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Cas:618-95-1
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inquiryDayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:618-95-1
Min.Order:1 Kilogram
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:618-95-1
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inquiryMethyl 3-nitrobenzoate Product name: Methyl 3-nitrobenzoate CAS NO. : 618-95-1 Molecular formula: C8H7NO4 Structural formula: Molecular weight:
Cas:618-95-1
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:618-95-1
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:618-95-1
Min.Order:1 Kilogram
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Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:618-95-1
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inquiryProduct name Methyl 3-nitrobenzoate CAS 618-95-1 Package 25kg/drum Purity 99.0% Appearance: White powder Storage:Store in cool and d
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Cas:618-95-1
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
superior quality moderate price & quick delivery Appearance:beige crystalline powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used t
Cas:618-95-1
Min.Order:1 Kilogram
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Type:Trading Company
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:618-95-1
Min.Order:0 Metric Ton
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:618-95-1
Min.Order:4 Kilogram
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Type:Lab/Research institutions
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:618-95-1
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:618-95-1
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Type:Lab/Research institutions
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:618-95-1
Min.Order:1 Kilogram
FOB Price: $30.0
Type:Lab/Research institutions
inquiryProduct name: Methyl 3-Nitrobenzoate CAS No.:618-95-1 Molecule Formula:C8H7NO4 Molecule Weight:181.15 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard
Cas:618-95-1
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Our company is engaged in customizing the benzene ring and pyridine derivative organic intermediates, and the quantity is flexible according to customer's needs. It mainly provides high-quality intermediates for domestic and foreign pharmaceutical an
Cas:618-95-1
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Type:Lab/Research institutions
inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:618-95-1
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Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
Cas:618-95-1
Min.Order:0
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Type:Lab/Research institutions
inquiryAcmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
Cas:618-95-1
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp
Fredchem focus on CRO/CMO business and its own R&D of API/Intermediates Package:Grams, Kilograms Application:Pharmaceutical field Transportation:According to customer request Port:Shanghai
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:25kg,50kg,180kg,200kg,250kg,1000kg,customization Application:Pharma;Industry;Agricultural;chemical reaserch Tran
Conditions | Yield |
---|---|
With 1-(ferrocenylbutyl)-4-(3-methylimidazolium) tetrafluoroborate; iodine; potassium carbonate at 50 - 60℃; for 24h; Inert atmosphere; | 100% |
With palladium 10% on activated carbon; oxygen; sodium carbonate at 90℃; under 15001.5 Torr; for 2h; Microwave irradiation; Green chemistry; | 98% |
With 3-(7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl)methyl-1-(2,4,6-trimethylphenyl)-1H-imidazol-3-ium bis(trifluoromethanesulfonimide) salt; caesium carbonate In toluene at 60℃; for 3h; | 98% |
Conditions | Yield |
---|---|
In 2-methyltetrahydrofuran; diethyl ether at 20℃; for 0.486667h; Flow reactor; | 99% |
With diethyl ether | |
In diethyl ether | |
at 0℃; for 0.25h; | 62.3 mg |
Conditions | Yield |
---|---|
With 4-methyl-morpholine; 2-chloro-4-methoxy-6-(N-phenylbenzamido)-1,3,5-triazine at 20℃; for 1h; | 99% |
With oxone at 65℃; for 30h; | 98% |
Stage #1: 3-nitrobenzoic acid With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; Stage #2: methanol In dichloromethane for 0.0833333h; | 98% |
methanol
m-iodonitrobenzene
carbon monoxide
methyl 3-nitrobenzoate
Conditions | Yield |
---|---|
With triethylamine at 100℃; under 3750.38 Torr; for 1.5h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With oxone at 65℃; for 30h; | 99% |
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide at 20℃; for 2h; | 98% |
In acetonitrile for 8h; Inert atmosphere; Alkaline conditions; |
Conditions | Yield |
---|---|
With sodium carbonate; palladium; silver(l) oxide at 80℃; for 48h; Molecular sieve; | 98% |
Stage #1: 3-Nitrobenzyl alcohol In toluene at 80℃; for 2h; Sonication; Stage #2: methanol With Oxone In toluene for 1.5h; Sonication; | 90% |
With dibromamine-T; potassium carbonate In acetonitrile at 20℃; for 0.5h; Reagent/catalyst; Solvent; | 88% |
Conditions | Yield |
---|---|
With oxone at 65℃; for 30h; | 98% |
Conditions | Yield |
---|---|
With oxone at 65℃; for 30h; | 95% |
Conditions | Yield |
---|---|
Stage #1: 3-nitrobenzoic acid With potassium carbonate In acetone for 0.5h; Stage #2: dimethyl sulfate In acetone at 20℃; for 2h; | 94.3% |
Conditions | Yield |
---|---|
With trifluoromethylsulfonic anhydride; ethylammonium nitrate at -5 - 20℃; for 2h; Inert atmosphere; regioselective reaction; | 94% |
With sulfuric acid; guanidine nitrate at 0 - 5℃; for 3h; | 76% |
With boron trifluoride; nitric acid |
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide for 0.0166667h; microwave irradiation; | 94% |
With layered double hydroxide - supported L-methionine at 180℃; for 6h; Autoclave; chemoselective reaction; | 89% |
3-nitrobenzoic acid
methyl salicylate
A
methyl 3-nitrobenzoate
B
salicylic acid
Conditions | Yield |
---|---|
Stage #1: 3-nitrobenzoic acid With potassium carbonate In N,N-dimethyl acetamide at 110℃; for 0.5h; Stage #2: methyl salicylate at 110℃; for 24h; | A 93% B n/a |
(4-(methoxycarbonyl)-2-nitrophenyl)boronic acid
A
dimethyl 2,2’-dinitro-[1,1’-biphenyl]-4,4’-dicarboxylate
B
methyl 3-nitrobenzoate
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); potassium fluoride dihydrate; tri tert-butylphosphoniumtetrafluoroborate In tetrahydrofuran for 1h; Suzuki-Miyaura Coupling; Inert atmosphere; Reflux; Schlenk technique; | A 10% B 88% |
Conditions | Yield |
---|---|
With N,N-dimethyl-formamide dimethyl acetal for 16h; Heating; | 87% |
3-nitrobenzoic acid
diazomethyl-trimethyl-silane
methyl 3-nitrobenzoate
Conditions | Yield |
---|---|
In methanol; toluene at 20℃; for 1.5h; | 87% |
In methanol; toluene at 20℃; for 1.5h; | 86.79% |
methyl 2-iodo-3-nitrobenzoate
methyl 3-nitrobenzoate
Conditions | Yield |
---|---|
With air; tributyl borane; water In benzene at 20℃; | 85% |
Conditions | Yield |
---|---|
With N,N-dimethyl-formamide dimethyl acetal for 16h; Heating; | 84% |
tris(o-methoxyphenyl)phosphine
3-nitrobenzoic acid
methyl 3-nitrobenzoate
Conditions | Yield |
---|---|
With dirhodium tetraacetate In cyclohexane at 120℃; for 12h; Schlenk technique; Inert atmosphere; | 81% |
Conditions | Yield |
---|---|
With 2-nitrobenzeneseleninic acid; dihydrogen peroxide at 20℃; for 48h; | 80% |
methyl 2-iodo-3-nitrobenzoate
phenylacetylene
A
methyl 3-nitro-2-(2-phenylethynyl)benzoate
B
methyl 3-nitrobenzoate
Conditions | Yield |
---|---|
With copper(l) iodide; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride In tetrahydrofuran at 45℃; for 48h; Sonogashira coupling; | A 80% B 28% |
Conditions | Yield |
---|---|
With pyridine; ferric(III) bromide; oxygen In chlorobenzene at 130℃; for 9h; Sealed tube; | 80% |
Conditions | Yield |
---|---|
With 2-nitrobenzeneseleninic acid; dihydrogen peroxide at 65℃; for 48h; | 79% |
[3-(methoxycarbonyl)phenyl]boronic acid
methyl 3-nitrobenzoate
Conditions | Yield |
---|---|
With Iron(III) nitrate nonahydrate In toluene at 80℃; for 18h; Inert atmosphere; | 78% |
Multi-step reaction with 2 steps 1.1: potassium hydrogen bifluoride / methanol; water / 0.03 h / 0 - 20 °C / Inert atmosphere 1.2: 0.02 h / 20 °C 2.1: Oxone / water; acetone / 2 h / 60 °C View Scheme |
(E,E)-1-(N,N-dimethylamino)-4-nitro-1,3-butadiene
propynoic acid methyl ester
methyl 3-nitrobenzoate
Conditions | Yield |
---|---|
In xylene for 8h; Heating; | 74.8% |
methanol
3-nitro-benzaldehyde
A
methyl 3-nitrobenzoate
B
3-nitrobenzoic acid
Conditions | Yield |
---|---|
With dihydrogen peroxide; calcium chloride at 65℃; for 48h; Reagent/catalyst; | A 74% B n/a |
With dihydrogen peroxide at 20 - 70℃; for 15h; Green chemistry; | A 68% B 31% |
With dihydrogen peroxide at 20℃; for 8h; |
Conditions | Yield |
---|---|
Stage #1: propan-1-ol; 3-nitro-benzaldehyde With sodium hypochlorite; sodium iodide In water for 0.166667h; Cooling with ice; Stage #2: With sodium hypochlorite In water for 1.33333h; Cooling with ice; | 74% |
Conditions | Yield |
---|---|
With potassium carbonate at 80℃; for 2h; Schlenk technique; Inert atmosphere; | 74% |
With potassium carbonate at 80℃; for 2h; Inert atmosphere; Sealed tube; | 74% |
Conditions | Yield |
---|---|
With pyridine; ferric(III) bromide; oxygen In chlorobenzene at 130℃; for 9h; Sealed tube; | 74% |
methanol
CYANAMID
3-nitro-benzaldehyde
A
methyl N-cyano-3-nitrobenzimidate
B
methyl 3-nitrobenzoate
Conditions | Yield |
---|---|
With N-Bromosuccinimide; sodium t-butanolate at 50℃; for 12h; | A 72% B 16% |
Conditions | Yield |
---|---|
With potassium fluoride; polymethylhydrosiloxane; palladium diacetate In tetrahydrofuran; water at 20℃; for 0.5h; | 100% |
With potassium fluoride; polymethylhydrosiloxane; palladium diacetate In tetrahydrofuran at 20℃; for 0.5h; | 100% |
With 5%-palladium/activated carbon; hydrogen In methanol at 20℃; | 100% |
methyl 3-nitrobenzoate
methyl 3-(hydroxylamino)benzoate
Conditions | Yield |
---|---|
With 5% Rh/C; hydrazine hydrate In tetrahydrofuran at 0℃; Inert atmosphere; Schlenk technique; Sealed tube; | 100% |
With 5% rhodium-on-charcoal; hydrazine hydrate In tetrahydrofuran at 0℃; for 2.5h; Inert atmosphere; | 99% |
With 5% rhodium-on-charcoal; hydrazine hydrate In tetrahydrofuran at 0℃; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With sulfur In methanol at 65℃; for 5h; Time; | 96.4% |
Conditions | Yield |
---|---|
With hydrazine hydrate In ethanol for 4h; Reflux; | 96% |
With hydrazine hydrate In ethanol at 85℃; for 4h; | 96.2% |
With hydrazine hydrate In ethanol for 0.2h; Reflux; Microwave irradiation; | 95% |
methyl 3-nitrobenzoate
sodium 4-methylbenzenesulfinate
methyl 3-{[(4-methylphenyl)sulfonyl]amino}benzoate
Conditions | Yield |
---|---|
With trans-N,N'-dimethyl-1,2-cyclohexyldiamine; sodium hydrogen sulfite; iron(II) chloride In dimethyl sulfoxide at 60℃; for 12h; Sealed tube; Inert atmosphere; | 95% |
With sodium hydrogensulfite In water at 60℃; for 20h; chemoselective reaction; | 86% |
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium hydroxide In methanol at 20℃; pH=> 10; | 93% |
Conditions | Yield |
---|---|
Stage #1: methyl 3-nitrobenzoate With ammonia In ethylene glycol at 40 - 45℃; for 20h; Stage #2: sodium methylate In ethylene glycol at 40 - 45℃; for 5h; Conversion of starting material; | 92% |
With ammonia; sodium methylate In methanol at 60 - 65℃; for 26h; Conversion of starting material; | 68% |
Stage #1: methyl 3-nitrobenzoate With ammonia In butan-1-ol at 40 - 45℃; for 20h; Stage #2: sodium methylate In butan-1-ol at 40 - 45℃; for 8h; Conversion of starting material; |
Conditions | Yield |
---|---|
With potassium phosphate; bis(acetylacetonato)palladium(II); dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine In cyclohexane at 130℃; for 24h; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; ethanol; cerium(III) chloride heptahydrate at 20℃; for 24h; chemospecific reaction; | 91% |
With sodium tetrahydroborate; zinc phthalocyanine In PEG-400 at 100℃; for 10h; | 90% |
With sodium tetrahydroborate In 1,4-dioxane; water for 2h; Ambient temperature; | 80% |
1-Bromo-2,4-dimethoxybenzene
methyl 3-nitrobenzoate
2,2',4,4'-tetramethoxy-3''-nitrotrityl alcohol
Conditions | Yield |
---|---|
Stage #1: 1-Bromo-2,4-dimethoxybenzene With iodine; magnesium In tetrahydrofuran for 0.333333h; Stage #2: methyl 3-nitrobenzoate In tetrahydrofuran at -78℃; | 91% |
Conditions | Yield |
---|---|
With sulfuric acid; dibromoisocyanuric acid | 90% |
With sulfuric acid; dibromoisocyanuric acid at 20℃; for 2h; | 86% |
With sulfuric acid; dibromoisocyanuric acid at 20℃; for 2h; Inert atmosphere; Schlenk technique; | 86% |
Conditions | Yield |
---|---|
With potassium hydroxide; Cumene hydroperoxide In ammonia at -33℃; | 90% |
methyl 3-nitrobenzoate
propan-1-ol-3-amine
N-(3-Hydroxypropyl)-3-nitrobenzamide
Conditions | Yield |
---|---|
In toluene at 94℃; for 3.5h; Acylation; | 90% |
methyl 3-nitrobenzoate
tert-butyl alcohol
3-nitro-benzoic acid t-butyl ester
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane for 1h; | 89% |
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