As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryAbout Product Technical Details Trimethylolpropane diallyl ether Chemical Properties Boiling point 135 °C/13 mmHg (lit.) density 0.955 g/mL at 25 °C (lit.) vap
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inquiryTrimethylolpropane diallyl ether Basic information Product Name: Trimethylolpropane diallyl ether Synonyms: 1,1,1-TRIMETHYLOLPROPANE DIALLYL ETHER;1,1,1-(TRIHYDROXYMETHYL)PROPANE DIALLYL
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Trimethylolpropane diallyl ether cas 682-09-7Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiryGood Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
1,1,1-tri(hydroxymethyl)propane
3-chloroprop-1-ene
trimethylol propane diallyl ether
Conditions | Yield |
---|---|
With sodium hydroxide In water at 90℃; Inert atmosphere; |
trimethylol propane diallyl ether
2,4,4-trimethyl-1-pentyl hypophosphorous acid
[3-(2-hydroxymethyl-2-{3-[hydroxy-(2,4,4-trimethylpentyl)phosphinoyl]propoxymethyl}butoxy)propyl]-(2,4,4-trimethylpentyl)phosphinic acid
Conditions | Yield |
---|---|
With di-tert-amyl peroxide at 140℃; for 6h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With potassium methanolate at 120℃; for 20.9h; Inert atmosphere; | 98.2% |
Conditions | Yield |
---|---|
With potassium methanolate at 120℃; for 21.7667h; Inert atmosphere; | 97.9% |
trimethylol propane diallyl ether
Conditions | Yield |
---|---|
With phosphorus trichloride In acetonitrile at -15 - 20℃; for 4h; Inert atmosphere; | 88% |
trimethylol propane diallyl ether
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran at 20℃; for 12h; | 56% |
Conditions | Yield |
---|---|
Stage #1: trimethylol propane diallyl ether With sodium In toluene at 110℃; for 4h; Stage #2: 1-bromo-octane In toluene for 6 - 10h; Heating / reflux; | 55% |
trimethylol propane diallyl ether
4-methoxybenzenediazonium tetrafluoroborate
ammonium thiocyanate
Conditions | Yield |
---|---|
copper(II) bis(tetrafluoroborate) In water; acetone at 10 - 15℃; | 35% |
trimethylol propane diallyl ether
ammonium thiocyanate
4-methylbenzenediazonium tetrafluoroborate
Conditions | Yield |
---|---|
copper(II) bis(tetrafluoroborate) In water; acetone at 10 - 15℃; | 35% |
trimethylol propane diallyl ether
ammonium thiocyanate
benzenediazonium tetrafluoroborate
Conditions | Yield |
---|---|
copper(II) bis(tetrafluoroborate) In water; acetone at 10 - 15℃; | 31% |
trimethylol propane diallyl ether
2-methylphenyl diazonium tetrafluoroborate
ammonium thiocyanate
Conditions | Yield |
---|---|
copper(II) bis(tetrafluoroborate) In water; acetone at 10 - 15℃; | 29% |
trimethylol propane diallyl ether
ammonium thiocyanate
3-methylbenzenediazonium tetrafluoroborate
Conditions | Yield |
---|---|
copper(II) bis(tetrafluoroborate) In water; acetone at 10 - 15℃; | 28% |
Conditions | Yield |
---|---|
With benzophenone In various solvent(s) Kinetics; UV-irradiation; | |
With 2,2-dimethoxy-2-phenylacetophenone In various solvent(s) Kinetics; Irradiation; |
Conditions | Yield |
---|---|
With 2,2-dimethoxy-2-phenylacetophenone In various solvent(s) Kinetics; Irradiation; | |
With 2,2-dimethoxy-2-phenylacetophenone at 20℃; for 30h; UV-irradiation; |
trimethylol propane diallyl ether
Conditions | Yield |
---|---|
tris(triphenylphosphine)ruthenium(II) chloride at 120℃; for 2h; |
trimethylol propane diallyl ether
Conditions | Yield |
---|---|
With triethylamine; trichlorophosphate In diethyl ether at -5 - 23℃; for 17.5h; |
bi(cyclopentadiene)
trimethylol propane diallyl ether
D
endo,exo,endo-pentacyclo<6.5.1.02,7.13,6.09,13>pentadeca-4,10-diene
Conditions | Yield |
---|---|
at 180℃; |
Conditions | Yield |
---|---|
With pyridine; dmap |
Conditions | Yield |
---|---|
With pyridine; dmap |
trimethylol propane diallyl ether
Conditions | Yield |
---|---|
With triethylamine; trichlorophosphate In diethyl ether at -5 - 23℃; for 17.5h; | 63.8g |
trimethylol propane diallyl ether
A
2,2-bis(3-sulfanylpropoxymethyl)butan-1-ol
B
C24H50O6S3
Conditions | Yield |
---|---|
With hydrogen sulfide; triethyl phosphite Concentration; Time; |
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile) at 60 - 70℃; for 10h; | |
With 2,2-dimethoxy-2-phenylacetophenone In methanol UV-irradiation; |
trimethylol propane diallyl ether
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 2,2'-azobis(isobutyronitrile) / 10 h / 60 - 70 °C 2: hydrogenchloride / methanol; water / 3 h / Reflux 3: toluene-4-sulfonic acid / toluene / 3 h / Reflux; Dean-Stark 4: DBN / N,N-dimethyl-formamide / 0.5 h / 20 °C View Scheme |
trimethylol propane diallyl ether
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 2,2'-azobis(isobutyronitrile) / 10 h / 60 - 70 °C 2: hydrogenchloride / methanol; water / 3 h / Reflux 3: toluene-4-sulfonic acid / toluene / 3 h / Reflux; Dean-Stark 4: DBN / N,N-dimethyl-formamide / 0.5 h / 20 °C 5: DBN / N,N-dimethyl-formamide / 0.5 h / 20 °C View Scheme |
trimethylol propane diallyl ether
2,2-bis(3-sulfanylpropoxymethyl)butan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 2,2'-azobis(isobutyronitrile) / 10 h / 60 - 70 °C 2: hydrogenchloride / methanol; water / 3 h / Reflux View Scheme | |
With 2,2'-azobis(isobutyronitrile); tiolacetic acid at 20 - 70℃; | 1.6 g |
trimethylol propane diallyl ether
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 2,2'-azobis(isobutyronitrile) / 10 h / 60 - 70 °C 2: hydrogenchloride / methanol; water / 3 h / Reflux 3: toluene-4-sulfonic acid / toluene / 3 h / Reflux; Dean-Stark View Scheme |
Conditions | Yield |
---|---|
With methanesulfonic acid; 4-methoxy-phenol In n-heptane at 20℃; | 808 g |
Conditions | Yield |
---|---|
In toluene at 45℃; |
Conditions | Yield |
---|---|
With 2,2-dimethoxy-2-phenylacetophenone In methanol UV-irradiation; |
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