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inquiry1-BENZYL-1-PHENYLHYDRAZINE HYDROCHLORIDE CAS:5705-15-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high q
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryProduct Name: 1-BENZYL-1-PHENYLHYDRAZINE HYDROCHLORIDE Synonyms: 1-benzyl-1-phenyl-hydrazinhydrochloride;1-phenyl-1-(phenylmethyl)-hydrazinmonohydrochloride;alpha-benzyl-alpha-phenylhydrazinehydrochloride;usafek-1666;1-BENZYL-1-PHENYLHYDRAZINE HY
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inquiryN-Benzyl-N-phenylhydrazine hydrochloride cas 5705-15-7Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryConditions | Yield |
---|---|
With pyridine; pyridine hydrochloride at 100℃; for 23h; Inert atmosphere; | 98% |
C14H17NO2
N-benzyl-N-phenylhydrazine hydrochloride
5-(1-benzyl-1H-indol-3-yl)-2-(benzyloxy)pentanenitrile
Conditions | Yield |
---|---|
With acetic acid at 100℃; for 1h; Fischer indole synthesis; Inert atmosphere; | 89% |
1-phenyl-2-(2-propenyloxy)ethanone
N-benzyl-N-phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
With L-Tartaric acid at 70℃; for 4h; | 87% |
N-benzyl-N-phenylhydrazine hydrochloride
α-dimethylaminomethylene-N-phenyl-γ-butyrolactam
A
2,3,4,9-Tetrahydro-2-phenyl-1H-pyrido<3,4-b>indol-1-one
B
9-benzyl-2-phenyl-1-oxo-1,2,3,4-tetrahydro-β-carboline
Conditions | Yield |
---|---|
In hydrogenchloride; isopropyl alcohol for 3h; Heating; | A 3% B 86% |
N-benzyl-N-phenylhydrazine hydrochloride
α-dimethylaminomethylene-γ-butyrolactam
A
1,2,3,4-tetrahydronorharman-1-one
B
9-benzyl-2,3,4,9-tetrahydro-1H-β-carbolin-1-one
Conditions | Yield |
---|---|
With hydrogenchloride In isopropyl alcohol for 3h; Heating; | A 5% B 82% |
N-benzyl-N-phenylhydrazine hydrochloride
3-<(N,N-dimethylamino)methylene>-1-methyl-2-pyrrolidinone
A
Strychnocarpine
B
2,3,4,9-Tetrahydro-2-methyl-9-(phenylmethyl)-1H-pyrido<3,4-b>indol-1-one
Conditions | Yield |
---|---|
With hydrogenchloride In water; isopropyl alcohol for 3h; Heating; | A n/a B 80% |
3,4-dihydro-2H-thiopyran
N-benzyl-N-phenylhydrazine hydrochloride
1-(2-tetrahydrothiopyranylthio)-3-(1-benzyl-3-indolyl)propane
Conditions | Yield |
---|---|
With water In 1,4-dioxane for 4h; Heating; | 79% |
hexyl 6-methoxy-2-naphthyl ketone
N-benzyl-N-phenylhydrazine hydrochloride
1-benzyl-2-(6-methoxynaphthalen-2-yl)-3-pentyl-1H-indole
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol; water at 70 - 80℃; for 7h; Fischer Indole Synthesis; Heating / reflux; | 78% |
N-benzyl-N-phenylhydrazine hydrochloride
3-[1-Dimethylamino-meth-(Z)-ylidene]-dihydro-thiophen-2-one
Conditions | Yield |
---|---|
With trifluoroacetic acid In 1,4-dioxane for 8h; Heating; | 77% |
Conditions | Yield |
---|---|
With hydrogenchloride In water; isopropyl alcohol for 3h; Reflux; | 76% |
With hydrogenchloride In water; isopropyl alcohol for 3h; Reflux; | 76% |
ethyl 4-acetyl-3,5-dimethylpyrrole-2-carboxylate
N-benzyl-N-phenylhydrazine hydrochloride
2,4-dimethyl-3-acetyl-5-ethoxycarbonylpyrrole N-benzyl-N-phenylhydrazone hydrochloride
Conditions | Yield |
---|---|
In ethanol for 5h; Heating; | 75% |
diethyl (3-oxopropyl)phosphonate
N-benzyl-N-phenylhydrazine hydrochloride
(1-Benzyl-1H-indol-3-ylmethyl)-phosphonic acid diethyl ester
Conditions | Yield |
---|---|
In ethanol Heating; | 72% |
N-benzyl-N-phenylhydrazine hydrochloride
α,α'-hydroxybis(1-methyl-3-methylene-2-piperidone)
10-benzyl-2-methyl-3,4,5,10-tetrahydroazepino[3,4-b]indol-1(2H)-one
Conditions | Yield |
---|---|
With sulfuric acid In ethanol; water for 4h; Heating; | 70% |
1-benzylpyrrolidine-2,3-dione
N-benzyl-N-phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
Stage #1: 1-benzylpyrrolidine-2,3-dione; N-benzyl-N-phenylhydrazine hydrochloride With acetic acid at 80℃; for 0.333333h; Stage #2: With hydrogenchloride In water at 80℃; for 2.5h; | 66% |
N-benzyl-N-phenylhydrazine hydrochloride
1-Methyl-3-formyl-2-pyrrolidone
2,3,4,9-Tetrahydro-2-methyl-9-(phenylmethyl)-1H-pyrido<3,4-b>indol-1-one
Conditions | Yield |
---|---|
With hydrogenchloride In water; isopropyl alcohol for 3h; Heating; | 62% |
N-benzyl-N-phenylhydrazine hydrochloride
N-methyl-α-dimethylaminomethylenesuccinimide
A
2-Methyl-4,9-dihydro-β-carboline-1,3-dione
B
9-Benzyl-2-methyl-4,9-dihydro-β-carboline-1,3-dione
Conditions | Yield |
---|---|
With hydrogenchloride In acetic acid for 3h; Heating; | A 13% B 61% |
N-benzyl-N-phenylhydrazine hydrochloride
N-methyl-α-dimethylaminomethyleneglutarimide
A
2-methyl-1,3-dioxo-1,2,3,4,5,10-hexahydroazepino<3,4-b>indole
B
2-methyl-10-benzyl-1,3-dioxo-1,2,3,4,5,10-hexahydroazepino<3,4-b>indole
Conditions | Yield |
---|---|
With hydrogenchloride In acetic acid for 3h; Heating; | A 7% B 61% |
N-benzyl-N-phenylhydrazine hydrochloride
α-dimethylaminomethylene-N-butyl-γ-butyrolactam
A
9-Benzyl-2-butyl-2,3,4,9-tetrahydro-β-carbolin-1-one
B
2-n-butyl-1-oxo-1,2,3,4-tetrahydro-β-carboline
Conditions | Yield |
---|---|
With hydrogenchloride In methanol; isopropyl alcohol for 3h; Heating; | A 60% B n/a |
1-methylpiperidin-2-one
N-benzyl-N-phenylhydrazine hydrochloride
N,N-dimethyl-formamide
10-benzyl-2-methyl-3,4,5,10-tetrahydroazepino[3,4-b]indol-1(2H)-one
Conditions | Yield |
---|---|
Stage #1: 1-methylpiperidin-2-one; N,N-dimethyl-formamide With trichlorophosphate In benzene for 5.5h; Vilsmeier Reaction; Reflux; Stage #2: N-benzyl-N-phenylhydrazine hydrochloride In ethanol for 2h; Reflux; | 60% |
Stage #1: 1-methylpiperidin-2-one; N,N-dimethyl-formamide With trichlorophosphate In benzene for 5.5h; Vilsmeier Reaction; Reflux; Stage #2: N-benzyl-N-phenylhydrazine hydrochloride In ethanol for 2h; Reflux; | 60% |
N-benzyl-N-phenylhydrazine hydrochloride
Ethyl β-(2,4-dimethyl-5-carboethoxypyrrolyl-3)-β-ketopropionate
2,4-dimethyl-3-acetyl-5-ethoxycarbonylpyrrole N-benzyl-N-phenylhydrazone hydrochloride
Conditions | Yield |
---|---|
In ethanol for 11h; Heating; than standing for 2 days; | 59% |
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 20℃; for 2h; | 59% |
Diphenyliodonium triflate
N-benzyl-N-phenylhydrazine hydrochloride
N′-benzyl-N′-phenylbenzenesulfonohydrazide
Conditions | Yield |
---|---|
With potassium pyrosulfite; C34H30N2O4 In dimethyl sulfoxide; acetonitrile at 20℃; for 2h; Inert atmosphere; Schlenk technique; Irradiation; | 59% |
α-hydroxymethylene-N-methyl-δ-valerolactam
N-benzyl-N-phenylhydrazine hydrochloride
A
10-benzyl-2-methyl-3,4,5,10-tetrahydroazepino[3,4-b]indol-1(2H)-one
B
2-methyl-3,4,5,10-tetrahydroazepino[3,4-b]indol-1(2H)-one
Conditions | Yield |
---|---|
With sulfuric acid In ethanol; water for 4h; Heating; | A 57% B 8% |
3-oxopentanedioic acid dimethyl ester
N-benzyl-N-phenylhydrazine hydrochloride
methyl 1-benzyl-2-(2-methoxy-2-oxoethyl)-1H-indole-3-carboxylate
Conditions | Yield |
---|---|
In methanol Fischer Indole Synthesis; Heating; | 57% |
In methanol for 12h; Fischer Indole Synthesis; Heating; | 57% |
N-benzyl-N-phenylhydrazine hydrochloride
diethyl 1,3-acetonedicarboxylate
1-benzyl-2-ethoxycarbonylmethyl-indole-3-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
In ethanol Fischer Indole Synthesis; Reflux; | 54% |
N-benzyl-N-phenylhydrazine hydrochloride
4a′-methyl-4′,4a′,7′,8′-tetrahydro-3′H-spiro[[1,3]dithiolane-2,2′-naphthalen]-5′(6′H)-one
Conditions | Yield |
---|---|
With acetic acid at 100℃; for 2h; Inert atmosphere; | 53% |
Conditions | Yield |
---|---|
In acetic acid for 1h; Fiacher indole synthesis; Heating; | 52% |
N-benzyl-N-phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene at 130℃; for 0.5h; Fischer Indole Synthesis; Microwave irradiation; | 51% |
3,4-dihydro-2H-thiopyran
N-benzyl-N-phenylhydrazine hydrochloride
5-(2-tetrahydrothiopyranylthio)pentanal α-benzylphenylhydrazone
Conditions | Yield |
---|---|
In 1,4-dioxane; water for 24h; Ambient temperature; | 50% |
N-benzyl-N-phenylhydrazine hydrochloride
3-[1-Dimethylamino-meth-(Z)-ylidene]-1-methyl-azepan-2-one
A
2-methyl-2,3,4,5,6,11-hexahydro-1H-azocino<3,4-b>indol-1-one
B
2-methyl-11-benzyl-2,3,4,5,6,11-hexahydro-1H-azocino<3,4-b>indol-1-one
Conditions | Yield |
---|---|
With sulfuric acid In ethanol; water for 4h; Heating; | A 17% B 45% |
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