ac2O / acetic acid View Scheme | |
Multi-step reaction with 3 steps 1: 1.)Bromine 2.)DBU / 2.)benzene 2: 71 percent 3: 10 percent View Scheme | |
Multi-step reaction with 4 steps 1: 55 percent / methylenetriphenylphosphorane 2: 1.)Bromine 2.)DBU / 2.)benzene 3: 71 percent 4: 25 percent / sulfuric acid, Ac2O / acetic acid View Scheme | |
Multi-step reaction with 4 steps 1: 55 percent / methylenetriphenylphosphorane 2: 1.)Bromine 2.)DBU / 2.)benzene 3: 71 percent 4: 10 percent View Scheme |
1,2,9a-trihydro-9a-methyl-9-anthracenone
10,10-dimethyl-9,10-dihydroanthracen-9-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1.)Bromine 2.)DBU / 2.)benzene 2: 71 percent 3: 25 percent / sulfuric acid, Ac2O / acetic acid View Scheme | |
Multi-step reaction with 3 steps 1: 1.)Bromine 2.)DBU / 2.)benzene 2: 71 percent 3: 10 percent View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: magnesium / tetrahydrofuran / 2 h / Reflux 1.2: 2 h / 20 °C 2.1: magnesium; iodine / tetrahydrofuran / 2 h / Reflux 2.2: 5 h / 20 °C 3.1: sulfuric acid / 5 h / 150 - 155 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: magnesium; iodine / tetrahydrofuran / 2 h / Reflux 1.2: 2 h / 20 °C 2.1: magnesium; iodine / tetrahydrofuran / 2 h / Reflux 2.2: 5 h / 20 °C 3.1: sulfuric acid / 5 h / 150 - 155 °C View Scheme |
Conditions | Yield |
---|---|
Stage #1: 3-(Dimethylamino)propyl chloride With iodine; magnesium In diethyl ether; ethylene dibromide at 30 - 35℃; for 9h; Reflux; Large scale; Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In diethyl ether; ethylene dibromide at 10 - 35℃; for 1h; Reflux; Large scale; | 97.2% |
10,10-dimethyl-9,10-dihydroanthracen-9-one
10,10-dimethylanthrone hydrazone
Conditions | Yield |
---|---|
With hydrazine hydrochloride; hydrazine hydrate In various solvent(s) Heating; | 95% |
With hydrazinium sulfate; hydrazine Heating; Yield given; |
Conditions | Yield |
---|---|
Stage #1: 9,10-Dibromoanthracene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Inert atmosphere; Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran; hexane at 20℃; for 16h; Inert atmosphere; | 93% |
10,10-dimethyl-9,10-dihydroanthracen-9-one
(4-bromophenyl)magnesium bromide
Conditions | Yield |
---|---|
In tetrahydrofuran at 60℃; for 24h; Grignard Reaction; | 88% |
Conditions | Yield |
---|---|
Stage #1: 1.4-dibromobenzene With magnesium In tetrahydrofuran for 4h; Inert atmosphere; Reflux; Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at 60℃; for 24h; | 88% |
10,10-dimethyl-9,10-dihydroanthracen-9-one
9,10-Dihydro-10,10-dimethylanthracen
Conditions | Yield |
---|---|
With dimethylsulfide borane complex In tetrahydrofuran for 2h; Reflux; | 85% |
With lithium aluminium tetrahydride; aluminium trichloride In diethyl ether for 0.333333h; Heating; | 27% |
With potassium hydroxide; hydrazine hydrate In ethylene glycol | |
With hydrazine In diethylene glycol for 4h; Heating; |
4-(4-bromophenyl)dibenzofuran
10,10-dimethyl-9,10-dihydroanthracen-9-one
Conditions | Yield |
---|---|
Stage #1: 4-(4-bromophenyl)dibenzofuran With magnesium In tetrahydrofuran for 4h; Inert atmosphere; Reflux; Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at 60℃; for 24h; Inert atmosphere; | 85% |
10,10-dimethyl-9,10-dihydroanthracen-9-one
Conditions | Yield |
---|---|
Stage #1: 4-(2-bromo-4-chlorophenyl)dibenzofuran With n-butyllithium In tetrahydrofuran at -78℃; for 0.5h; Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at -78 - 20℃; for 1h; | 85% |
10,10-dimethyl-9,10-dihydroanthracen-9-one
(4-(di([1,1’-biphenyl]-4-yl)amino)phenyl)boronic acid
Conditions | Yield |
---|---|
Stage #1: 10,10-dimethyl-9,10-dihydroanthracen-9-one With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h; Stage #2: (4-(di([1,1’-biphenyl]-4-yl)amino)phenyl)boronic acid With potassium carbonate In toluene at 110℃; for 5h; | 84% |
Conditions | Yield |
---|---|
Stage #1: 10,10-dimethyl-9,10-dihydroanthracen-9-one With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h; Stage #2: C44H39BN2O2 With potassium carbonate In toluene at 110℃; for 5h; | 84% |
Conditions | Yield |
---|---|
Stage #1: 10,10-dimethyl-9,10-dihydroanthracen-9-one With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h; Stage #2: C32H24BNO2 With potassium carbonate In toluene at 110℃; for 5h; | 83% |
10,10-dimethyl-9,10-dihydroanthracen-9-one
Conditions | Yield |
---|---|
With N-Bromosuccinimide In N,N-dimethyl-formamide at 20℃; for 18h; Darkness; | 83% |
10,10-dimethyl-9,10-dihydroanthracen-9-one
1-Bromo-5-chloronaphthalene
Conditions | Yield |
---|---|
Stage #1: 1-Bromo-5-chloronaphthalene With n-butyllithium In tetrahydrofuran at -78 - 20℃; for 2h; Inert atmosphere; Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at 0℃; for 10h; Inert atmosphere; | 83% |
Conditions | Yield |
---|---|
Stage #1: 2-bromo-7-chloronaphthalene With n-butyllithium In tetrahydrofuran at -78 - 20℃; for 2h; Inert atmosphere; Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at 20℃; for 10h; Inert atmosphere; | 83% |
Conditions | Yield |
---|---|
Stage #1: 2-(4-bromophenyl]pyridine With magnesium In tetrahydrofuran for 4h; Inert atmosphere; Reflux; Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at 60℃; for 24h; Inert atmosphere; | 82% |
bromobenzene
10,10-dimethyl-9,10-dihydroanthracen-9-one
10,10-dimethyl-9-phenyl-9,10-dihydroanthracen-9-ol
Conditions | Yield |
---|---|
Stage #1: bromobenzene With n-butyllithium In tetrahydrofuran at -78 - 20℃; for 3.5h; Inert atmosphere; Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at -78 - 20℃; for 16h; | 82% |
Stage #1: bromobenzene With iodine; magnesium In tetrahydrofuran at 40 - 80℃; for 4h; Inert atmosphere; Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran for 15h; Inert atmosphere; Reflux; | 76.8% |
Stage #1: bromobenzene With iodine; magnesium In tetrahydrofuran at 40 - 80℃; for 4h; Inert atmosphere; Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran for 15h; Inert atmosphere; Reflux; | 76.3% |
10,10-dimethyl-9,10-dihydroanthracen-9-one
1-bromo-4-chloronaphthalene
Conditions | Yield |
---|---|
Stage #1: 1-bromo-4-chloronaphthalene With n-butyllithium In tetrahydrofuran at -78 - 20℃; for 2h; Inert atmosphere; Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at 20℃; for 10h; Inert atmosphere; | 82% |
Conditions | Yield |
---|---|
Stage #1: 10,10-dimethyl-9,10-dihydroanthracen-9-one With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h; Stage #2: C27H25BN2O3 With potassium carbonate In toluene at 110℃; for 5h; | 81% |
Conditions | Yield |
---|---|
Stage #1: 10,10-dimethyl-9,10-dihydroanthracen-9-one With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h; Stage #2: C41H35BN2O2 With potassium carbonate In toluene at 110℃; for 5h; | 81% |
10,10-dimethyl-9,10-dihydroanthracen-9-one
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid at 5℃; for 0.5h; | 80% |
With sulfuric acid; nitric acid at 5 - 10℃; for 0.5h; | 80% |
With sulfuric acid; nitric acid at 5 - 10℃; for 0.5h; | 80% |
With nitric acid at 5 - 10℃; for 0.5h; | 80% |
With sulfuric acid; nitric acid at 5 - 10℃; for 0.5h; | 80% |
10,10-dimethyl-9,10-dihydroanthracen-9-one
4-(diphenylamino)phenyl boronic acid
Conditions | Yield |
---|---|
Stage #1: 10,10-dimethyl-9,10-dihydroanthracen-9-one With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h; Stage #2: 4-(diphenylamino)phenyl boronic acid With potassium carbonate In toluene at 110℃; for 5h; | 80% |
10,10-dimethyl-9,10-dihydroanthracen-9-one
4-(di-naphthalene-2-yl-amino)-phenylboronic acid
Conditions | Yield |
---|---|
Stage #1: 10,10-dimethyl-9,10-dihydroanthracen-9-one With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h; Stage #2: 4-(di-naphthalene-2-yl-amino)-phenylboronic acid With potassium carbonate In toluene at 110℃; for 5h; | 80% |
10,10-dimethyl-9,10-dihydroanthracen-9-one
(2,6-dimethylphenyl)magnesium bromide
Conditions | Yield |
---|---|
In tetrahydrofuran 1.) RT, 3 h, 2.) 80 deg C, 1 h; | 78% |
Conditions | Yield |
---|---|
Stage #1: C12H8BrClO With n-butyllithium In tetrahydrofuran at -78℃; for 0.5h; Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at -78 - 20℃; for 1h; | 75.8% |
Conditions | Yield |
---|---|
Stage #1: 2-bromo-4-chloro-1-phenoxybenzene With n-butyllithium In tetrahydrofuran at -78℃; for 0.166667h; Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran Stage #3: With sulfuric acid; acetic acid Reflux; | 75.58% |
10,10-dimethyl-9,10-dihydroanthracen-9-one
N,N-dimethylethylenediamine
N'-(10,10-Dimethyl-10H-anthracen-9-ylidene)-N,N-dimethyl-ethane-1,2-diamine
Conditions | Yield |
---|---|
With N,N,N,N,N,N-hexamethylphosphoric triamide; titanium tetrachloride In benzene for 144h; Ambient temperature; | 69% |
10,10-dimethyl-9,10-dihydroanthracen-9-one
Conditions | Yield |
---|---|
With water-d2; magnesium; ethylene dibromide In tetrahydrofuran at 70℃; for 2h; Inert atmosphere; Schlenk technique; | 69% |
With water-d2; magnesium; ethylene dibromide In tetrahydrofuran | 69% |
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