2-benzhydrylsulfanyl-N-hydroxyacetamide
adrafinil
Conditions | Yield |
---|---|
With dihydrogen peroxide; acetic acid at 40℃; | 72% |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 99 percent / trifluoroacetic acid / 3 h / 20 °C 2: 99 percent / H2SO4 / Heating 3: 92 percent / hydroxylamine hydrochloride; KOH / methanol / 0.25 h 4: 72 percent / aq. H2O2; acetic acid / 40 °C View Scheme |
(benzhydrylthio)acetic acid
adrafinil
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 99 percent / H2SO4 / Heating 2: 92 percent / hydroxylamine hydrochloride; KOH / methanol / 0.25 h 3: 72 percent / aq. H2O2; acetic acid / 40 °C View Scheme |
(diphenylmethyl)(ethyl acetate)sulfide
adrafinil
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 92 percent / hydroxylamine hydrochloride; KOH / methanol / 0.25 h 2: 72 percent / aq. H2O2; acetic acid / 40 °C View Scheme |
adrafinil
Conditions | Yield |
---|---|
In water; acetonitrile pH=6.0; Inert atmosphere; |
Conditions | Yield |
---|---|
In water; acetonitrile pH=6.0; Inert atmosphere; |
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