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Hangzhou ZeErRui Chemical Co., Ltd.

Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home

1,4,7-Triazacyclononane trihydrochloride manufacture

Cas:58966-93-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine c

1,4,7-Triazacyclononane trihydrochloride

Cas:58966-93-1

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

1,4,7-Triazacyclononane trihydrochloride

Cas:58966-93-1

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

Product Name: 1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE Synonyms: OCTAHYDRO-1H-1,4,7-TRIAZONINE TRIHYDROCHLORIDE;1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE;1,4,7-TriazacyclononanetriHCl;1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE 97+%;1,4,7-

58966-93-1 1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE

Cas:58966-93-1

Min.Order:1 Kilogram

FOB Price: $8900.0

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 58966-93-1 with best quality

Cas:58966-93-1

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE

Cas:58966-93-1

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

1H-1,4,7-Triazonine, octahydro-, hydrochloride (1:3) 58966-93-1

Cas:58966-93-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

1H-1,4,7-Triazonine, octahydro-, hydrochloride (1:3)

Cas:58966-93-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

1,4,7-Triazacyclononane trihydrochloride

Cas:58966-93-1

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE

Cas:58966-93-1

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

1H-1,4,7-Triazonine, octahydro-, hydrochloride (1:3)

Cas:58966-93-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE

Cas:58966-93-1

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

Siwei Development Group Ltd.

Product name: 1,4,7-Triazacyclononane Trihydrochloride CAS No.: 58966-93-1 Molecule Formula:C6H18Cl3N3 Molecule Weight:238.59 Purity: 99.0% Package: 25kg/drum Description:Yellow to white solid Manufacture Standards:Enterprise Standard

Lower Price 1,4,7-Triazacyclononane Trihydrochloride on stock

Cas:58966-93-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

Product Name: 1,4,7-Triazacyclononane Trihydrochloride Synonyms: OCTAHYDRO-1H-1,4,7-TRIAZONINE TRIHYDROCHLORIDE;1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE;1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE 97+%;1,4,7-TriazacyclononanetriHCl;1,4,7-Triazacy

1,4,7-Triazacyclononane Trihydrochloride

Cas:58966-93-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE

Cas:58966-93-1

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Hangzhou Huarong Pharm Co., Ltd.

We Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O

1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE

Cas:58966-93-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE

Cas:58966-93-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE

Cas:58966-93-1

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE

Cas:58966-93-1

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE cas no. 58966-93-1 98%

Cas:58966-93-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE

Cas:58966-93-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

1,4,7-triazonane trihydrochloride

Cas:58966-93-1

Min.Order:0

Negotiable

Type:Other

inquiry

JINHUA HUAYI CHEMICAL CO., LTD.

Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands

1,4,7-Triazacyclononane Hydrochloride

Cas:58966-93-1

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Acmec Biochemical Technology Co., Ltd.

Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea

Acmec 1,4,7-Triazonane Trihydrochloride 25g

Cas:58966-93-1

Min.Order:1 bottle

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE

Cas:58966-93-1

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hubei Taiho Chemical Co.,LTD

TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp

1,4,7-triazonane trihydrochloride

Cas:58966-93-1

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

1H-1,4,7-Triazonine,octahydro-, hydrochloride (1:3)

Cas:58966-93-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present

1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE

Cas:58966-93-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

We are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for

1,4,7-TRIAZACYCLONONANE TRIHYDROCHLORIDE

Cas:58966-93-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

BOC Sciences

We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white to yellow crystal powder Storage:Room temperature with sealed well Package:according to the clients requirement Applicatio

Octahydro-1H-1,4,7-triazonine Trihydrochloride

Cas:58966-93-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

N,N',N-tris(p-toluenesulfonyl)-1,4,7-triazacyclononane
52667-89-7

N,N',N-tris(p-toluenesulfonyl)-1,4,7-triazacyclononane

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

Conditions
ConditionsYield
Stage #1: N,N',N-tris(p-toluenesulfonyl)-1,4,7-triazacyclononane With sulfuric acid at 100℃; for 72h; Inert atmosphere;
Stage #2: With sodium hydroxide In water Inert atmosphere;
Stage #3: With hydrogenchloride In water pH=1;
99%
With sulfuric acid at 180℃; for 0.133333h; other linear and macrocyclic p-toluenesulfonamides;92%
With sulfuric acid at 180℃; for 0.133333h;92%
1,4-di-tert-butyl-1,4,7-triazacyclononane

1,4-di-tert-butyl-1,4,7-triazacyclononane

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

Conditions
ConditionsYield
With hydrogenchloride In water at 95℃; Sealed tube;89%
N,N'-bis(p-toluenesulfonyl)-1,4,7-triazacyclononane
95388-08-2

N,N'-bis(p-toluenesulfonyl)-1,4,7-triazacyclononane

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

Conditions
ConditionsYield
Stage #1: N,N'-bis(p-toluenesulfonyl)-1,4,7-triazacyclononane With sulfuric acid at 120℃; for 72h; Green chemistry;
Stage #2: With hydrogenchloride In ethanol; water Green chemistry;
84%
C14H27N3O2

C14H27N3O2

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / diethyl ether; tetrahydrofuran / 20 °C / Glovebox
2: hydrogenchloride / water / 95 °C / Sealed tube
View Scheme
N,N′-bis(2-chloroacetyl)-N,N′-di-tert-butylethylenediamine

N,N′-bis(2-chloroacetyl)-N,N′-di-tert-butylethylenediamine

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: ammonium hydroxide / acetonitrile / 6 h / 100 °C / Sealed tube
2: lithium aluminium tetrahydride / diethyl ether; tetrahydrofuran / 20 °C / Glovebox
3: hydrogenchloride / water / 95 °C / Sealed tube
View Scheme
ethylene dibromide
106-93-4

ethylene dibromide

1,5-diamino-3-azapentane
111-40-0

1,5-diamino-3-azapentane

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

Conditions
ConditionsYield
Stage #1: ethylene dibromide; 3-azapentane-1,5-diamine With potassium carbonate; p-toluenesulfonyl chloride In ethylene dibromide
Stage #2: With sulfuric acid at 90℃; for 48h;
Stage #3: With hydrogenchloride
methyl 4-{[4-(2-ethoxy-2-oxoethoxy)-2,6-dimethylphenyl]ethynyl}-6-{[(methylsulfonyl)oxy]methyl}picolinate

methyl 4-{[4-(2-ethoxy-2-oxoethoxy)-2,6-dimethylphenyl]ethynyl}-6-{[(methylsulfonyl)oxy]methyl}picolinate

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

C72H78N6O15

C72H78N6O15

Conditions
ConditionsYield
With potassium carbonate In acetonitrile at 60℃; Inert atmosphere;100%
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile
58632-95-4

2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

1,4-di-tert-butyl 1,4,7-triazonane-1,4-dicarboxylate
174138-01-3

1,4-di-tert-butyl 1,4,7-triazonane-1,4-dicarboxylate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In chloroform for 120h;100%
ethyl 4-((2-ethoxy-2-oxoethyl)thio)-6-(((methylsulfonyl)oxy)methyl)picolinate

ethyl 4-((2-ethoxy-2-oxoethyl)thio)-6-(((methylsulfonyl)oxy)methyl)picolinate

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

triethyl-6,6',6''-((1,4,7-triazacyclononane-1,4,7-triyl)tris(methylene))tris(4-((2-ethoxy-2-oxoethyl)thio)picolinate)

triethyl-6,6',6''-((1,4,7-triazacyclononane-1,4,7-triyl)tris(methylene))tris(4-((2-ethoxy-2-oxoethyl)thio)picolinate)

Conditions
ConditionsYield
With potassium carbonate In acetonitrile at 60℃; for 12h; Inert atmosphere;100%
(4-((3-(diethylamino)-4-methoxyphenyl)ethynyl)-6-(ethoxy(methyl)phosphoryl)pyridin-2-yl)methyl methanesulfonate

(4-((3-(diethylamino)-4-methoxyphenyl)ethynyl)-6-(ethoxy(methyl)phosphoryl)pyridin-2-yl)methyl methanesulfonate

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

triethyl (((1,4,7-triazacyclononane-1,4,7-triyl)tris(methylene))tris(4-((3-(diethylamino)-4-methoxyphenyl)ethynyl)pyridine-6,2-diyl))tris(methylphosphinate)

triethyl (((1,4,7-triazacyclononane-1,4,7-triyl)tris(methylene))tris(4-((3-(diethylamino)-4-methoxyphenyl)ethynyl)pyridine-6,2-diyl))tris(methylphosphinate)

Conditions
ConditionsYield
With potassium carbonate In acetonitrile at 50℃; for 12h; Inert atmosphere;100%
99mtechnetium pertechnetate

99mtechnetium pertechnetate

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

[(99)TcO3(tacn)](1+)
910095-44-2

[(99)TcO3(tacn)](1+)

Conditions
ConditionsYield
With sodium tetrahydroborate; sodium hydroxide at 20℃; for 0.25h; Product distribution / selectivity; Inert atmosphere;97%
ethyl 2-[4-({2-[ethoxy(methyl)phosphoryl]-6-{[(methylsulfonyl)-oxy]methyl}pyridin-4-yl}ethynyl)-3,5-dimethylphenoxy]acetate

ethyl 2-[4-({2-[ethoxy(methyl)phosphoryl]-6-{[(methylsulfonyl)-oxy]methyl}pyridin-4-yl}ethynyl)-3,5-dimethylphenoxy]acetate

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

triethyl-2,2’,2’’-[({(6,6’,6’’-[(1,4,7-triazacyclononane-1,4,7-triyl)tris(methylene)]tris{2-[ethoxy(methyl)phosphoryl]pyridine-6,4-diyl})tris(ethyne-2,1-diyl)}tris(3,5-dimethylbenzene-4,1-diyl))tris(oxy)]triacetate

triethyl-2,2’,2’’-[({(6,6’,6’’-[(1,4,7-triazacyclononane-1,4,7-triyl)tris(methylene)]tris{2-[ethoxy(methyl)phosphoryl]pyridine-6,4-diyl})tris(ethyne-2,1-diyl)}tris(3,5-dimethylbenzene-4,1-diyl))tris(oxy)]triacetate

Conditions
ConditionsYield
With potassium carbonate In acetonitrile at 60℃; for 24h; Inert atmosphere;95%
4-nitrophenyl 2-(2-(dioctylamino)-2-oxoethoxy)acetate
1354344-55-0

4-nitrophenyl 2-(2-(dioctylamino)-2-oxoethoxy)acetate

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

2,2′,2′′-(((1,4,7-triazonane-1,4,7-triyl)tris(2-oxoethane-2,1-diyl))tris(oxy))tris(N,N-dioctylacetamide)

2,2′,2′′-(((1,4,7-triazonane-1,4,7-triyl)tris(2-oxoethane-2,1-diyl))tris(oxy))tris(N,N-dioctylacetamide)

Conditions
ConditionsYield
With triethylamine In toluene for 15h; Reflux;95%
1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

1,4,7-triazacyclononane
4730-54-5

1,4,7-triazacyclononane

Conditions
ConditionsYield
With sodium hydroxide In water; toluene Heating;91%
With sodium hydroxide In water pH=12;89%
With sodium hydroxide In water pH=13;79.4%
chloroacetic acid cholesterylester
3464-50-4

chloroacetic acid cholesterylester

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

1,4,7-tris[(cholesteryloxycarbonyl)methyl]-1,4,7-triazacyclononane
1246210-95-6

1,4,7-tris[(cholesteryloxycarbonyl)methyl]-1,4,7-triazacyclononane

Conditions
ConditionsYield
Stage #1: 1,4,7-triazacyclononane trihydrochloride With potassium carbonate In acetonitrile for 1.5h; Reflux; Inert atmosphere;
Stage #2: chloroacetic acid cholesterylester In dichloromethane; acetonitrile for 7h; Reflux; Inert atmosphere;
91%
methyl 4-((4-methoxyphenyl)ethynyl)-6-(((methylsulfonyl)oxy)methyl)picolinate
1417730-34-7

methyl 4-((4-methoxyphenyl)ethynyl)-6-(((methylsulfonyl)oxy)methyl)picolinate

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

C57H54N6O9
1417730-05-2

C57H54N6O9

Conditions
ConditionsYield
Stage #1: 1,4,7-triazacyclononane trihydrochloride With potassium carbonate In acetonitrile at 65℃; for 0.25h;
Stage #2: methyl 4-((4-methoxyphenyl)ethynyl)-6-(((methylsulfonyl)oxy)methyl)picolinate In acetonitrile at 65℃; for 3h;
87%
With potassium carbonate In acetonitrile at 60℃; for 3h; Inert atmosphere;87%
With potassium carbonate In acetonitrile at 60℃; for 4h;85%
aquapentaamminecobalt(III) perchlorate
13820-81-0

aquapentaamminecobalt(III) perchlorate

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

[Co(1,4,7-triazacyclononane)2](ClO4)3

[Co(1,4,7-triazacyclononane)2](ClO4)3

Conditions
ConditionsYield
In water heating with activated carbon for 3 h at 80°C; cooling; filtration; evapn. to half the volume; addn. of ethanol; pptn.; filtration; washing (ethanol, ether); chromy. (Sephadex-C-25, HClO4); evapn.; addn. of ethanol or propanol; pptn.; elem. anal.;85%
methyl 4-((4-methoxy-3-((methyl(phenyl)amino)methyl)phenyl)-ethynyl)-6-(((methylsulfonyl)oxy)methyl)picolinate

methyl 4-((4-methoxy-3-((methyl(phenyl)amino)methyl)phenyl)-ethynyl)-6-(((methylsulfonyl)oxy)methyl)picolinate

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

trimethyl 6,6’,6’’-((1,4,7-triazacyclononane-1,4,7-triyl)tris(methylene))tris(4-((4-methoxy-3-((methyl(phenyl)amino)methyl)phenyl)ethynyl)picolinate)

trimethyl 6,6’,6’’-((1,4,7-triazacyclononane-1,4,7-triyl)tris(methylene))tris(4-((4-methoxy-3-((methyl(phenyl)amino)methyl)phenyl)ethynyl)picolinate)

Conditions
ConditionsYield
With potassium carbonate In acetonitrile at 60℃; for 24h; Inert atmosphere;85%
tetrafluoroboric acid

tetrafluoroboric acid

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

C6H15N3*ClH*2BF4(1-)*2H(1+)

C6H15N3*ClH*2BF4(1-)*2H(1+)

Conditions
ConditionsYield
In water81%
copper(II) perchlorate hexahydrate

copper(II) perchlorate hexahydrate

sodium bis(4-nitrophenyl) phosphate
4043-96-3

sodium bis(4-nitrophenyl) phosphate

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

[Cu(1,4,7-triazacyclononane)2](bis(p-nitrophenyl)phosphate)2

[Cu(1,4,7-triazacyclononane)2](bis(p-nitrophenyl)phosphate)2

Conditions
ConditionsYield
With NaOH In water aq. soln. of Cu salt added to aq. soln. of ligand (molar ratio 1:2); pH adjusted to 5-6 (1 M NaOH); soln. of phosphate (1 equiv.) in min. amt. of water added; pH increased to ca. 7 (1 M NaOH); stored overnight; crystals collected by vac. filtration; washed with water and EtOH; air dried; elem. anal.;80%
methyl 4-((4-methoxy-2,6-dimethylphenyl)ethynyl)-6-(((methylsulfonyl)oxy)methyl)picolinate

methyl 4-((4-methoxy-2,6-dimethylphenyl)ethynyl)-6-(((methylsulfonyl)oxy)methyl)picolinate

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

C63H66N6O9

C63H66N6O9

Conditions
ConditionsYield
Stage #1: 1,4,7-triazacyclononane trihydrochloride With potassium carbonate In acetonitrile at 65℃; for 0.333333h;
Stage #2: methyl 4-((4-methoxy-2,6-dimethylphenyl)ethynyl)-6-(((methylsulfonyl)oxy)methyl)picolinate In acetonitrile at 65℃; for 20h;
80%
methyl 6-(bromomethyl)-4-methoxypicolinate

methyl 6-(bromomethyl)-4-methoxypicolinate

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

C24H33N5O6

C24H33N5O6

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In methanol at 50℃; for 16h;80%
2-(4-methoxybenzyloxycarbonyloxyimino)-2-phenylacetonitrile
59577-32-1

2-(4-methoxybenzyloxycarbonyloxyimino)-2-phenylacetonitrile

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

1,4-bis(4-methoxybenzyloxycarbonyl)-1,4,7-triazacyclononane
1417729-26-0

1,4-bis(4-methoxybenzyloxycarbonyl)-1,4,7-triazacyclononane

Conditions
ConditionsYield
Stage #1: 2-(4-methoxybenzyloxycarbonyloxyimino)-2-phenylacetonitrile; 1,4,7-triazacyclononane trihydrochloride In 1,4-dioxane; water at 23℃; for 0.0833333h; Inert atmosphere;
Stage #2: With triethylamine In 1,4-dioxane; water for 24h; Inert atmosphere;
78%
With triethylamine In 1,4-dioxane; water for 24h;74%
With triethylamine In 1,4-dioxane; water for 24h;74%
N,N-dimethyl-formamide dimethyl acetal
4637-24-5

N,N-dimethyl-formamide dimethyl acetal

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

tacnoa
67705-38-8

tacnoa

Conditions
ConditionsYield
Stage #1: 1,4,7-triazacyclononane trihydrochloride With sodium hydroxide In water
Stage #2: N,N-dimethyl-formamide dimethyl acetal In toluene at 90℃; for 4h; Further stages.;
77%
C26H26BrNO3S
1245085-00-0

C26H26BrNO3S

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

NOTA(CysC(C6H5)3OC2H5)3

NOTA(CysC(C6H5)3OC2H5)3

Conditions
ConditionsYield
With potassium carbonate In acetonitrile at 20℃; for 16h; Inert atmosphere;77%
C22H29NO9S

C22H29NO9S

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

C69H90N6O18

C69H90N6O18

Conditions
ConditionsYield
With sodium carbonate In acetonitrile at 60℃; for 48h; Schlenk technique; Inert atmosphere;75%
Stage #1: 1,4,7-triazacyclononane trihydrochloride With sodium carbonate In acetonitrile at 20℃; for 0.166667h; Inert atmosphere;
Stage #2: C22H29NO9S In acetonitrile at 20 - 60℃; for 48h; Inert atmosphere;
75%
(4-bromo-6-(ethoxy(methyl)phosphoryl)pyridin-2-yl)methylmethanesulfonate

(4-bromo-6-(ethoxy(methyl)phosphoryl)pyridin-2-yl)methylmethanesulfonate

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

C33H48Br3N6O6P3

C33H48Br3N6O6P3

Conditions
ConditionsYield
With potassium carbonate In acetonitrile Inert atmosphere; Reflux;74%
C8H7BrClNO2

C8H7BrClNO2

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

C22H27Cl2N5O4

C22H27Cl2N5O4

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In methanol at 50℃; for 16h;74%
1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

6-(bromomethyl)pyridine-2-carbonitrile
104508-24-9

6-(bromomethyl)pyridine-2-carbonitrile

1,4,7-tris[(6-cyanopyridin-2-yl)methyl]-1,4,7-triazacyclononane
1030597-88-6

1,4,7-tris[(6-cyanopyridin-2-yl)methyl]-1,4,7-triazacyclononane

Conditions
ConditionsYield
With potassium carbonate In acetonitrile for 6h; Inert atmosphere; Reflux;71%
copper(II) choride dihydrate

copper(II) choride dihydrate

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

dichloro(1,4,7-triazacyclononane)copper(II)

dichloro(1,4,7-triazacyclononane)copper(II)

Conditions
ConditionsYield
With sodium hydroxide In water byproducts: NaCl; stoich. amts.; crystn., dissoln. in water, dropwise addn. of EtOH (to turbidity), cooling, filtration off of NaCl, evapn., recrystn. (water); elem. anal.;70%
C37H44N2O5S

C37H44N2O5S

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

C114H135N9O6

C114H135N9O6

Conditions
ConditionsYield
With sodium carbonate In acetonitrile at 55℃; Inert atmosphere;70%
iron(III) chloride

iron(III) chloride

C3H3(2)H6N3O3*ClH

C3H3(2)H6N3O3*ClH

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

C9H15(2)H6FeN6O3(1+)*Cl(1-)

C9H15(2)H6FeN6O3(1+)*Cl(1-)

Conditions
ConditionsYield
With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene In methanol at 20℃; for 25h; Sealed tube;69%
C24H33NO9S

C24H33NO9S

1,4,7-triazacyclononane trihydrochloride
58966-93-1

1,4,7-triazacyclononane trihydrochloride

C75H102N6O18

C75H102N6O18

Conditions
ConditionsYield
Stage #1: 1,4,7-triazacyclononane trihydrochloride With sodium carbonate In acetonitrile at 20℃; for 0.0833333h;
Stage #2: C24H33NO9S In acetonitrile at 60℃; for 96h;
66%

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