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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

10,10-Dimethylanthrone Manufacturer/High quality/Best price/In stock

Cas:5447-86-9

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

10,10-Dimethylanthrone

Cas:5447-86-9

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 10,10-dimethylanthracen-9(10H)-one

Cas:5447-86-9

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Quality 99% 5447-86-9 10,10-dimethylanthracen-9(10H)-one Manufacturer

Cas:5447-86-9

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

10,10-Dimethyl-9-anthrone

Cas:5447-86-9

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com/pro01en/id/1699.html Product Name 10,10-Dimethylanthrone CAS No. 5447-86-9

10,10-Dimethylanthrone

Cas:5447-86-9

Min.Order:1 Gram

FOB Price: $2.0

Type:Lab/Research institutions

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Henan Tianfu Chemical Co., Ltd.

10,10-Dimethylanthrone 10,10-Dimethylanthrone Basic information Product Name: 10,10-Dimethylanthrone Synonyms: 10,10-dimethylanthracen-9(10H)-one;10,10-Dimethylanthrone;10,10-D

5447-86-9

Cas:5447-86-9

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

10,10-Dimethylanthrone

Cas:5447-86-9

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 5447-86-9 with competitive price

Cas:5447-86-9

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

10,10-dimethylanthracen-9(10H)-one

Cas:5447-86-9

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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LIDE PHARMACEUTICALS LIMITED

Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&amp

10,10-Dimethylanthrone/ LIDE PHARMA- Factory supply / Best price

Cas:5447-86-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after the dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available &diam

10,10-Dimethylanthrone CAS 5447-86-9

Cas:5447-86-9

Min.Order:1 Kilogram

FOB Price: $5.0 / 10.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1,In No Less five years exporting experience. 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Appearance:white-off solid or colorless liquid

Hotsale 10,10-Dimethylanthrone

Cas:5447-86-9

Min.Order:25 Kilogram

FOB Price: $9.0

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

10,10-Dimethylanthrone CAS:5447-86-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic int

10,10-Dimethylanthrone CAS:5447-86-9

Cas:5447-86-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Terui OP New Material Technology Co., Ltd.

We have overseas warehouses in California, New Laredo Mexico, Vancouver Canada, Amsterdam Netherlands, and Melbourne Australia. Overseas warehouses can provide some of the best-selling products. We look forward to the cooperation of local powerful

factory Outlet CAS 5447-86-9 10,10-Dimethylanthrone

Cas:5447-86-9

Min.Order:0 Metric Ton

Negotiable

Type:Trading Company

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

10,10-Dimethylanthrone

Cas:5447-86-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:5447-86-9

Cas:5447-86-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

10,10-Dimethylanthrone

Cas:5447-86-9

Min.Order:0

Negotiable

Type:Manufacturers

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Triumph International Development Limilted

Appearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By

10,10-dimethylanthracen-9(10H)-one

Cas:5447-86-9

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

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Luhan Pharmachem Co., Lt

10-10-DIMETHYLANTHRONE (5447-86-9) Information The produce is Meritroxine intermediate. Quality Advanced technology Supper quality Effective & safety package

10,10-Dimethylanthrone,High purity

Cas:5447-86-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

10,10-Dimethylanthrone

Cas:5447-86-9

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

10,10-DIMETHYLANTHRONE

Cas:5447-86-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

10,10-Dimethylanthrone

Cas:5447-86-9

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

10,10-Dimethylanthrone

Cas:5447-86-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Lingrui Chemical Co.,Ltd.

Hot sale Top quality 5447-86-9 low price 10,10-Dimethylanthrone Molecular Formula C16H14O Molar Mass 222.28 Density 1.105±0.06 g/cm3(Predicted) Melting Point 101-103°C Boling Point

Hot sale Top quality 5447-86-9 low price 10,10-Dimethylanthrone

Cas:5447-86-9

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

Hefei Zhaobo Technology Co., Ltd.

Our Advantages Production: Advanced chemical equipment with years of experience.Staffs for producing various extract products. Quality Control:A complete set of Testing Professional and Analysis Equipment ensures the Quality Requirements and Speci

10,10-Dimethylanthrone CAS 5447-86-9

Cas:5447-86-9

Min.Order:1 Kilogram

FOB Price: $150.0 / 180.0

Type:Trading Company

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 10,10-Dimethylanthrone

Cas:5447-86-9

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

10,10-dimethylanthracen-9(10H)-one

Cas:5447-86-9

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

Siwei Development Group Ltd.

Product name: 10,10-Dimethylanthracen-9(10)-One CAS No.: 5447-86-9 Molecule Formula:C16H14O Molecule Weight:222.28 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard

Lower Price 10,10-Dimethylanthracen-9(10)-One

Cas:5447-86-9

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

10,10-Dimethylanthrone Manufacturer/High quality/Best price/In stock

Cas:5447-86-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

9,9-Dimethyl-10-(trimethylsilyl)-9,10-dihydroanthracene
136590-96-0

9,9-Dimethyl-10-(trimethylsilyl)-9,10-dihydroanthracene

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

Conditions
ConditionsYield
With sodium dichromate; acetic acid for 12h; Ambient temperature;90%
With sodium dichromate; acetic acid for 12h; Ambient temperature; other 9,9-dialkyl-10-(trimethylsilyl)- and 9,9-dialkyl-9,10-dihydroanthracenes;90%
9-diazo-10,10-dimethyl-9,10-dihydroanthracene
85199-64-0

9-diazo-10,10-dimethyl-9,10-dihydroanthracene

A

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

B

10-[10,10-dimethyl-9(10H)-anthracenyl]-9,10-dihydro-9,9-dimethylanthracene
85199-69-5

10-[10,10-dimethyl-9(10H)-anthracenyl]-9,10-dihydro-9,9-dimethylanthracene

Conditions
ConditionsYield
With (Z)-2-Butene Irradiation;A 8%
B 80%
9,10-Dihydro-10,10-dimethylanthracen
42332-94-5

9,10-Dihydro-10,10-dimethylanthracen

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

Conditions
ConditionsYield
With bromine In tetrachloromethane for 6h; Heating; Irradiation;70%
With chromium(VI) oxide In acetic acid
(8aR,9R)-8a,9-Dimethyl-8a,9-dihydro-anthracen-9-ol
80716-32-1

(8aR,9R)-8a,9-Dimethyl-8a,9-dihydro-anthracen-9-ol

A

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

B

9,10-Dihydro-10,10-dimethylanthracen
42332-94-5

9,10-Dihydro-10,10-dimethylanthracen

Conditions
ConditionsYield
With sulfuric acid; acetic anhydride In acetic acidA 25%
B 53%
9,9a-dihydro-9,9a-dimethyl-9-anthracenol
80716-32-1

9,9a-dihydro-9,9a-dimethyl-9-anthracenol

A

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

B

9,10-Dihydro-10,10-dimethylanthracen
42332-94-5

9,10-Dihydro-10,10-dimethylanthracen

Conditions
ConditionsYield
With sulfuric acid; acetic anhydride In acetic acid at 23℃; for 2.25h;A 25%
B 53%
acetic anhydride
108-24-7

acetic anhydride

9,9a-dihydro-9,9a-dimethyl-9-anthracenol
80716-32-1

9,9a-dihydro-9,9a-dimethyl-9-anthracenol

A

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

B

9,10-Dihydro-10,10-dimethylanthracen
42332-94-5

9,10-Dihydro-10,10-dimethylanthracen

C

10,10-dimethyl-9,10-dihydroanthranylacetic acid
80716-37-6

10,10-dimethyl-9,10-dihydroanthranylacetic acid

Conditions
ConditionsYield
With sulfuric acid for 2h; Yields of byproduct given;A n/a
B n/a
C 45%
dimethylketene
598-26-5

dimethylketene

N-(10,10-dimethyl-9,10-dihydroanthracen-9-ylidene)phenylamine N-oxide
101023-20-5

N-(10,10-dimethyl-9,10-dihydroanthracen-9-ylidene)phenylamine N-oxide

A

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

B

4',4',10,10-tetramethyl-3'-phenyl-9,10-dihydroanthracene-9-spiro-2'-oxazolidin-5'-one
101023-21-6

4',4',10,10-tetramethyl-3'-phenyl-9,10-dihydroanthracene-9-spiro-2'-oxazolidin-5'-one

Conditions
ConditionsYield
In ethyl acetate Ambient temperature;A 150 mg
B 24%
2-(1-hydroxy-1-methyl-ethyl)-benzophenone cyclohemiacetal
1023-91-2

2-(1-hydroxy-1-methyl-ethyl)-benzophenone cyclohemiacetal

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

Conditions
ConditionsYield
With sulfuric acid at 150℃; for 1.5h;20%
With PPA
With sulfuric acid at 150 - 155℃; for 5h;105 g
(8aR,9R)-8a,9-Dimethyl-8a,9-dihydro-anthracen-9-ol
80716-32-1

(8aR,9R)-8a,9-Dimethyl-8a,9-dihydro-anthracen-9-ol

A

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

B

9,10-Dihydro-10,10-dimethylanthracen
42332-94-5

9,10-Dihydro-10,10-dimethylanthracen

C

10,10-dimethyl-9,10-dihydroanthranylacetic acid
80716-37-6

10,10-dimethyl-9,10-dihydroanthranylacetic acid

Conditions
ConditionsYield
A 10%
B 15%
C 75 % Spectr.
anthracen-9(10H)-one
90-44-8

anthracen-9(10H)-one

methyl iodide
74-88-4

methyl iodide

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

Conditions
ConditionsYield
12%
With potassium hydroxide
(i) Li, MeOH, toluene, (ii) /BRN= 969135/, tBuOH; Multistep reaction;
With lithium methanolate 1) toluene, 100-120 deg C; 140 deg C 2) tBuOH, 24 h, 140-150 deg C; Yield given. Multistep reaction;
With sodium hydroxide In dichloromethane at 20℃; for 15h;100 % Spectr.
9-anthrol
529-86-2

9-anthrol

methyl iodide
74-88-4

methyl iodide

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

Conditions
ConditionsYield
Lithium-Verbindung;
With water; potassium carbonate
anthracen-9(10H)-one
90-44-8

anthracen-9(10H)-one

methyl iodide
74-88-4

methyl iodide

A

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

B

methyl-9-methoxy-10-anthracene
21992-33-6

methyl-9-methoxy-10-anthracene

Conditions
ConditionsYield
With potassium hydroxide
o-Isopropylbenzophenon-oxim
71104-02-4

o-Isopropylbenzophenon-oxim

chloroacetic acid
79-11-8

chloroacetic acid

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

Conditions
ConditionsYield
(i) NaOH, aq. EtOH, (ii) K2S2O8, aq. NaOH; Multistep reaction;
9,10-dihydro-10,10-dimethyl-9-anthracenol
18792-73-9

9,10-dihydro-10,10-dimethyl-9-anthracenol

A

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

B

9,10-Dihydro-10,10-dimethylanthracen
42332-94-5

9,10-Dihydro-10,10-dimethylanthracen

Conditions
ConditionsYield
With sulfuric acid In acetic acid for 3h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
methylene chloride
74-87-3

methylene chloride

10-nitro-9-methylanthracene
84457-22-7

10-nitro-9-methylanthracene

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

Conditions
ConditionsYield
Yield given. Multistep reaction;
9,10-dihydro-10,10-dimethyl-9-anthracenol
18792-73-9

9,10-dihydro-10,10-dimethyl-9-anthracenol

acetic anhydride
108-24-7

acetic anhydride

A

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

B

9,10-Dihydro-10,10-dimethylanthracen
42332-94-5

9,10-Dihydro-10,10-dimethylanthracen

C

10,10-dimethyl-9,10-dihydroanthranylacetic acid
80716-37-6

10,10-dimethyl-9,10-dihydroanthranylacetic acid

Conditions
ConditionsYield
With sulfuric acid for 2h; Yields of byproduct given;
anthracen-9(10H)-one
90-44-8

anthracen-9(10H)-one

methyl iodide
74-88-4

methyl iodide

A

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

B

methyl-9-methoxy-10-anthracene
21992-33-6

methyl-9-methoxy-10-anthracene

C

9-methoxyanthracene
2395-96-2

9-methoxyanthracene

D

9,10-phenanthrenequinone
84-65-1

9,10-phenanthrenequinone

Conditions
ConditionsYield
With potassium hydroxide; 18-crown-6 ether 1.) toluene, 70 deg C, 2.) toluene, 70 deg C, 3.5 h; r.t. 12 h; Yield given. Multistep reaction. Yields of byproduct given;
With potassium hydroxide; 18-crown-6 ether 1.) toluene, 70 deg C, 2.) toluene, 70 deg C, 3.5 h; r.t. 12 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
anthracen-9(10H)-one
90-44-8

anthracen-9(10H)-one

methanol. lithium methylate

methanol. lithium methylate

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

Conditions
ConditionsYield
With toluene Erhitzen des Reaktionsprodukts mit CH3I und wenig tert-Butylalkohol;
anthracen-9(10H)-one
90-44-8

anthracen-9(10H)-one

methyl iodide
74-88-4

methyl iodide

KOH-solution

KOH-solution

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

3,3-Dimethyl-3H-isobenzofuran-1-one
1689-09-4

3,3-Dimethyl-3H-isobenzofuran-1-one

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 83 percent / diethyl ether / 0 °C
2: 20 percent / H2SO4 / 1.5 h / 150 °C
View Scheme
Multi-step reaction with 2 steps
2: polyphosphoric acid
View Scheme
Multi-step reaction with 2 steps
1.1: magnesium; iodine / tetrahydrofuran / 2 h / Reflux
1.2: 5 h / 20 °C
2.1: sulfuric acid / 5 h / 150 - 155 °C
View Scheme
9a-hydro-9a-methyl-9-anthracenone
80716-28-5

9a-hydro-9a-methyl-9-anthracenone

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 71 percent / diethyl ether / 1.) -70 deg C -> 0 deg C, 1 h, 2.) 23 deg C, 1 h
2: 25 percent / conc. sulfuric acid, acetic anhydride / acetic acid / 2.25 h / 23 °C
View Scheme
Multi-step reaction with 2 steps
1: 71 percent
2: 25 percent / sulfuric acid, Ac2O / acetic acid
View Scheme
Multi-step reaction with 2 steps
1: 71 percent
2: 10 percent
View Scheme
C23H22N2O2S
85199-72-0

C23H22N2O2S

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 77 percent / sodium methoxide / pyridine / 70 °C
2: 8 percent / cis-2-butene / Irradiation
View Scheme
9-nitroanthracene
602-60-8

9-nitroanthracene

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

1,4,9a-trihydro-9a-methyl-9-anthracenone
80716-26-3

1,4,9a-trihydro-9a-methyl-9-anthracenone

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.)Bromine 2.)DBU / 2.)benzene
2: 71 percent
3: 25 percent / sulfuric acid, Ac2O / acetic acid
View Scheme
Multi-step reaction with 3 steps
1: 1.)Bromine 2.)DBU / 2.)benzene
2: 71 percent
3: 10 percent
View Scheme
Multi-step reaction with 4 steps
1: 55 percent / methylenetriphenylphosphorane
2: 1.)Bromine 2.)DBU / 2.)benzene
3: 71 percent
4: 25 percent / sulfuric acid, Ac2O / acetic acid
View Scheme
Multi-step reaction with 4 steps
1: 55 percent / methylenetriphenylphosphorane
2: 1.)Bromine 2.)DBU / 2.)benzene
3: 71 percent
4: 10 percent
View Scheme
1,2,9a-trihydro-9a-methyl-9-anthracenone
80716-27-4

1,2,9a-trihydro-9a-methyl-9-anthracenone

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.)Bromine 2.)DBU / 2.)benzene
2: 71 percent
3: 25 percent / sulfuric acid, Ac2O / acetic acid
View Scheme
Multi-step reaction with 3 steps
1: 1.)Bromine 2.)DBU / 2.)benzene
2: 71 percent
3: 10 percent
View Scheme
phthalic anhydride
85-44-9

phthalic anhydride

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: magnesium / tetrahydrofuran / 2 h / Reflux
1.2: 2 h / 20 °C
2.1: magnesium; iodine / tetrahydrofuran / 2 h / Reflux
2.2: 5 h / 20 °C
3.1: sulfuric acid / 5 h / 150 - 155 °C
View Scheme
Multi-step reaction with 3 steps
1.1: magnesium; iodine / tetrahydrofuran / 2 h / Reflux
1.2: 2 h / 20 °C
2.1: magnesium; iodine / tetrahydrofuran / 2 h / Reflux
2.2: 5 h / 20 °C
3.1: sulfuric acid / 5 h / 150 - 155 °C
View Scheme
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

3-(Dimethylamino)propyl chloride
109-54-6

3-(Dimethylamino)propyl chloride

C20H25NO

C20H25NO

Conditions
ConditionsYield
Stage #1: 3-(Dimethylamino)propyl chloride With iodine; magnesium In diethyl ether; ethylene dibromide at 30 - 35℃; for 9h; Reflux; Large scale;
Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In diethyl ether; ethylene dibromide at 10 - 35℃; for 1h; Reflux; Large scale;
97.2%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

10,10-dimethylanthrone hydrazone
90624-29-6

10,10-dimethylanthrone hydrazone

Conditions
ConditionsYield
With hydrazine hydrochloride; hydrazine hydrate In various solvent(s) Heating;95%
With hydrazinium sulfate; hydrazine Heating; Yield given;
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

9,10-Dibromoanthracene
523-27-3

9,10-Dibromoanthracene

10′-bromo-10,10-dimethyl-[9,9′-bianthracen]-9(10H)-ol

10′-bromo-10,10-dimethyl-[9,9′-bianthracen]-9(10H)-ol

Conditions
ConditionsYield
Stage #1: 9,10-Dibromoanthracene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Inert atmosphere;
Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran; hexane at 20℃; for 16h; Inert atmosphere;
93%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

(4-bromophenyl)magnesium bromide
18620-02-5

(4-bromophenyl)magnesium bromide

C22H19BrO

C22H19BrO

Conditions
ConditionsYield
In tetrahydrofuran at 60℃; for 24h; Grignard Reaction;88%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

1.4-dibromobenzene
106-37-6

1.4-dibromobenzene

C22H19BrO

C22H19BrO

Conditions
ConditionsYield
Stage #1: 1.4-dibromobenzene With magnesium In tetrahydrofuran for 4h; Inert atmosphere; Reflux;
Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at 60℃; for 24h;
88%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

9,10-Dihydro-10,10-dimethylanthracen
42332-94-5

9,10-Dihydro-10,10-dimethylanthracen

Conditions
ConditionsYield
With dimethylsulfide borane complex In tetrahydrofuran for 2h; Reflux;85%
With lithium aluminium tetrahydride; aluminium trichloride In diethyl ether for 0.333333h; Heating;27%
With potassium hydroxide; hydrazine hydrate In ethylene glycol
With hydrazine In diethylene glycol for 4h; Heating;
4-(4-bromophenyl)dibenzofuran
955959-84-9

4-(4-bromophenyl)dibenzofuran

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

C34H26O2

C34H26O2

Conditions
ConditionsYield
Stage #1: 4-(4-bromophenyl)dibenzofuran With magnesium In tetrahydrofuran for 4h; Inert atmosphere; Reflux;
Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at 60℃; for 24h; Inert atmosphere;
85%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

4-(2-bromo-4-chlorophenyl)dibenzofuran

4-(2-bromo-4-chlorophenyl)dibenzofuran

9-(5-chloro-2-(dibenzofuran-4-yl)phenyl)-10,10-dimethyl-9,10-dihydroanthracen-9-ol

9-(5-chloro-2-(dibenzofuran-4-yl)phenyl)-10,10-dimethyl-9,10-dihydroanthracen-9-ol

Conditions
ConditionsYield
Stage #1: 4-(2-bromo-4-chlorophenyl)dibenzofuran With n-butyllithium In tetrahydrofuran at -78℃; for 0.5h;
Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at -78 - 20℃; for 1h;
85%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

(4-(di([1,1’-biphenyl]-4-yl)amino)phenyl)boronic acid
943836-24-6

(4-(di([1,1’-biphenyl]-4-yl)amino)phenyl)boronic acid

C46H37N

C46H37N

Conditions
ConditionsYield
Stage #1: 10,10-dimethyl-9,10-dihydroanthracen-9-one With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h;
Stage #2: (4-(di([1,1’-biphenyl]-4-yl)amino)phenyl)boronic acid With potassium carbonate In toluene at 110℃; for 5h;
84%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

C44H39BN2O2

C44H39BN2O2

C60H52N2

C60H52N2

Conditions
ConditionsYield
Stage #1: 10,10-dimethyl-9,10-dihydroanthracen-9-one With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h;
Stage #2: C44H39BN2O2 With potassium carbonate In toluene at 110℃; for 5h;
84%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

C32H24BNO2

C32H24BNO2

C48H37N

C48H37N

Conditions
ConditionsYield
Stage #1: 10,10-dimethyl-9,10-dihydroanthracen-9-one With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h;
Stage #2: C32H24BNO2 With potassium carbonate In toluene at 110℃; for 5h;
83%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

2-bromo-10,10-dimethyl-10H-anthracen-9-one

2-bromo-10,10-dimethyl-10H-anthracen-9-one

Conditions
ConditionsYield
With N-Bromosuccinimide In N,N-dimethyl-formamide at 20℃; for 18h; Darkness;83%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

1-Bromo-5-chloronaphthalene
77332-65-1

1-Bromo-5-chloronaphthalene

C26H21ClO

C26H21ClO

Conditions
ConditionsYield
Stage #1: 1-Bromo-5-chloronaphthalene With n-butyllithium In tetrahydrofuran at -78 - 20℃; for 2h; Inert atmosphere;
Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at 0℃; for 10h; Inert atmosphere;
83%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

2-bromo-7-chloronaphthalene

2-bromo-7-chloronaphthalene

C26H21ClO

C26H21ClO

Conditions
ConditionsYield
Stage #1: 2-bromo-7-chloronaphthalene With n-butyllithium In tetrahydrofuran at -78 - 20℃; for 2h; Inert atmosphere;
Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at 20℃; for 10h; Inert atmosphere;
83%
2-(4-bromophenyl]pyridine
63996-36-1

2-(4-bromophenyl]pyridine

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

C27H23NO

C27H23NO

Conditions
ConditionsYield
Stage #1: 2-(4-bromophenyl]pyridine With magnesium In tetrahydrofuran for 4h; Inert atmosphere; Reflux;
Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at 60℃; for 24h; Inert atmosphere;
82%
bromobenzene
108-86-1

bromobenzene

10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

10,10-dimethyl-9-phenyl-9,10-dihydroanthracen-9-ol
39615-41-3

10,10-dimethyl-9-phenyl-9,10-dihydroanthracen-9-ol

Conditions
ConditionsYield
Stage #1: bromobenzene With n-butyllithium In tetrahydrofuran at -78 - 20℃; for 3.5h; Inert atmosphere;
Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at -78 - 20℃; for 16h;
82%
Stage #1: bromobenzene With iodine; magnesium In tetrahydrofuran at 40 - 80℃; for 4h; Inert atmosphere;
Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran for 15h; Inert atmosphere; Reflux;
76.8%
Stage #1: bromobenzene With iodine; magnesium In tetrahydrofuran at 40 - 80℃; for 4h; Inert atmosphere;
Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran for 15h; Inert atmosphere; Reflux;
76.3%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

1-bromo-4-chloronaphthalene
53220-82-9

1-bromo-4-chloronaphthalene

C26H21ClO

C26H21ClO

Conditions
ConditionsYield
Stage #1: 1-bromo-4-chloronaphthalene With n-butyllithium In tetrahydrofuran at -78 - 20℃; for 2h; Inert atmosphere;
Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at 20℃; for 10h; Inert atmosphere;
82%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

C27H25BN2O3

C27H25BN2O3

C43H38N2O

C43H38N2O

Conditions
ConditionsYield
Stage #1: 10,10-dimethyl-9,10-dihydroanthracen-9-one With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h;
Stage #2: C27H25BN2O3 With potassium carbonate In toluene at 110℃; for 5h;
81%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

C41H35BN2O2

C41H35BN2O2

C57H48N2

C57H48N2

Conditions
ConditionsYield
Stage #1: 10,10-dimethyl-9,10-dihydroanthracen-9-one With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h;
Stage #2: C41H35BN2O2 With potassium carbonate In toluene at 110℃; for 5h;
81%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

C16H12N2O5

C16H12N2O5

Conditions
ConditionsYield
With sulfuric acid; nitric acid at 5℃; for 0.5h;80%
With sulfuric acid; nitric acid at 5 - 10℃; for 0.5h;80%
With sulfuric acid; nitric acid at 5 - 10℃; for 0.5h;80%
With nitric acid at 5 - 10℃; for 0.5h;80%
With sulfuric acid; nitric acid at 5 - 10℃; for 0.5h;80%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

4-(diphenylamino)phenyl boronic acid
201802-67-7

4-(diphenylamino)phenyl boronic acid

C34H29N

C34H29N

Conditions
ConditionsYield
Stage #1: 10,10-dimethyl-9,10-dihydroanthracen-9-one With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h;
Stage #2: 4-(diphenylamino)phenyl boronic acid With potassium carbonate In toluene at 110℃; for 5h;
80%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

4-(di-naphthalene-2-yl-amino)-phenylboronic acid
1232102-18-9

4-(di-naphthalene-2-yl-amino)-phenylboronic acid

C42H33N

C42H33N

Conditions
ConditionsYield
Stage #1: 10,10-dimethyl-9,10-dihydroanthracen-9-one With toluene-4-sulfonic acid hydrazide In toluene at 80℃; for 2h;
Stage #2: 4-(di-naphthalene-2-yl-amino)-phenylboronic acid With potassium carbonate In toluene at 110℃; for 5h;
80%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

(2,6-dimethylphenyl)magnesium bromide
21450-64-6

(2,6-dimethylphenyl)magnesium bromide

9-(2,6-xylyl)-10,10-dimethyl-9,10-dihydroanthracen-9-ol

9-(2,6-xylyl)-10,10-dimethyl-9,10-dihydroanthracen-9-ol

Conditions
ConditionsYield
In tetrahydrofuran 1.) RT, 3 h, 2.) 80 deg C, 1 h;78%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

C12H8BrClO

C12H8BrClO

C28H21ClO

C28H21ClO

Conditions
ConditionsYield
Stage #1: C12H8BrClO With n-butyllithium In tetrahydrofuran at -78℃; for 0.5h;
Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran at -78 - 20℃; for 1h;
75.8%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

2-bromo-4-chloro-1-phenoxybenzene

2-bromo-4-chloro-1-phenoxybenzene

C28H21ClO

C28H21ClO

Conditions
ConditionsYield
Stage #1: 2-bromo-4-chloro-1-phenoxybenzene With n-butyllithium In tetrahydrofuran at -78℃; for 0.166667h;
Stage #2: 10,10-dimethyl-9,10-dihydroanthracen-9-one In tetrahydrofuran
Stage #3: With sulfuric acid; acetic acid Reflux;
75.58%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

N,N-dimethylethylenediamine
108-00-9

N,N-dimethylethylenediamine

N'-(10,10-Dimethyl-10H-anthracen-9-ylidene)-N,N-dimethyl-ethane-1,2-diamine
76596-08-2

N'-(10,10-Dimethyl-10H-anthracen-9-ylidene)-N,N-dimethyl-ethane-1,2-diamine

Conditions
ConditionsYield
With N,N,N,N,N,N-hexamethylphosphoric triamide; titanium tetrachloride In benzene for 144h; Ambient temperature;69%
10,10-dimethyl-9,10-dihydroanthracen-9-one
5447-86-9

10,10-dimethyl-9,10-dihydroanthracen-9-one

C16H15(2)HO

C16H15(2)HO

Conditions
ConditionsYield
With water-d2; magnesium; ethylene dibromide In tetrahydrofuran at 70℃; for 2h; Inert atmosphere; Schlenk technique;69%
With water-d2; magnesium; ethylene dibromide In tetrahydrofuran69%

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