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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 2-Bromo-1-Cyclohexylethanone supplier in China

Cas:56077-28-2

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine c

2-Bromo-1-cyclohexylethanone

Cas:56077-28-2

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

Ethanone, 2-bromo-1-cyclohexyl- (9CI)

Cas:56077-28-2

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

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Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

Ethanone, 2-bromo-1-cyclohexyl- (9CI) 56077-28-2

Cas:56077-28-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

2-Bromo-1-Cyclohexylethanone

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Ethanone,2-bromo-1-cyclohexyl-

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

Ethanone, 2-bromo-1-cyclohexyl- (9CI)

Cas:56077-28-2

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

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Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

2-Bromo-1-cyclohexyl-ethanone cas no. 56077-28-2 98%

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

2-bromo-1-cyclohexylethanone

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Other

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GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier

2-Bromo-1-cyclohexylethanone

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

2-broMo-1-cyclohexylethan-1-one

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

2-Bromo-1-Cyclohexylethanone

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Shanghai Finebiotech Co.,Ltd.

Shanghai Finebiotech Co.,Ltd.was established in 2020, which providing professional chemical services. As a customer-oriented company, we have distinguished ourself from others in providing worldwide customers with cost-effective and efficient service

2-BroMo-1-cyclohexylethanone

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

2-Bromo-1-cyclohexylethanone

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

2-BroMo-1-cyclohexylethanone

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Ocean Chemical Co., Ltd.

★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support

2-Bromo-1-cyclohexylethanone

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fandachem Co.,Ltd

2-Bromo-1-cyclohexylethanone cas 56077-28-2Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

2-Bromo-1-cyclohexylethanone cas 56077-28-2

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Other

inquiry

Asure Biochem CO.,LTD.

*stable and better quality products*efficient and meticulous servicesAppearance:Powder Storage:Store in dry, cool and ventilated place Package:10G/bottle 1kg/tin 5kg/tin 25kg/carton Application:1. Chemical raw materials 2. Used as an analytical reage

2-Bromo-1-cyclohexylethanone

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

2-Bromo-1-cyclohexylethanone 56077-28-2

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

Ethanone, 2-bromo-1-cyclohexyl- (9CI)

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Suzhou Sibian Chemical Technology Co., Ltd

Lower price, sample is available,large stock in warehouse.Best service, high quality and reasonable price.If you are looking for the material's manufacturer or supplier in China, Sibian chemical is your best choice. Application:Drug R&D

2-Bromo-1-cyclohexylethan-1-one

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

LEAP CHEM Co., Ltd.

Best Seller, High Quality, Competitive Price, Fast Delivery, Quick ResponseAppearance:powder, or liquid Storage:Stored in room temperature, ventilated place Package:Bottle, barrel, cargo, container, etc. Application:Pharmaceuticals, intermediates, AP

2-Bromo-1-cyclohexylethanone

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

2-Bromo-1-cyclohexylethanone

Cas:56077-28-2

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

HENAN SUNLAKE ENTERPRISE CORPORATION

56077-28-2 C8H13BrO Ethanone, 2-bromo-1-cyclohexyl- (9CI)

Cas:56077-28-2

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

suzhou BetterBioChem Co., Ltd.

Betterbiochem is specialized in APIs, pharmaceutical intermediates & fine chemicals. 1. The best quality, competitive price. 2. The best service before or after shipment. 3. Rich experience in export operation. 4. Rich experience in

2-BROMO-1-CYCLOHEXYLETHANONE

Cas:56077-28-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen BaiFuchem Co.,Ltd

BaiFuChem is a Professional chemical raw material supplier in China, our main products include Biochemical , Pharma Intermediate and Organic chemical etc. BaiFuChem have wealth of products,experience , expertise and state-of-the-art

Hot Sale 2-Bromo-1-Cyclohexylethanone

Cas:56077-28-2

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Nanjing Chemlin Chemical Co., Ltd.

Compound sourcing ServicesAgency of testing serviceFactory audit serviceFounded in Dec. 1999, Nanjing Chemlin Chemical Industrial Co.,Ltd(CHEMLIN) has been covering the business scope from trading of chemicals to custom-synthesis & Manufacturing. Co

56077-28-2

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Yinghao Pharm Co.,Ltd.

Yinghao Pharm products include: leader molecule, heterocyclic compounds,chiral compounds, photoelectric materials, biochemical reagents etc. For example:benzene, pyrimidine, boricacid,pyridine, pyrazole, imidazole, pyrrole, fluorine and other derivat

Ethanone, 2-broMo-1-cyclohexyl- (9CI)

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

ORCHID CHEMICAL SUPPLIES LTD

2-Bromo-1-Cyclohexylethanone supplierAppearance:Colorless to Brown Sticky Liquid Storage:Keep away of light,cool place Package:25kg/drum;200kg/drum Application:Pharma Intermediate Transportation:Sea/air/courier

2-Bromo-1-Cyclohexylethanone

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Other

inquiry

Wuhan MoonZY Biological Technology Co.,Ltd

instock with good quality and wholesale price Storage:Keep in a cool & dry place Package:Packing material and QTY as your request Application:Pharma;Industry;other application Transportation:Express or as your request Port:Any port of China

Ethanone, 2-bromo-1-cyclohexyl- (9CI),56077-28-2

Cas:56077-28-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

Cyclohexyl methyl ketone
823-76-7

Cyclohexyl methyl ketone

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

Conditions
ConditionsYield
With bromine100%
With bromine In methanol for 2h; Cooling with ice;100%
With PhCH2N(CH3)3Br3 In dichloromethane at 5 - 20℃; for 4h;98%
chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

Cyclohexyl methyl ketone
823-76-7

Cyclohexyl methyl ketone

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

Conditions
ConditionsYield
Stage #1: Cyclohexyl methyl ketone With lithium diisopropyl amide In tetrahydrofuran; n-heptane; ethylbenzene at -78℃; for 1h;
Stage #2: chloro-trimethyl-silane In tetrahydrofuran; n-heptane; ethylbenzene at -78℃; for 3.5h;
Stage #3: With N-Bromosuccinimide; sodium hydrogencarbonate In tetrahydrofuran at 0 - 20℃; for 1.17h;
100%
dimethyltitanocene
1271-66-5

dimethyltitanocene

N,N-dimethylcyclohexanecarboxamide
17566-51-7

N,N-dimethylcyclohexanecarboxamide

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

Conditions
ConditionsYield
Stage #1: dimethyltitanocene; N,N-dimethylcyclohexanecarboxamide In toluene at 65℃; Schlenk technique; Inert atmosphere;
Stage #2: With bromine In toluene at -78℃; for 0.0333333h; Schlenk technique; Inert atmosphere;
Stage #3: With water In toluene at 20℃; for 1h; Schlenk technique; Inert atmosphere; regioselective reaction;
94%
(bromoethynyl)cyclohexane
66684-39-7

(bromoethynyl)cyclohexane

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

Conditions
ConditionsYield
With water; copper(II) acetate monohydrate; trifluoroacetic acid at 70℃; for 6h; chemoselective reaction;90%
With cerium(IV) sulphate; sulfuric acid; water In dichloromethane at 80℃; for 12h; Sealed tube; regioselective reaction;88%
With 2-(dicyclohexylphosphino)-2',4',6'-triisopropylbiphenyl Au bis(trifluoromethylsulfonyl)imide; water In 1,2-dichloro-ethane at 20℃; for 14h;87%
With water In 1,2-dichloro-ethane at 20℃; for 14h;85%
With indium(III) triflate; water In acetic acid at 100℃; Sealed tube;84%
2-cyclohexylacetylene
931-48-6

2-cyclohexylacetylene

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

Conditions
ConditionsYield
With N,N'-ethylenethiourea; 1,3-dibromo-5,5-dimethylhydantoin; water In acetone at 45℃;80%
Multi-step reaction with 2 steps
1: N-Bromosuccinimide; silver nitrate / acetone / 20 °C
2: water; 2-(dicyclohexylphosphino)-2',4',6'-triisopropylbiphenyl Au bis(trifluoromethylsulfonyl)imide / 1,2-dichloro-ethane / 14 h / 20 °C
View Scheme
2-cyclohexyl-1-diazo-2-ethanone
31151-40-3

2-cyclohexyl-1-diazo-2-ethanone

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

Conditions
ConditionsYield
With hydrogen bromide In hexane; water at 20℃; for 2h;78%
With ferric(III) bromide; silica gel In dichloromethane at 20℃; for 0.166667h;63%
With water; hydrogen bromide
cyclohexanylcarbonyl chloride
2719-27-9

cyclohexanylcarbonyl chloride

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

Conditions
ConditionsYield
(i) Et2O, (ii) HBr; Multistep reaction;
cyclohexylbromoacetylene

cyclohexylbromoacetylene

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

Conditions
ConditionsYield
With sulfuric acid; mercury(II) sulfate
sulfuric acid
7664-93-9

sulfuric acid

(bromoethynyl)cyclohexane
66684-39-7

(bromoethynyl)cyclohexane

mercury(II) sulfate

mercury(II) sulfate

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: tetrahydrofuran; cyclohexane / 2 h / 0 °C
1.2: 50 percent / TMSCl; aq. HCl / tetrahydrofuran; cyclohexane / 0.5 h
2.1: 70 percent / Br2 / methanol / 3 h / 0 - 15 °C
View Scheme
Multi-step reaction with 2 steps
1.1: tetrahydrofuran / 2 h / 0 °C
1.2: 50 percent / TMSCl; aq. HCl / tetrahydrofuran / 0.5 h
2.1: Br2 / methanol / 3 h / below 15 deg C
2.2: 70 percent / H2O / methanol / 15 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1.1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 2.33 h / 0 - 20 °C
2.1: dichloromethane; tetrahydrofuran / 20 °C / Cooling with ice
3.1: toluene / 65 °C / Schlenk technique; Inert atmosphere
3.2: 0.03 h / -78 °C / Schlenk technique; Inert atmosphere
3.3: 1 h / 20 °C / Schlenk technique; Inert atmosphere
View Scheme
cyclohexanoyl bromide
10500-30-8

cyclohexanoyl bromide

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
2: water; HBr
View Scheme
cyclohexanylcarbonyl chloride
2719-27-9

cyclohexanylcarbonyl chloride

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: tetrahydrofuran; diethyl ether; acetonitrile / 0 - 20 °C / Inert atmosphere
2: hydrogen bromide / hexane; water / 2 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1.1: dichloromethane; tetrahydrofuran / 20 °C / Cooling with ice
2.1: toluene / 65 °C / Schlenk technique; Inert atmosphere
2.2: 0.03 h / -78 °C / Schlenk technique; Inert atmosphere
2.3: 1 h / 20 °C / Schlenk technique; Inert atmosphere
View Scheme
cyclohexanylcarbonyl chloride
2719-27-9

cyclohexanylcarbonyl chloride

diazomethyl-trimethyl-silane
18107-18-1

diazomethyl-trimethyl-silane

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

Conditions
ConditionsYield
Stage #1: cyclohexanylcarbonyl chloride; diazomethyl-trimethyl-silane
Stage #2: With hydrogen bromide
(1-Cyclohexyl-aethyl)-benzyl-aether
92729-26-5

(1-Cyclohexyl-aethyl)-benzyl-aether

A

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

B

1-(1-bromocyclohexyl)ethan-1-one
56077-27-1

1-(1-bromocyclohexyl)ethan-1-one

Conditions
ConditionsYield
With hydrogen bromide; oxygen; sodium nitrite In water; acetonitrile at 0 - 60℃; under 760.051 Torr; for 24.5h; Overall yield = 89%;
vinylcyclohexane
695-12-5

vinylcyclohexane

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

Conditions
ConditionsYield
With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; water at 60℃; for 2h;
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

sodium triazole
41253-21-8

sodium triazole

C10H15N3O
111229-33-5

C10H15N3O

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 5℃;91%
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

thioacetamide
62-55-5

thioacetamide

4-cyclohexyl-2-methyl-thiazole
100133-05-9

4-cyclohexyl-2-methyl-thiazole

Conditions
ConditionsYield
at 130℃; for 2.5h; Neat (no solvent);89%
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

4-(R,S)-(4-cyanophenyl)-4-methyl-2,5-dioxoimidazolidine
169808-00-8

4-(R,S)-(4-cyanophenyl)-4-methyl-2,5-dioxoimidazolidine

4-(1-(2-cyclohexyl-2-oxoethyl)-4-methyl-2,5-dioxoimidazolidin-4-yl)benzonitrile

4-(1-(2-cyclohexyl-2-oxoethyl)-4-methyl-2,5-dioxoimidazolidin-4-yl)benzonitrile

Conditions
ConditionsYield
Stage #1: 4-(R,S)-(4-cyanophenyl)-4-methyl-2,5-dioxoimidazolidine With potassium carbonate
Stage #2: Bromomethyl cyclohexyl ketone at 20℃;
89%
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

1-(2-iodophenyl)-N-methylmethanamine
113258-86-9

1-(2-iodophenyl)-N-methylmethanamine

1-Cyclohexyl-2-[(2-iodo-benzyl)-methyl-amino]-ethanone
140420-20-8

1-Cyclohexyl-2-[(2-iodo-benzyl)-methyl-amino]-ethanone

Conditions
ConditionsYield
In 1,4-dioxane for 4h; Ambient temperature;88%
N-(5-(p-toluenesulfonyl)pyrrolo[2,3-b]pyrazin-2-yl)carbamic acid tert-butyl ester
1201187-44-1

N-(5-(p-toluenesulfonyl)pyrrolo[2,3-b]pyrazin-2-yl)carbamic acid tert-butyl ester

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

tert-butyl 2-cyclohexyl-2-oxoethyl-(5-tosyl-5H-pyrrolo[2,3-b]pyrazin-2-yl)carbamate
1201187-50-9

tert-butyl 2-cyclohexyl-2-oxoethyl-(5-tosyl-5H-pyrrolo[2,3-b]pyrazin-2-yl)carbamate

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide at 0℃; for 1h;83%
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

4-amino-5-(2,4,5,6-tetrahydrocyclopenta[c]pyrazol-3-yl)-4H-1,2,4-triazole-3-thiol

4-amino-5-(2,4,5,6-tetrahydrocyclopenta[c]pyrazol-3-yl)-4H-1,2,4-triazole-3-thiol

6-cyclohexyl-3-(2,4,5,6-tetrahydrocyclopenta[c]pyrazol-3-yl)-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazine

6-cyclohexyl-3-(2,4,5,6-tetrahydrocyclopenta[c]pyrazol-3-yl)-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazine

Conditions
ConditionsYield
In ethanol at 95℃; for 1.5h; Inert atmosphere; Microwave irradiation; Sealed tube;83%
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

2-Allyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
72824-04-5

2-Allyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

(S)-1-bromo-2-cyclohexylpent-4-en-2-ol

(S)-1-bromo-2-cyclohexylpent-4-en-2-ol

Conditions
ConditionsYield
With methanol; (S)-2-((2-hydroxy-3-(triphenylsilyl)benzyl)amino)-3-methyl-1-(pyrrolidin-1-yl)butan-1-one; zinc dimethoxide In toluene at 22℃; for 4h; Inert atmosphere; enantioselective reaction;81%
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

(3RS)-3-benzyloxycarbonylamino-2,3-dihydro-5,9-dimethyl-1H-1,4-benzodiazepin-2-one
205993-40-4

(3RS)-3-benzyloxycarbonylamino-2,3-dihydro-5,9-dimethyl-1H-1,4-benzodiazepin-2-one

N-(3RS)-3-benzyloxycarbonylamino-1-cyclohexylcarbonylmethyl-2,3-dihydro-5,9-dimethyl-1H-1,4-benzodiazepin-2-one
205992-81-0

N-(3RS)-3-benzyloxycarbonylamino-1-cyclohexylcarbonylmethyl-2,3-dihydro-5,9-dimethyl-1H-1,4-benzodiazepin-2-one

Conditions
ConditionsYield
Stage #1: (3RS)-3-benzyloxycarbonylamino-2,3-dihydro-5,9-dimethyl-1H-1,4-benzodiazepin-2-one With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 4h; deprotonation;
Stage #2: Bromomethyl cyclohexyl ketone In N,N-dimethyl-formamide at 20℃; for 5.5h; Alkylation;
80.4%
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

4-amino-5-(5-phenyl-2H-pyrazol-3-yl)-4H-[1,2,4]triazole-3-thiol
366007-57-0

4-amino-5-(5-phenyl-2H-pyrazol-3-yl)-4H-[1,2,4]triazole-3-thiol

6-cyclohexyl-3-(3-phenyl-1H-pyrazol-5-yl)-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazine

6-cyclohexyl-3-(3-phenyl-1H-pyrazol-5-yl)-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazine

Conditions
ConditionsYield
In ethanol at 95℃; for 1.5h; Inert atmosphere; Microwave irradiation; Sealed tube;79%
6-chloro-pyridazin-3-ylamine
5469-69-2

6-chloro-pyridazin-3-ylamine

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

6-chloro-2-cyclohexylimidazo<1,2-b>pyridazine
144449-20-7

6-chloro-2-cyclohexylimidazo<1,2-b>pyridazine

Conditions
ConditionsYield
With sodium hydrogencarbonate In ethanol Heating;78%
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

1-cyclohexyl-2-fluoroethan-1-one
768-04-7

1-cyclohexyl-2-fluoroethan-1-one

Conditions
ConditionsYield
With potassium fluoride; 18-crown-6 ether In benzene at 80℃; for 24h;78%
2-aminopyridine
504-29-0

2-aminopyridine

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

2-cyclohexylimidazo[1,2-a]pyridine
1557840-36-4

2-cyclohexylimidazo[1,2-a]pyridine

Conditions
ConditionsYield
In water at 20℃; for 8h; Green chemistry;78%
ethyl 7-hydroxy-4-methyl-2-oxo-2H-chromene-3-carboxylate

ethyl 7-hydroxy-4-methyl-2-oxo-2H-chromene-3-carboxylate

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

ethyl 7-(2-cyclohexyl-2-oxoethoxy)-4-methyl-2-oxo-2H-chromene-3-carboxylate

ethyl 7-(2-cyclohexyl-2-oxoethoxy)-4-methyl-2-oxo-2H-chromene-3-carboxylate

Conditions
ConditionsYield
Stage #1: ethyl 7-hydroxy-4-methyl-2-oxo-2H-chromene-3-carboxylate With potassium carbonate; potassium iodide In 1,4-dioxane for 0.0833333h;
Stage #2: Bromomethyl cyclohexyl ketone In 1,4-dioxane at 100℃; for 24h;
78%
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

(3RS)-3-benzyloxycarbonylamino-2,3-dihydro-5-isobutyl-9-methyl-1H-1,4-benzodiazepin-2-one
205996-00-5

(3RS)-3-benzyloxycarbonylamino-2,3-dihydro-5-isobutyl-9-methyl-1H-1,4-benzodiazepin-2-one

(3RS)-3-benzyloxycarbonylamino-1-cyclohexyl-carbonylmethyl-2,3-dihydro-5-isobutyl-9-methyl-1H-1,4-benzodiazepin-2-one
205998-75-0

(3RS)-3-benzyloxycarbonylamino-1-cyclohexyl-carbonylmethyl-2,3-dihydro-5-isobutyl-9-methyl-1H-1,4-benzodiazepin-2-one

Conditions
ConditionsYield
Stage #1: (3RS)-3-benzyloxycarbonylamino-2,3-dihydro-5-isobutyl-9-methyl-1H-1,4-benzodiazepin-2-one With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 4h; deprotonation;
Stage #2: Bromomethyl cyclohexyl ketone In N,N-dimethyl-formamide at 20℃; for 5.5h; Alkylation;
77.8%
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

vinyl magnesium bromide
1826-67-1

vinyl magnesium bromide

1-bromo-2-cyclohexyl-3-buten-2-ol
1418143-59-5

1-bromo-2-cyclohexyl-3-buten-2-ol

Conditions
ConditionsYield
In tetrahydrofuran at -78℃; for 2.5h; Inert atmosphere;76%
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

(2-aminophenyl)(phenyl)methanone
2835-77-0

(2-aminophenyl)(phenyl)methanone

3-bromo-2-cyclohexyl-4-phenylquinoline
1312213-28-7

3-bromo-2-cyclohexyl-4-phenylquinoline

Conditions
ConditionsYield
Stage #1: Bromomethyl cyclohexyl ketone; (2-aminophenyl)(phenyl)methanone With trimethylsilyl bromide In N,N-dimethyl-formamide at 0℃; Fridlaender reaction; Heating; Sealed;
Stage #2: With water In N,N-dimethyl-formamide at 20℃; for 1h; Fridlaender reaction; Sonication;
73%
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

triphenylphosphine
603-35-0

triphenylphosphine

1-cyclohexyl-2-(triphenyl-λ5-phosphanylidene)ethan-1-one
17615-02-0

1-cyclohexyl-2-(triphenyl-λ5-phosphanylidene)ethan-1-one

Conditions
ConditionsYield
In toluene at 23℃; for 17h; Inert atmosphere;73%
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

5-tosyloxyphenyl 2-methylpyridyl sulfone
133804-17-8

5-tosyloxyphenyl 2-methylpyridyl sulfone

2-Cyclohexyl-1-(4-tosyloxybenzenesulphonyl)indolizine
114432-29-0

2-Cyclohexyl-1-(4-tosyloxybenzenesulphonyl)indolizine

Conditions
ConditionsYield
With potassium carbonate In butanone for 2h; Heating;71%
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

(3RS)-3-benzyloxycarbonylamino-5-cyclopropyl-2,3-dihydro-9-methyl-1H-1,4-benzodiazepin-2-one
205995-94-4

(3RS)-3-benzyloxycarbonylamino-5-cyclopropyl-2,3-dihydro-9-methyl-1H-1,4-benzodiazepin-2-one

(3RS)-3-benzyloxycarbonylamino-1-cyclohexyl-carbonylmethyl-2,3-dihydro-5-cyclopropyl-9-methyl-1H-1,4-benzodiazepin-2-one
205997-11-1

(3RS)-3-benzyloxycarbonylamino-1-cyclohexyl-carbonylmethyl-2,3-dihydro-5-cyclopropyl-9-methyl-1H-1,4-benzodiazepin-2-one

Conditions
ConditionsYield
Stage #1: (3RS)-3-benzyloxycarbonylamino-5-cyclopropyl-2,3-dihydro-9-methyl-1H-1,4-benzodiazepin-2-one With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 4h; deprotonation;
Stage #2: Bromomethyl cyclohexyl ketone In N,N-dimethyl-formamide at 20℃; for 5.5h; Alkylation;
70.8%
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

4-(4-methyl-2,5-dioxoimidazolidin-4-yl)benzenesulfonamide

4-(4-methyl-2,5-dioxoimidazolidin-4-yl)benzenesulfonamide

4-(1-(2-cyclohexyl-2-oxoethyl)-4-methyl-2,5-dioxoimidazolidin-4-yl)benzenesulfonamide

4-(1-(2-cyclohexyl-2-oxoethyl)-4-methyl-2,5-dioxoimidazolidin-4-yl)benzenesulfonamide

Conditions
ConditionsYield
Stage #1: 4-(4-methyl-2,5-dioxoimidazolidin-4-yl)benzenesulfonamide With potassium carbonate
Stage #2: Bromomethyl cyclohexyl ketone at 20℃;
69%
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

(S)-2-cyclohexyloxirane
3483-39-4, 97859-93-3, 61393-19-9

(S)-2-cyclohexyloxirane

Conditions
ConditionsYield
With dimethylsulfide borane complex; (3a'S)-3',3'-diphenylhexahydrospiro[[1,3,2]dioxaborolane-2,1'-pyrrolo[1,2-c][1,3,2]oxazaborol]-7'-ium-6-uide In tetrahydrofuran at 0℃; for 80h; Inert atmosphere;68%
Multi-step reaction with 2 steps
1: 2-[(1,3,2-dioxaborolan-2-yloxy)diphenylmethyl]pyrrolidine; dimethylsulfide borane complex / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
2: sodium hydroxide / tetrahydrofuran; water / 2 h
View Scheme
2-Amino-4-methylpyridine
695-34-1

2-Amino-4-methylpyridine

Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

2-cyclohexyl-7-methylimidazo[1,2-a]pyridine

2-cyclohexyl-7-methylimidazo[1,2-a]pyridine

Conditions
ConditionsYield
In water at 20℃; for 8h; Green chemistry;67%
Bromomethyl cyclohexyl ketone
56077-28-2

Bromomethyl cyclohexyl ketone

(3RS)-3-benzyloxycarbonylamino-2,3-dihydro-5-isopropyl-9-methyl-1H-1,4-benzodiazepin-2-one
205993-09-5

(3RS)-3-benzyloxycarbonylamino-2,3-dihydro-5-isopropyl-9-methyl-1H-1,4-benzodiazepin-2-one

(3RS)-3-benzyloxycarbonylamino-1-cyclohexyl-carbonylmethyl-2,3-dihydro-5-isopropyl-9-methyl-1H-1,4-benzodiazepin-2-one
205996-62-9

(3RS)-3-benzyloxycarbonylamino-1-cyclohexyl-carbonylmethyl-2,3-dihydro-5-isopropyl-9-methyl-1H-1,4-benzodiazepin-2-one

Conditions
ConditionsYield
Stage #1: (3RS)-3-benzyloxycarbonylamino-2,3-dihydro-5-isopropyl-9-methyl-1H-1,4-benzodiazepin-2-one With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 4h; deprotonation;
Stage #2: Bromomethyl cyclohexyl ketone In N,N-dimethyl-formamide at 20℃; for 5.5h; Alkylation;
66.4%

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