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Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

Amadis Chemical offer CAS#65-30-5;CAT#A835058

Cas:65-30-5

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

S-(-)-nicotine hemisulfate
65-30-5

S-(-)-nicotine hemisulfate

4-(6-hydroxy-[3]pyridyl)-4-oxo-butyric acid
15873-27-5

4-(6-hydroxy-[3]pyridyl)-4-oxo-butyric acid

Conditions
ConditionsYield
With Pseudomonas sp. DSM 8653; citric acid; yeast extract In water at 30℃; for 15h;91%
S-(-)-nicotine hemisulfate
65-30-5

S-(-)-nicotine hemisulfate

(S)-6-hydroxy-D-nicotine
10516-09-3

(S)-6-hydroxy-D-nicotine

Conditions
ConditionsYield
With Arthrobacter oxydans NRRL-B-3603; corn steep liquor In water at 30℃; for 38h; pH 5.5;51%
S-(-)-nicotine hemisulfate
65-30-5

S-(-)-nicotine hemisulfate

(S)-5,6-dichloronicotine
197641-90-0

(S)-5,6-dichloronicotine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 51 percent / Arthrobacter oxydans NRRL-B-3603, corn steep liquor / H2O / 38 h / 30 °C / pH 5.5
2: 91 percent / chlorine / methanol / 5 h / 19 °C
3: 70 percent / PCl5 / POCl3 / 1 h / 50 - 95 °C
View Scheme
S-(-)-nicotine hemisulfate
65-30-5

S-(-)-nicotine hemisulfate

5-chloro-6-hydroxy-(S)-nicotine

5-chloro-6-hydroxy-(S)-nicotine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 51 percent / Arthrobacter oxydans NRRL-B-3603, corn steep liquor / H2O / 38 h / 30 °C / pH 5.5
2: 91 percent / chlorine / methanol / 5 h / 19 °C
View Scheme
S-(-)-nicotine hemisulfate
65-30-5

S-(-)-nicotine hemisulfate

(S)-6-chloronicotine
112091-17-5

(S)-6-chloronicotine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 51 percent / Arthrobacter oxydans NRRL-B-3603, corn steep liquor / H2O / 38 h / 30 °C / pH 5.5
2: 88.6 percent / PCl5 / POCl3 / 1 h / 40 - 92 °C
View Scheme
cadmium sulfate

cadmium sulfate

S-(-)-nicotine hemisulfate
65-30-5

S-(-)-nicotine hemisulfate

nicotinium disulfatocadmate

nicotinium disulfatocadmate

Conditions
ConditionsYield
In ethanol; water pptn. with abs. alcohol;
In ethanol; water pptn. with abs. alcohol;
ammonium thiocyanate

ammonium thiocyanate

nickel(II) sulphate

nickel(II) sulphate

S-(-)-nicotine hemisulfate
65-30-5

S-(-)-nicotine hemisulfate

Ni(SCN)2 * nicotine

Ni(SCN)2 * nicotine

Conditions
ConditionsYield
In water addn. of a few drops of aq. soln. of NiSO4*6H2O and NH4SCN to aq. soln. of tech. nicotinium sulfate (40% nicotine);; pptn.;;
In water addn. of a few drops of aq. soln. of NiSO4*6H2O and NH4SCN to aq. soln. of tech. nicotinium sulfate (40% nicotine);; pptn.;;
copper(II) sulfate
7758-99-8

copper(II) sulfate

S-(-)-nicotine hemisulfate
65-30-5

S-(-)-nicotine hemisulfate

Cu(2+)*2SO4(2-)*2C10H15N2(1+)*8H2O=CuSO4*2C10H14N2*H2SO4*8H2O

Cu(2+)*2SO4(2-)*2C10H15N2(1+)*8H2O=CuSO4*2C10H14N2*H2SO4*8H2O

Conditions
ConditionsYield
With water In ethanol; water mixing of an aq. soln. of CuSO4 and a soln. of neutral nicotinium sulfate in abs. ethanol;; pptn. by further addn. of abs. ethanol; sepn. after a few hours; washing with 95% ethanol; drying on air;;>99
With H2O In ethanol; water mixing of an aq. soln. of CuSO4 and a soln. of neutral nicotinium sulfate in abs. ethanol;; pptn. by further addn. of abs. ethanol; sepn. after a few hours; washing with 95% ethanol; drying on air;;>99
nickel(II) sulphate

nickel(II) sulphate

S-(-)-nicotine hemisulfate
65-30-5

S-(-)-nicotine hemisulfate

NiSO4 * 2 nicotine * H2SO4 * 9 H2O

NiSO4 * 2 nicotine * H2SO4 * 9 H2O

Conditions
ConditionsYield
In ethanol; water addn. of abs. ethanol to mixt. of 0.03 mol NiSO4 in H2O and 0.04 mol neutral nicotinium sulfate in abs. ethanol, concg.;; pptn., washing with 95% ethanol and drying in air;;
In ethanol; water addn. of abs. ethanol to mixt. of 0.03 mol NiSO4 in H2O and 0.04 mol neutral nicotinium sulfate in abs. ethanol, concg.;; pptn., washing with 95% ethanol and drying in air;;

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