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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Sanguinarium chloride Manufacturer/High quality/Best price/In stock

Cas:5578-73-4

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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shanghai Tauto Biotech Co., Ltd

17-year experience in Phytochemicals Each product has passed very strict tests (NMR\MS\HPLC) Agents in 13 countries Certified by ISO 9001:2008 quality management system Leader Supplier of Botanical Reference Materials in China

Sanguinarium chloride

Cas:5578-73-4

Min.Order:10 Milligram

Negotiable

Type:Manufacturers

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Content Natural Extract Sanguinarine chloride HACCP manufacturer

Cas:5578-73-4

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Shanghai Seasonsgreen Chemical Co.,Ltd

Shanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu

lower price High quality SANGUINARINE CHLORIDE

Cas:5578-73-4

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Manufacturers

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 5578-73-4 with competitive price

Cas:5578-73-4

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Sanguinarine chloride

Cas:5578-73-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Chengdu Biopurify Phytochemicals Ltd.

Chengdu Biopurify Phytochemicals Ltd. is a leading company in the research, development, manufacture and marketing of High Quality Phytochemicals and Extracts(especially Active Ingredients from Traditional Chinese Medicine,Traditional Chinese Medic

Sanguinarium chloride

Cas:5578-73-4

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Nanjing Spring & Autumn Biological Engineering Co., Ltd.

Nanjing Spring & Autumn Biological Engineering Co., Ltd. Which was founded at 2008, has an R & D team composed very experienced natural products chemists. The company is a high-tech enterprise engaged in functional health care products raw ma

SANGUINARINE CHLORIDE

Cas:5578-73-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

[1,3]Benzodioxolo[5,6-c]-1,3-dioxolo[4,5-i]phenanthridinium,13-methyl-, chloride (1:1)

Cas:5578-73-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shaanxi Cuicheng Biomedical Technology Co., Ltd.

Why Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu

SANGUINARINE CHLORIDE

Cas:5578-73-4

Min.Order:1 Gram

Negotiable

Type:Other

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Henan Wentao Chemical Product Co., Ltd.

1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea

Sanguinarium chlorideCAS NO.: 5578-73-4

Cas:5578-73-4

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

SanguinarineChloride

Cas:5578-73-4

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Hubei CuiRan Biotechnology Co., Ltd

Hubei CuiRan Biotechnology Co., Ltd is a leading company in the research, development, manufacture and marketing of High Quality Phytochemicals and Extracts(especially Active Ingredients from Traditional Chinese Medicine,Traditional Chinese Medicine)

Sanguinarine chloride

Cas:5578-73-4

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

[1,3]Benzodioxolo[5,6-c]-1,3-dioxolo[4,5-i]phenanthridinium,13-methyl-, chloride (1:1)

Cas:5578-73-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Sinoway Industrial Co., Ltd.

Why is SINOWAY:1) Specialized in pharmaceutical and healthcare industrial since 19872) ISO 9001:2015 & SGS audited supplier . 3) Accept various payment terms : T.T 30-60 days.4) We have warehouse in USA with quickly shipment . Application:Herbal extr

Hangzhou Dingyan Chem Co., Ltd

high purity, manufacturer Application:Intermediate

Sanguinarine Hydrochloride

Cas:5578-73-4

Min.Order:0

Negotiable

Type:Manufacturers

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Shanghai Acmec Biochemical Technology Co., Ltd.

Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea

Acmec Sanguinarine (chloride) 20mg

Cas:5578-73-4

Min.Order:1 bottle

Negotiable

Type:Lab/Research institutions

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Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

SANGUINARINE CHLORIDE

Cas:5578-73-4

Min.Order:0

Negotiable

Type:Manufacturers

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Chengdu Lemeitian Pharmaceutical Technology Co,. Ltd

1.High quality and competetive price1)We are manufacturer with own lab and factory, can provide high quality products with factory price. 2)Products purity is test by our quality department strictly before sending, and you can also ask the third test

Sanguinarine chloride CAS No:5578-73-4

Cas:5578-73-4

Min.Order:0

Negotiable

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

best price high quality Storage:Room Temperature Application:For pharmacy chemicals Transportation:by sea, air

SANGUINARINE CHLORIDE

Cas:5578-73-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Antimex Chemical Limied

Our own factory produces direct sales with absolute price advantage Application:Pharmaceutical industry Transportation:By sea Port:Shanghai/tianjin

Phosphoric acid,lanthanum(3+) sodium salt (2:1:3) (9CI)

Cas:5578-73-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Guangdong Juda Chemical Industrial Co.,Limited

Appearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China

SANGUINARINE CHLORIDE CAS No.5578-73-4

Cas:5578-73-4

Min.Order:0

Negotiable

Type:Trading Company

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Hangzhou Fandachem Co.,Ltd

Sanguinarium chloride cas 5578-73-4Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

Sanguinarium chloride cas 5578-73-4

Cas:5578-73-4

Min.Order:0

Negotiable

Type:Other

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DB BIOTECH CO., LTD

SANGUINARINE CHLORIDEAppearance:fine powder Storage:cool, dry place and avoid strongl light Package:1kg/bag, 25kg/drum Application:health supplement Transportation:DHL,TNT,FEDEX,EMS, by air, by sea

SANGUINARINE CHLORIDE

Cas:5578-73-4

Min.Order:0

Negotiable

Type:Trading Company

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Asure Biochem CO.,LTD.

*stable and better quality products*efficient and meticulous servicesAppearance:Powder Storage:Store in dry, cool and ventilated place Package:1kg/tin 5kg/tin 25kg/carton Application:Use in healthcare products. Use in food products. Use in Cosmetic p

Sanguinarium chloride

Cas:5578-73-4

Min.Order:0

Negotiable

Type:Trading Company

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BOC Sciences

BOC Sciences provides a wide range of research chemicals and biochemicals including inhibitors, building blocks, GMP Products, impurities and metabolites, APIs for Veterinary, Natural Compounds, ADCs, Stem Cell Molecule and chiral compounds.Appearanc

Sanguinarine chloride hydrate

Cas:5578-73-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai Yuanye Bio-Technology Co., Ltd.

good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:20mg Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by express or by sea Port:Any por

Sanguinarine chloride

Cas:5578-73-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

SANGUINARINE CHLORIDE

Cas:5578-73-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

LEAP CHEM Co., Ltd.

Best Seller, High Quality, Competitive Price, Fast Delivery, Quick ResponseAppearance:powder, or liquid Storage:Stored in room temperature, ventilated place Package:Bottle, barrel, cargo, container, etc. Application:Pharmaceuticals, intermediates, AP

SANGUINARINE CHLORIDE

Cas:5578-73-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

HENAN SUNLAKE ENTERPRISE CORPORATION

HENAN SUNLAKE ENTERPRISE CORPORATION Our company advantages: 1、The highest quality with the competitive price. 2、Professional human services. 3、The fastest and safest delivery service. 4、The faster and safest delivery service. 5、The hig

SANGUINARINE CHLORIDE

Cas:5578-73-4

Min.Order:1 Gram

Negotiable

Type:Trading Company

inquiry

Synthetic route

oxysanguinarine
548-30-1

oxysanguinarine

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Stage #1: oxysanguinarine With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; for 0.333333h; Inert atmosphere;
Stage #2: With hydrogenchloride In water at 20℃;
98%
dihydrosanguinarine
3606-45-9

dihydrosanguinarine

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
With hydrogenchloride; sodium hydroxide; jones reagent In acetone at 0℃; for 0.5h;85.4%
With sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone In benzene
With sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone In water; benzene for 1h; Ambient temperature;2.1 g
Stage #1: dihydrosanguinarine With 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide In toluene at 20℃; for 2h;
Stage #2: With hydrogenchloride
Stage #1: dihydrosanguinarine With 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide In water; toluene at 20℃; for 1h;
Stage #2: With hydrogenchloride In chloroform; water at 0℃;
sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
With hydrogenchloride; palladium on activated charcoal; maleic acid In water; acetic acid47%
norsanguinarine
522-30-5

norsanguinarine

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
(methylation);
Multi-step reaction with 2 steps
1.1: sodium tetrahydroborate / 40 °C
2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide / toluene; water / 1 h / 20 °C
2.2: 0 °C
View Scheme
sanguinarine hydrosulfate

sanguinarine hydrosulfate

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
With hydrogenchloride In water Heating;
dihydrosanguinarine

dihydrosanguinarine

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
With iron(III) chloride
O-acetyl-chelidonine

O-acetyl-chelidonine

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
With mercury(II) diacetate
(+)-chelidonine

(+)-chelidonine

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 9.8 g / pyridine / 6 h / Ambient temperature
2: HgO / acetic acid / 4 h / Heating
3: 2.1 g / 2,3-dichloro-5,6-dicyano-p-benzoquinone, 5percent NaOH / benzene; H2O / 1 h / Ambient temperature
View Scheme
(+)-chelidonine acetate

(+)-chelidonine acetate

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: HgO / acetic acid / 4 h / Heating
2: 2.1 g / 2,3-dichloro-5,6-dicyano-p-benzoquinone, 5percent NaOH / benzene; H2O / 1 h / Ambient temperature
View Scheme
13-methyl-6,7,13,14-tetrahydro-[1,3]dioxolo[4,5-i][1,3]dioxolo[4',5':4,5]benzo[1,2-c]phenanthridine
22855-17-0

13-methyl-6,7,13,14-tetrahydro-[1,3]dioxolo[4,5-i][1,3]dioxolo[4',5':4,5]benzo[1,2-c]phenanthridine

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Pd-C
2: DDQ, aq. NaOH / benzene
View Scheme
8-hydroxydihydosanguinarine
4070-41-1

8-hydroxydihydosanguinarine

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Acidic aq. solution;
methyl 5-iodobenzo[d][1,3]dioxole-4-carboxylate
33842-29-4

methyl 5-iodobenzo[d][1,3]dioxole-4-carboxylate

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: bis-triphenylphosphine-palladium(II) chloride; triethylamine; zinc(II) chloride; zinc / tetrahydrofuran / 24 h / 60 °C / Inert atmosphere
2.1: potassium hydroxide / aacetone / 2 h / Reflux; Inert atmosphere
3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene / 2 h / Inert atmosphere; Reflux
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere
4.2: 20 °C
View Scheme
C8H4ClIO3

C8H4ClIO3

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: 0.5 h / Inert atmosphere
2.1: bis-triphenylphosphine-palladium(II) chloride; triethylamine; zinc(II) chloride; zinc / tetrahydrofuran / 24 h / 60 °C / Inert atmosphere
3.1: potassium hydroxide / aacetone / 2 h / Reflux; Inert atmosphere
4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene / 2 h / Inert atmosphere; Reflux
5.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere
5.2: 20 °C
View Scheme
7,8-methylenedioxy-13,14-cis-dihydrobenzodioxolebenzo[c]phenanthridin-6-one

7,8-methylenedioxy-13,14-cis-dihydrobenzodioxolebenzo[c]phenanthridin-6-one

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: potassium hydroxide / aacetone / 2 h / Reflux; Inert atmosphere
2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene / 2 h / Inert atmosphere; Reflux
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere
3.2: 20 °C
View Scheme
C20H15NO5

C20H15NO5

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene / 2 h / Inert atmosphere; Reflux
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere
2.2: 20 °C
View Scheme
5-iodobenzo[d][1,3]dioxole-4-carboxylic acid
1309123-33-8

5-iodobenzo[d][1,3]dioxole-4-carboxylic acid

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / Inert atmosphere
2.1: 0.5 h / Inert atmosphere
3.1: bis-triphenylphosphine-palladium(II) chloride; triethylamine; zinc(II) chloride; zinc / tetrahydrofuran / 24 h / 60 °C / Inert atmosphere
4.1: potassium hydroxide / aacetone / 2 h / Reflux; Inert atmosphere
5.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene / 2 h / Inert atmosphere; Reflux
6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere
6.2: 20 °C
View Scheme
5-iodobenzo[d][1,3]dioxole-4-carbaldehyde
249636-72-4

5-iodobenzo[d][1,3]dioxole-4-carbaldehyde

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1.1: dihydrogen peroxide; potassium hydroxide / methanol; water / 0.5 h / 65 °C / Inert atmosphere
2.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / Inert atmosphere
3.1: 0.5 h / Inert atmosphere
4.1: bis-triphenylphosphine-palladium(II) chloride; triethylamine; zinc(II) chloride; zinc / tetrahydrofuran / 24 h / 60 °C / Inert atmosphere
5.1: potassium hydroxide / aacetone / 2 h / Reflux; Inert atmosphere
6.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene / 2 h / Inert atmosphere; Reflux
7.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere
7.2: 20 °C
View Scheme
sanguinarine acetate
55438-13-6

sanguinarine acetate

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Stage #1: sanguinarine acetate With potassium hydroxide In water
Stage #2: With hydrogenchloride In water
7-methyl-5H-indeno[5,6-d][1,3]dioxole

7-methyl-5H-indeno[5,6-d][1,3]dioxole

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 18 h
2: IO4(1-)*Na(1+)*O2Si / dichloromethane / 1 h / Inert atmosphere
3: zinc(II) chloride / diethyl ether; 1,2-dichloro-ethane / 36 h / 55 °C / Inert atmosphere; Microwave irradiation
4: 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 5 h / 100 °C / Inert atmosphere; Schlenk technique
5: sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / 20 °C
View Scheme
Multi-step reaction with 5 steps
1: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 18 h
2: IO4(1-)*Na(1+)*O2Si / dichloromethane / 1 h / Inert atmosphere
3: zinc(II) chloride / dichloromethane; diethyl ether / 18 h / 55 °C / Inert atmosphere; Microwave irradiation
4: 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 5 h / 100 °C / Inert atmosphere; Schlenk technique
5: sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / 20 °C
View Scheme
5,6-methylenedioxy-1-indanone
6412-87-9

5,6-methylenedioxy-1-indanone

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1.1: cerium(III) chloride / tetrahydrofuran / 0.08 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: toluene-4-sulfonic acid / dichloromethane / 0.5 h / Inert atmosphere
3.1: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 18 h
4.1: IO4(1-)*Na(1+)*O2Si / dichloromethane / 1 h / Inert atmosphere
5.1: zinc(II) chloride / dichloromethane; diethyl ether / 18 h / 55 °C / Inert atmosphere; Microwave irradiation
6.1: 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 5 h / 100 °C / Inert atmosphere; Schlenk technique
7.1: sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / 20 °C
View Scheme
Multi-step reaction with 7 steps
1.1: cerium(III) chloride / tetrahydrofuran / 0.08 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: toluene-4-sulfonic acid / dichloromethane / 0.5 h / Inert atmosphere
3.1: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 18 h
4.1: IO4(1-)*Na(1+)*O2Si / dichloromethane / 1 h / Inert atmosphere
5.1: zinc(II) chloride / diethyl ether; 1,2-dichloro-ethane / 36 h / 55 °C / Inert atmosphere; Microwave irradiation
6.1: 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 5 h / 100 °C / Inert atmosphere; Schlenk technique
7.1: sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / 20 °C
View Scheme
2-(6-acetylbenzo[d][1,3]dioxol-5-yl)acetaldehyde

2-(6-acetylbenzo[d][1,3]dioxol-5-yl)acetaldehyde

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: zinc(II) chloride / dichloromethane; diethyl ether / 18 h / 55 °C / Inert atmosphere; Microwave irradiation
2: 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 5 h / 100 °C / Inert atmosphere; Schlenk technique
3: sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1: zinc(II) chloride / diethyl ether; 1,2-dichloro-ethane / 36 h / 55 °C / Inert atmosphere; Microwave irradiation
2: 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 5 h / 100 °C / Inert atmosphere; Schlenk technique
3: sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / 20 °C
View Scheme
5-bromo-benzo[1,3]dioxole-4-carbaldehyde
72744-54-8

5-bromo-benzo[1,3]dioxole-4-carbaldehyde

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: methanol / 3 h / 20 °C / Inert atmosphere
2: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C
3: zinc(II) chloride / dichloromethane; diethyl ether / 18 h / 55 °C / Inert atmosphere; Microwave irradiation
4: 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 5 h / 100 °C / Inert atmosphere; Schlenk technique
5: sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / 20 °C
View Scheme
Multi-step reaction with 5 steps
1: methanol / 3 h / 20 °C / Inert atmosphere
2: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C
3: zinc(II) chloride / diethyl ether; 1,2-dichloro-ethane / 36 h / 55 °C / Inert atmosphere; Microwave irradiation
4: 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 5 h / 100 °C / Inert atmosphere; Schlenk technique
5: sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / 20 °C
View Scheme
Multi-step reaction with 6 steps
1.1: sodium tetrahydroborate; methanol / 0.5 h / 0 °C
2.1: pyridine; phosphorus tribromide / dichloromethane / 1 h / 0 - 20 °C
3.1: potassium carbonate / N,N-dimethyl-formamide / 110 °C
4.1: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 16 h / 90 - 110 °C / Inert atmosphere
5.1: sodium tetrahydroborate / 40 °C
6.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide / toluene; water / 1 h / 20 °C
6.2: 0 °C
View Scheme
1-(5-bromobenzo[d][1,3]dioxol-4-yl)-N-methylmethanamine

1-(5-bromobenzo[d][1,3]dioxol-4-yl)-N-methylmethanamine

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: zinc(II) chloride / dichloromethane; diethyl ether / 18 h / 55 °C / Inert atmosphere; Microwave irradiation
2: 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 5 h / 100 °C / Inert atmosphere; Schlenk technique
3: sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1: zinc(II) chloride / diethyl ether; 1,2-dichloro-ethane / 36 h / 55 °C / Inert atmosphere; Microwave irradiation
2: 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 5 h / 100 °C / Inert atmosphere; Schlenk technique
3: sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / 20 °C
View Scheme
C9H8BrNO2
1207666-53-2

C9H8BrNO2

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C
2: zinc(II) chloride / dichloromethane; diethyl ether / 18 h / 55 °C / Inert atmosphere; Microwave irradiation
3: 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 5 h / 100 °C / Inert atmosphere; Schlenk technique
4: sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / 20 °C
View Scheme
Multi-step reaction with 4 steps
1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C
2: zinc(II) chloride / diethyl ether; 1,2-dichloro-ethane / 36 h / 55 °C / Inert atmosphere; Microwave irradiation
3: 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 5 h / 100 °C / Inert atmosphere; Schlenk technique
4: sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / 20 °C
View Scheme
N-((5-bromobenzo[d][1,3]dioxol-4-yl)methyl)-N-methylnaphtho[2,3-d][1,3]dioxol-5-amine

N-((5-bromobenzo[d][1,3]dioxol-4-yl)methyl)-N-methylnaphtho[2,3-d][1,3]dioxol-5-amine

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 5 h / 100 °C / Inert atmosphere; Schlenk technique
2: sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / 20 °C
View Scheme
C11H12O3

C11H12O3

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: toluene-4-sulfonic acid / dichloromethane / 0.5 h / Inert atmosphere
2: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 18 h
3: IO4(1-)*Na(1+)*O2Si / dichloromethane / 1 h / Inert atmosphere
4: zinc(II) chloride / diethyl ether; 1,2-dichloro-ethane / 36 h / 55 °C / Inert atmosphere; Microwave irradiation
5: 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 5 h / 100 °C / Inert atmosphere; Schlenk technique
6: sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / 20 °C
View Scheme
Multi-step reaction with 6 steps
1: toluene-4-sulfonic acid / dichloromethane / 0.5 h / Inert atmosphere
2: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 18 h
3: IO4(1-)*Na(1+)*O2Si / dichloromethane / 1 h / Inert atmosphere
4: zinc(II) chloride / dichloromethane; diethyl ether / 18 h / 55 °C / Inert atmosphere; Microwave irradiation
5: 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 5 h / 100 °C / Inert atmosphere; Schlenk technique
6: sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / 20 °C
View Scheme
7-methyl-5H-indeno[5,6-d][1,3]dioxole

7-methyl-5H-indeno[5,6-d][1,3]dioxole

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: IO4(1-)*Na(1+)*O2Si / dichloromethane / 1 h / Inert atmosphere
2: zinc(II) chloride / dichloromethane; diethyl ether / 18 h / 55 °C / Inert atmosphere; Microwave irradiation
3: 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 5 h / 100 °C / Inert atmosphere; Schlenk technique
4: sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / 20 °C
View Scheme
Multi-step reaction with 4 steps
1: IO4(1-)*Na(1+)*O2Si / dichloromethane / 1 h / Inert atmosphere
2: zinc(II) chloride / diethyl ether; 1,2-dichloro-ethane / 36 h / 55 °C / Inert atmosphere; Microwave irradiation
3: 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 5 h / 100 °C / Inert atmosphere; Schlenk technique
4: sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / 20 °C
View Scheme
2,3-methylenedioxy-5-nitronaphthalene
142886-75-7

2,3-methylenedioxy-5-nitronaphthalene

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C / 760.05 Torr
2.1: potassium carbonate / N,N-dimethyl-formamide / 110 °C
3.1: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 16 h / 90 - 110 °C / Inert atmosphere
4.1: sodium tetrahydroborate / 40 °C
5.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide / toluene; water / 1 h / 20 °C
5.2: 0 °C
View Scheme
naphtho[2,3-d][1,3]dioxol-5-amine
53811-49-7

naphtho[2,3-d][1,3]dioxol-5-amine

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 110 °C
2.1: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 16 h / 90 - 110 °C / Inert atmosphere
3.1: sodium tetrahydroborate / 40 °C
4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide / toluene; water / 1 h / 20 °C
4.2: 0 °C
View Scheme
N-(6'-bromo-2',3'-methylenedioxybenzyl)-6,7-methylenedioxy-1-naphthylamine
93666-99-0

N-(6'-bromo-2',3'-methylenedioxybenzyl)-6,7-methylenedioxy-1-naphthylamine

sanguinarine chloride
5578-73-4

sanguinarine chloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 16 h / 90 - 110 °C / Inert atmosphere
2.1: sodium tetrahydroborate / 40 °C
3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide / toluene; water / 1 h / 20 °C
3.2: 0 °C
View Scheme
sanguinarine chloride
5578-73-4

sanguinarine chloride

butan-1-ol
71-36-3

butan-1-ol

6-butoxy-5,6-dihydrosanguinarine
49702-43-4

6-butoxy-5,6-dihydrosanguinarine

Conditions
ConditionsYield
With copper(II) chloride dihydrate; oxygen at 80℃; for 10h;99%
With sodium carbonate In water
propan-1-ol
71-23-8

propan-1-ol

sanguinarine chloride
5578-73-4

sanguinarine chloride

13-methyl-14-propoxy-13,14-dihydro-[1,3]dioxolo[4,5-i][1,3]dioxolo[4',5':4,5]benzo[1,2-c]phenanthridine
49702-42-3

13-methyl-14-propoxy-13,14-dihydro-[1,3]dioxolo[4,5-i][1,3]dioxolo[4',5':4,5]benzo[1,2-c]phenanthridine

Conditions
ConditionsYield
With copper(II) chloride dihydrate; oxygen at 80℃; for 10h;99%
sanguinarine chloride
5578-73-4

sanguinarine chloride

isopropyl alcohol
67-63-0

isopropyl alcohol

Conditions
ConditionsYield
With copper(II) chloride dihydrate; oxygen at 80℃; for 10h;98%
ethanol
64-17-5

ethanol

sanguinarine chloride
5578-73-4

sanguinarine chloride

6-Ethoxy-5,6-dihydrosanguinarine
28342-31-6

6-Ethoxy-5,6-dihydrosanguinarine

Conditions
ConditionsYield
With copper(II) chloride dihydrate; oxygen at 80℃; for 10h;97%
methanol
67-56-1

methanol

sanguinarine chloride
5578-73-4

sanguinarine chloride

6-methoxy-5,6-dihydrosanguinarine
72401-54-8, 88544-84-7

6-methoxy-5,6-dihydrosanguinarine

Conditions
ConditionsYield
With copper(II) chloride dihydrate; oxygen at 80℃; for 10h;96%
potassium cyanide

potassium cyanide

sanguinarine chloride
5578-73-4

sanguinarine chloride

sanguinarine φ-cyanide
23701-59-9

sanguinarine φ-cyanide

Conditions
ConditionsYield
In water at 60℃; for 0.5h;83%
trimethylsilyl cyanide
7677-24-9

trimethylsilyl cyanide

sanguinarine chloride
5578-73-4

sanguinarine chloride

sanguinarine φ-cyanide
23701-59-9

sanguinarine φ-cyanide

Conditions
ConditionsYield
With cesium fluoride In acetonitrile at 20℃;59%
sanguinarine chloride
5578-73-4

sanguinarine chloride

dihydrosanguinarine
3606-45-9

dihydrosanguinarine

Conditions
ConditionsYield
With methanol; sodium tetrahydroborate at 20℃; for 0.5h; Darkness;55%
With sodium tetrahydroborate In methanol at 20℃; for 0.5h;36%
With 1,4-dihydronicotinamide adenine dinucleotide In water at 25℃; Rate constant; Kinetics; Thermodynamic data; other coenzyme, var. pH, ΔH(excit.), ΔS(excit.);
With sodium tetrahydroborate In methanol
sodium methylate
124-41-4

sodium methylate

sanguinarine chloride
5578-73-4

sanguinarine chloride

6-methoxy-5,6-dihydrosanguinarine
72401-54-8, 88544-84-7

6-methoxy-5,6-dihydrosanguinarine

Conditions
ConditionsYield
In methanol for 6h; pH=10; Reflux;51%
sanguinarine chloride
5578-73-4

sanguinarine chloride

9H-carbazole
86-74-8

9H-carbazole

6-(carbazol-1-yl)-5,6-dihydrosanguinarine
1452540-22-5

6-(carbazol-1-yl)-5,6-dihydrosanguinarine

Conditions
ConditionsYield
Stage #1: 9H-carbazole With sodium hydride In tetrahydrofuran Inert atmosphere; Sonication;
Stage #2: sanguinarine chloride In tetrahydrofuran at 20℃;
45%
sanguinarine chloride
5578-73-4

sanguinarine chloride

oxysanguinarine
548-30-1

oxysanguinarine

Conditions
ConditionsYield
With hydrogenchloride; potassium hydroxide; potassium hexacyanoferrate(III) In water at 90℃; for 3h;43%
With sodium hydroxide
methylmagnesium bromide
75-16-1

methylmagnesium bromide

sanguinarine chloride
5578-73-4

sanguinarine chloride

C21H17NO4

C21H17NO4

Conditions
ConditionsYield
In tetrahydrofuran at 0 - 20℃; for 10h;29%
indole
120-72-9

indole

sanguinarine chloride
5578-73-4

sanguinarine chloride

14-(1H-indol-3-yl)-13-methyl-13,14-dihydro[1,3]dioxolo[4',5':4,5]benzo[1,2-c][1,3]dioxolo[4,5-i]phenanthridine

14-(1H-indol-3-yl)-13-methyl-13,14-dihydro[1,3]dioxolo[4',5':4,5]benzo[1,2-c][1,3]dioxolo[4,5-i]phenanthridine

Conditions
ConditionsYield
With triethylamine In acetonitrile for 10h; Reflux;17.4%
potassium cyanide
151-50-8

potassium cyanide

sanguinarine chloride
5578-73-4

sanguinarine chloride

sanguinarine φ-cyanide
23701-59-9

sanguinarine φ-cyanide

Conditions
ConditionsYield
With water
sanguinarine chloride
5578-73-4

sanguinarine chloride

benzyl alcohol
100-51-6

benzyl alcohol

norsanguinarine
522-30-5

norsanguinarine

sanguinarine chloride
5578-73-4

sanguinarine chloride

8-hydroxydihydosanguinarine
4070-41-1

8-hydroxydihydosanguinarine

Conditions
ConditionsYield
With sodium hydroxide
With potassium hydroxide
sanguinarine chloride
5578-73-4

sanguinarine chloride

acetone
67-64-1

acetone

(+/-)-6-acetonyldihydrosanguinarine
37687-34-6, 88588-10-7

(+/-)-6-acetonyldihydrosanguinarine

Conditions
ConditionsYield
With sodium carbonate Heating;
sanguinarine chloride
5578-73-4

sanguinarine chloride

norsanguinarine
522-30-5

norsanguinarine

Conditions
ConditionsYield
at 207℃; for 0.116667h;
sanguinarine chloride
5578-73-4

sanguinarine chloride

bis<6-(5,6-dihydrosanguinarinyl)> ether

bis<6-(5,6-dihydrosanguinarinyl)> ether

Conditions
ConditionsYield
With sodium carbonate In water
sanguinarine chloride
5578-73-4

sanguinarine chloride

C20H12(2)H3NO4

C20H12(2)H3NO4

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 0.12 h / 207 °C
2: 1.3 g / NaBH4 / hexamethylphosphoric acid triamide / 2 h / 50 °C
View Scheme

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