CAS No.55021-77-7,4-(Methylthio)-1-butylamine Suppliers

GIHI CHEMICALS CO.,LIMITED

Product Name:4-(METHYLTHIO)-1-BUTYLAMINE CAS No.: 55021-77-7 Chemical formula: C5H13NS Molecular weight:119.23 Item Standard Appearance white powder Identification H-

4-(METHYLTHIO)-1-BUTYLAMINE

Cas:55021-77-7

Min.Order:1 Kilogram

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

4-(Methylthio)-1-butylamine

Cas:55021-77-7

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Antimex Chemical Limied

hight degree of purity Application:Fine chemical intermediates, used as the main raw material for he synthesis of various pesticides, medicines, surfactants, polymer monomers, Ond Ontifungal agents

4-(Methylthio)-1-butylamine

Cas:55021-77-7

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Hangzhou Fandachem Co.,Ltd

4-(METHYLTHIO)-1-BUTYLAMINEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

4-(METHYLTHIO)-1-BUTYLAMINE

Cas:55021-77-7

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Finetech Industry Limited

FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 4-(Methylthio)-1-butylamine, CAS:55021-77-7 with the most competitive price and the b

4-(Methylthio)-1-butylamine

Cas:55021-77-7

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Debye Scientific

Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen

4-(Methylthio)-1-butylamine

Cas:55021-77-7

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Xiamen Xindano Biotechnology Co., Ltd.

Provide R & D and production from gram class to ton class, customized chemicals and process development according to customer needs Package:1KG；100KG;100G Application:Pharmaceutical Intermediate

4-(METHYLTHIO)-1-BUTYLAMINE

Cas:55021-77-7

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Type:Lab/Research institutions

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yuyongmei

YUYONGMEI was established in Aug,1999, located in the industrial park of Nanjing University of Technology, It is a private enterprises in Jiangsu Province with 1200 square meters’ R&D center. Our R&D center has a well-equipped synthetic laboratory a

4-(Methylthio)-1-butylamine

Cas:55021-77-7

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Type:Trading Company

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Medical Isotopes, Inc.

4-(Methylthio)-1-butylamine

Cas:55021-77-7

Min.Order:0

Negotiable

Type:Trading Company

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Synthetic route

: 59121-24-3
4-(methylthio)butyronitrile

: 55021-77-7
4-(methylthio)-1-butylamine

Conditions

Conditions	Yield
With lithium aluminium tetrahydride In diethyl ether for 0.5h; Reflux;	93%
With borane In tetrahydrofuran at 20℃;	63%
With ethanol; sodium

: 52096-68-1
2-<2-(Methylthio)butyl>-1H-isoindole-1,3(2H)-dione

: 55021-77-7
4-(methylthio)-1-butylamine

Conditions

Conditions	Yield
With hydrazine hydrate In ethanol for 5h; Reflux;	83.2%
With hydrazine In ethanol for 3h; Heating / reflux;	80%
With hydrazine hydrate In ethanol for 3h; Reflux;	80%

: 57775-01-6
1-azido-(4-methylsulfenyl)butane

: 55021-77-7
4-(methylthio)-1-butylamine

Conditions

Conditions	Yield
With lithium aluminium tetrahydride	54%

: 64-17-5
ethanol

: 59121-24-3
4-(methylthio)butyronitrile

sodium: sodium

: 55021-77-7
4-(methylthio)-1-butylamine

...Expand

: 27160-24-3
ω-chloro-1-methylsulfanylbutane

: 55021-77-7
4-(methylthio)-1-butylamine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: tetrabutylammomium bromide / toluene / 18 h / 0 - 20 °C 2: hydrazine hydrate / ethanol / 5 h / Reflux View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: 84104-30-3
(+/-)-1-amino-4-(methylsulfinyl)butane

Conditions

Conditions	Yield
With dihydrogen peroxide In 2,2,2-trifluoroethanol at 0 - 20℃; for 1.33333h; Inert atmosphere;	90%
With sulfuric acid; dihydrogen peroxide; isopropyl alcohol In methanol at 20℃; for 2h;	64%
With sulfuric acid; dihydrogen peroxide In methanol; water; isopropyl alcohol at 20℃; for 3h;	63%
With dihydrogen peroxide; acetone

: 55021-77-7
4-(methylthio)-1-butylamine

: 4430-36-8
erucin

: 1,3-bis(4-(methylthio)-butyl)thiourea

Conditions

Conditions	Yield
In dichloromethane for 2h; Reflux;	89%

: 463-71-8
thiophosgene

: 55021-77-7
4-(methylthio)-1-butylamine

: 4430-36-8
erucin

Conditions

Conditions	Yield
With sodium hydroxide In dichloromethane at 0 - 20℃; for 3h;	86.5%
With sodium hydroxide In dichloromethane at 0 - 20℃; for 3.5h;	84%
With sodium hydroxide In dichloromethane at 0 - 20℃; for 3.5h; Inert atmosphere;	84%

: 55021-77-7
4-(methylthio)-1-butylamine

: 552838-69-4
4-methanesulfonyl-butylamine

Conditions

Conditions	Yield
With potassium permanganate

: 55021-77-7
4-(methylthio)-1-butylamine

: 103-72-0
phenyl isothiocyanate

: 100317-76-8
1-benzyl-3-(4-(methylthio)butyl)thiourea

: 75-15-0
carbon disulfide

: 55021-77-7
4-(methylthio)-1-butylamine

: 4430-36-8
erucin

Conditions

Conditions	Yield
Yield given. Multistep reaction;
Stage #1: carbon disulfide; 4-(methylthio)-1-butylamine With triethylamine In tetrahydrofuran at 0 - 20℃; Stage #2: With methanesulfonyl chloride In tetrahydrofuran at 0 - 20℃; for 0.5h;

: 55021-77-7
4-(methylthio)-1-butylamine

CS2: CS2

: 4430-36-8
erucin

Conditions

Conditions	Yield
With ethanol Oxydation des Reaktionsprodukts mit 0.5 Mol Jod in Aethanol, Einwirkung von Natriumaethylat-Loesung und erneute Oxydation mit 0.5 Mol Jod in Aethanol bei 0grad;

: 55021-77-7
4-(methylthio)-1-butylamine

CS2: CS2

: 1,3-bis(4-(methylthio)-butyl)thiourea

: 55021-77-7
4-(methylthio)-1-butylamine

: 4478-93-7
D,L-sulforaphane

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 12.5 mmol / sodium hydroxide / CHCl3 2: 100 percent / m-chloroperbenzoic acid / CH2Cl2 / 0.5 h View Scheme
Multi-step reaction with 2 steps 1: 64 percent / aq. H2O2; H2SO4; i-PrOH / methanol / 2 h / 20 °C 2: 57 percent / aq. NaOH / CHCl3 / 0.58 h View Scheme
Multi-step reaction with 2 steps 1: sulfuric acid; dihydrogen peroxide / methanol; water; isopropyl alcohol / 3 h / 20 °C 2: sodium hydroxide / chloroform / 1 h / 20 °C View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: N-acetyl-S-{N-[4-(methylthio)butyl]thiocarbamoyl}-L-cysteine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 12.5 mmol / sodium hydroxide / CHCl3 2: 7.1 mmol / sodium hydrogen carbonate / ethanol; H2O View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: N-acetyl-S-{N-[4-(methylsulfinyl)butyl]thiocarbamoyl}-L-cysteine

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 12.5 mmol / sodium hydroxide / CHCl3 2: 100 percent / m-chloroperbenzoic acid / CH2Cl2 / 0.5 h 3: 69.5 percent / sodium hydrogen carbonate / ethanol; H2O View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: 142825-10-3
R-sulforaphane

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 2: aq. ethanol / 48 h / 27 °C / Helminthosporium species NRRL 4671 View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: 155320-20-0
(S)-Sulforaphane

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 2: aq. ethanol / 48 h / 27 °C / Helminthosporium species NRRL 4671 View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: 7431-78-9
(4-methylsulfanyl-butyl)-thiourea

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: ethanol / Oxydation des Reaktionsprodukts mit 0.5 Mol Jod in Aethanol, Einwirkung von Natriumaethylat-Loesung und erneute Oxydation mit 0.5 Mol Jod in Aethanol bei 0grad 2: ethanol; NH3 View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: N,N'-bis-(4-methylsulfanyl-butyl)-urea

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: ethanol / Oxydation des Reaktionsprodukts mit 0.5 Mol Jod in Aethanol, Einwirkung von Natriumaethylat-Loesung und erneute Oxydation mit 0.5 Mol Jod in Aethanol bei 0grad 2: Ag2O; aqueous dioxane / 70 °C View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: 504-84-7
erysolin

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: KMnO4 2: alcohol / laesst auf das Reaktionsprodukt Jod einwirken, versetzt mit Natriumaethylatloesung und behandelt mit Jod View Scheme
Multi-step reaction with 3 steps 1.1: dihydrogen peroxide / 2,2,2-trifluoroethanol / 1.33 h / 0 - 20 °C / Inert atmosphere 2.1: triethylamine / ethanol / 0.5 h / 20 °C / Inert atmosphere 2.2: 2.25 h / 0 - 20 °C 3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / -20 - 20 °C / Inert atmosphere View Scheme
Multi-step reaction with 2 steps 1: sodium hydroxide / dichloromethane / 3.5 h / 0 - 20 °C / Inert atmosphere 2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / Inert atmosphere View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: N,N'-bis-(4-methanesulfonyl-butyl)-thiourea

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: KMnO4 View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: (4-methanesulfonyl-butyl)-trimethyl-ammonium; iodide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: KMnO4 2: sodium methylate View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: 100801-39-6
N-benzyl-N'-(4-methylsulfanyl-butyl)-thiourea

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: chloroform; aqueous NaOH-solution View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: 1356472-68-8
N-(4-(methylsulfonyl)butyl)morpholine-4-carbothioamide

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1.1: dihydrogen peroxide / 2,2,2-trifluoroethanol / 1.33 h / 0 - 20 °C / Inert atmosphere 2.1: triethylamine / ethanol / 0.5 h / 20 °C / Inert atmosphere 2.2: 2.25 h / 0 - 20 °C 3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / -20 - 20 °C / Inert atmosphere 4.1: dichloromethane / 1 h / Reflux View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: 1356472-67-7
O-ethyl 4-(methylsulfinyl)butylcarbamothioate

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: dihydrogen peroxide / 2,2,2-trifluoroethanol / 1.33 h / 0 - 20 °C / Inert atmosphere 2.1: triethylamine / ethanol / 0.5 h / 20 °C / Inert atmosphere 2.2: 2.25 h / 0 - 20 °C 3.1: Reflux; Inert atmosphere View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: 1356346-97-8
1-(4-(methylsulfinyl)butyl)-3-(5-oxohexyl)thiourea

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: dihydrogen peroxide / 2,2,2-trifluoroethanol / 1.33 h / 0 - 20 °C / Inert atmosphere 2: dichloromethane / 3 h / Reflux View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: N,N’-di-(4-methylsulfinylbutyl)thiourea

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: dihydrogen peroxide / 2,2,2-trifluoroethanol / 1.33 h / 0 - 20 °C / Inert atmosphere 2: dichloromethane / 1 h / Reflux View Scheme
Multi-step reaction with 3 steps 1.1: dihydrogen peroxide / 2,2,2-trifluoroethanol / 1.33 h / 0 - 20 °C / Inert atmosphere 2.1: triethylamine / ethanol / 0.5 h / 20 °C / Inert atmosphere 2.2: 2.25 h / 0 - 20 °C 3.1: dichloromethane / 1 h / Reflux View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: 1350914-98-5
N-(4-(methylsulfinyl)butyl)piperidine-1-carbothioamide

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: dihydrogen peroxide / 2,2,2-trifluoroethanol / 1.33 h / 0 - 20 °C / Inert atmosphere 2.1: triethylamine / ethanol / 0.5 h / 20 °C / Inert atmosphere 2.2: 2.25 h / 0 - 20 °C 3.1: dichloromethane / 1 h / Reflux View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: 1356472-66-6
4-methyl-N-(4-(methylsulfinyl)-butyl)piperazine-1-carbothioamide

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: dihydrogen peroxide / 2,2,2-trifluoroethanol / 1.33 h / 0 - 20 °C / Inert atmosphere 2.1: triethylamine / ethanol / 0.5 h / 20 °C / Inert atmosphere 2.2: 2.25 h / 0 - 20 °C 3.1: dichloromethane / 1 h / Reflux View Scheme

: 55021-77-7
4-(methylthio)-1-butylamine

: 1356346-82-1
N-(4-(methylsulfinyl)butyl)-morpholine-4-carbothioamide

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: dihydrogen peroxide / 2,2,2-trifluoroethanol / 1.33 h / 0 - 20 °C / Inert atmosphere 2.1: triethylamine / ethanol / 0.5 h / 20 °C / Inert atmosphere 2.2: 2.25 h / 0 - 20 °C 3.1: dichloromethane / 1 h / Reflux View Scheme

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