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Cas:6914-76-7
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1-Methylcyclopropane-1-carboxylic acid CAS: 6914-76-7 Specification Product name 1-Methylcyclopropane-1-carboxylic acid CAS number 6914-76-7 Assay ≥99% Appearance White crystalline powder
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inquiryProduct name: 1-Methylcyclopropane-1-Carboxylic Acid CAS No.:6914-76-7 Molecule Formula:C5H8O2 Molecule Weight:100.11 Purity: 99% Package: 25kg/drum Description:White to yellow crystalline powder Manufacture Standards:Enterprise Standard
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inquiry1-METHYLCYCLOPROPANE-1-CARBOXYLIC ACID Basic information Product Name: 1-METHYLCYCLOPROPANE-1-CARBOXYLIC ACID Synonyms: Cyclopropanecarboxylic acid, 1-methyl-;Einecs 230-020-7;1-METHYLCYCLOPROPANECARBOXYLIC ACID;1-METHYLCYCLOPROPANE-1-CARBOXYL
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inquiryProduct Name: 1-METHYLCYCLOPROPANE-1-CARBOXYLIC ACID Synonyms: 1-Carboxy-1-methylcyclopropane;1-Methylcyclopropanecarboxylic acid 98%;1-METHYLCYCLOPROPAN-1-CARBOXYLIC ACID;1-METHYLCYCLOPROPANECARBOXYLIC ACID;1-METHYLCYCLOPROPANE-1-CARBOXYLIC ACI
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1-Methylcyclopropancarbonsaeurenitril
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
With sodium hydroxide for 3h; Heating; | 99% |
With sodium hydroxide for 3h; Reflux; | 87% |
With sodium hydroxide |
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
Stage #1: benzyl 2,2-dibromo-1-methylcyclopropylcarboxylate With sodium In tetrahydrofuran; ethanol; water; toluene at 20℃; for 1h; Inert atmosphere; Stage #2: With hydrogenchloride In tetrahydrofuran; ethanol; water; toluene pH=1; | 94.1% |
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
Stage #1: benzyl 2,2-dichloro-1-methylcyclopropylcarboxylate With sodium In tetrahydrofuran; ethanol; water; toluene at 20℃; for 1h; Inert atmosphere; Stage #2: With hydrogenchloride In tetrahydrofuran; ethanol; water; toluene pH=1; | 93.3% |
methyl 2,2-dichloro-1-methylcyclopropanecarboxylate
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
Stage #1: methyl 2,2-dichloro-1-methylcyclopropanecarboxylate With sodium In tetrahydrofuran; ethanol; water; toluene at 20℃; for 1h; Inert atmosphere; Stage #2: With hydrogenchloride In tetrahydrofuran; ethanol; water; toluene for 0.5h; pH=1; | 93.1% |
Conditions | Yield |
---|---|
With sodium In tetrahydrofuran; ethanol; water; toluene at 20℃; for 1h; Inert atmosphere; | 92.7% |
methyl 2,2-dibromo-1-methylcyclopropanecarboxylate
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
Stage #1: methyl 2,2-dibromo-1-methylcyclopropanecarboxylate With sodium In tetrahydrofuran; ethanol; water; toluene at 20℃; for 1h; Inert atmosphere; Stage #2: With hydrogenchloride In tetrahydrofuran; ethanol; water; toluene pH=1; | 92.7% |
Conditions | Yield |
---|---|
With sodium In tetrahydrofuran; ethanol; water; toluene at 20℃; for 1h; Inert atmosphere; | 92.6% |
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
With potassium tert-butylate; water In tetrahydrofuran for 36h; Heating; | 87% |
1-methylcyclopropanecarboxamide
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
With sodium hydroxide for 3h; Reflux; | 86% |
1-methylcyclopropanecarboxylic acid ethyl ester
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
Stage #1: 1-methylcyclopropanecarboxylic acid ethyl ester With methanol; sodium hydroxide; water at 50 - 60℃; for 5h; Stage #2: With hydrogenchloride; water pH=1; | 84% |
Stage #1: 1-methylcyclopropanecarboxylic acid ethyl ester With sodium hydroxide In methanol at 60℃; Stage #2: With hydrogenchloride In methanol; water pH=2; |
Conditions | Yield |
---|---|
With potassium hydroxide at 100℃; im Rohr; | |
(hydrolysis); | |
(saponification); | |
With hydrogenchloride; sodium hydroxide In methanol; 5,5-dimethyl-1,3-cyclohexadiene; water |
carbon dioxide
2-methylallylmagnesium chloride
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
With water Irradiation; |
Conditions | Yield |
---|---|
With sodium hypobromide In water | |
With sodium hydroxide; sodium hypobromide; bromine |
Conditions | Yield |
---|---|
With ozone |
lithium α-lithiocyclopropanecarboxylate
methyl iodide
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
In tetrahydrofuran 1.) -20 deg C, 2.) to room temp., 1 h; | 32 % Spectr. |
Conditions | Yield |
---|---|
With lithium diisopropyl amide 1.) THF, 0 deg C, 10 min, 2.) room temperature, 1 h; Yield given. Multistep reaction; |
1-methylcyclopropanecarbonyl chloride
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
With aluminium trichloride In benzene |
diazomethane
methacrylic acid methyl ester
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
(i), (ii) (alkaline hydrolysis); Multistep reaction; |
3-bromo-2-bromomethyl-2-methyl-propionic acid methyl ester
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: zinc dust; methanol 2: aqueous-methanolic KOH-solution / 100 °C / im Rohr View Scheme |
C9H16O2
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
With hydrogenchloride; water In 1,4-dioxane at 20℃; |
2,2-dichloro-1-methylcyclopropylcarboxamide
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium / toluene; ethanol; water; tetrahydrofuran / 1 h / 20 °C / Inert atmosphere 2: sodium hydroxide / 3 h / Reflux View Scheme |
2,2-dibromo-1-metil-ciclopropilcarbossamide
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium / toluene; ethanol; water; tetrahydrofuran / 1 h / 20 °C / Inert atmosphere 2: sodium hydroxide / 3 h / Reflux View Scheme |
2,2-dichloro-1-methylcyclopropanecarbonitrile
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium / toluene; ethanol; water / 1 h / 20 °C / Inert atmosphere 2: sodium hydroxide / 3 h / Reflux View Scheme |
4-{5-[3-(5-tert-butyl-2-p-tolyl-2H-pyrazol-3-yl)-ureido]-6-methyl-pyridin-2-yloxy}-piperidine-1-carboxylic acid tert-butyl ester
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
With benzotriazol-1-ol; dicyclohexyl-carbodiimide In dichloromethane at 22℃; for 18h; | 100% |
1-Methyl-cyclopropanoic acid
N,O-dimethylhydroxylamine*hydrochloride
N-methoxy-N,1-dimethylcyclopropane-1-carboxamide
Conditions | Yield |
---|---|
Stage #1: 1-Methyl-cyclopropanoic acid With oxalyl dichloride In diethyl ether at 0 - 20℃; for 11h; Inert atmosphere; Stage #2: N,O-dimethylhydroxylamine*hydrochloride With pyridine In diethyl ether; chloroform at 0 - 20℃; for 23h; Inert atmosphere; | 99% |
With triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 2h; | 75.6% |
Stage #1: 1-Methyl-cyclopropanoic acid With 1,1'-carbonyldiimidazole In dichloromethane at 20℃; for 2h; Stage #2: N,O-dimethylhydroxylamine*hydrochloride | 63% |
1-Methyl-cyclopropanoic acid
1-methylcyclopropanecarboxylic acid [1-(cyanomethylcarbamoyl)-2-naphthalen-2-ylethyl]amide
Conditions | Yield |
---|---|
Stage #1: 1-Methyl-cyclopropanoic acid With 1-hydroxybenzotriazole-6-sulfonamidomethyl polystyrene; benzotriazol-1-yloxytripyrrolidinophosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In DMF (N,N-dimethyl-formamide) at 20℃; for 10h; Stage #2: With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 20h; | 98% |
Stage #1: 1-Methyl-cyclopropanoic acid With 1-hydroxybenzotriazole-6-sulfonamidomethyl polystyrene; benzotriazol-1-yloxytripyrrolidinophosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In DMF (N,N-dimethyl-formamide) at 20℃; for 10h; Stage #2: With 1-hydroxybenzotriazole-6-sulfonamidomethyl polystyrene; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 20h; | 98% |
1-Methyl-cyclopropanoic acid
1-methylcyclopropanecarbonyl chloride
Conditions | Yield |
---|---|
With thionyl chloride; N,N-dimethyl-formamide at -40 - 40℃; for 2h; Solvent; Temperature; Time; Reagent/catalyst; | 96.8% |
With thionyl chloride; N,N-dimethyl-formamide at 40℃; for 2h; | 96.8% |
With thionyl chloride for 3h; Heating; | 95% |
1-Methyl-cyclopropanoic acid
(3S)-3-amino-1-(tert-butoxycarbonyl)-pyrrolidine
tert-butyl (3S)-3-{[(1-methylcyclopropyl)carbonyl]amino}pyrrolidine-1-carboxylate
Conditions | Yield |
---|---|
Stage #1: 1-Methyl-cyclopropanoic acid; (3S)-3-amino-1-(tert-butoxycarbonyl)-pyrrolidine With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine In dichloromethane; ethyl acetate at 0 - 20℃; for 1h; Stage #2: With potassium carbonate In dichloromethane; water at 20℃; for 18h; | 95% |
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide | 95% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; boron trifluoride diethyl etherate In tetrahydrofuran; diethyl ether at 20℃; for 2h; | 92% |
With sodium tetrahydroborate; boron trifluoride diethyl etherate In tetrahydrofuran at 20℃; for 72h; | 70 g |
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 18h; Inert atmosphere; | |
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 2h; |
4-carbethoxypiperidine
1-Methyl-cyclopropanoic acid
1-(1-Methyl-cyclopropanecarbonyl)-piperidine-4-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
Stage #1: 1-Methyl-cyclopropanoic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 20℃; for 1h; Stage #2: 4-carbethoxypiperidine In dichloromethane at 20℃; | 92% |
Stage #1: 1-Methyl-cyclopropanoic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 20℃; for 1h; Stage #2: 4-carbethoxypiperidine In dichloromethane at 20℃; | 92% |
1-Methyl-cyclopropanoic acid
N-hydroxy-3,4,5,6-tetrachlorophthalimide
Conditions | Yield |
---|---|
With dmap; diisopropyl-carbodiimide In dichloromethane | 91% |
1-Methyl-cyclopropanoic acid
diethylamine
1-methyl-cyclopropanecarboxylic acid diethylamide
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 12h; | 90% |
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 3h; | 90% |
Conditions | Yield |
---|---|
With triethylamine; HATU In dichloromethane at 30℃; for 1h; | 88.2% |
1-Methyl-cyclopropanoic acid
4-(4-bromophenyl)-5-[(3S)-3-pyrrolidinylmethyl]-2,4-dihydro-3H-1,2,4-triazol-3-one hydrochloride
4-(4-bromophenyl)-5-({(3S)-1-[(1-methylcyclopropyl)carbonyl]-3-pyrrolidinyl}methyl)-2,4-dihydro-3H-1,2,4-triazol-3-one
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 4h; Inert atmosphere; Microwave irradiation; Capped vial; | 87% |
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In acetonitrile for 1h; | 87% |
1-Methyl-cyclopropanoic acid
(1S,4S)-5-(1-methyl cyclopropanecarbonyl)-2-oxa-5-aza-bicyclo[2.2.1]heptan-3-one
Conditions | Yield |
---|---|
Stage #1: 1-Methyl-cyclopropanoic acid With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 2 - 20℃; for 1.5h; Stage #2: (1S,4S)-3-oxo-2-oxa-5-azonia-bicyclo [2.2.1]heptane methanesulfonate With triethylamine In dichloromethane at 2 - 20℃; for 1.16667h; | 86% |
1-Methyl-cyclopropanoic acid
1-methylcyclopropylamine hydrochloride
Conditions | Yield |
---|---|
Stage #1: 1-Methyl-cyclopropanoic acid With diphenyl phosphoryl azide; triethylamine In tert-butyl alcohol at 20 - 75℃; for 16h; Stage #2: With hydrogenchloride In 1,4-dioxane; water for 3h; | 85% |
Stage #1: 1-Methyl-cyclopropanoic acid With diphenyl phosphoryl azide; triethylamine In tert-butyl alcohol at 75℃; Stage #2: With hydrogenchloride In 1,4-dioxane; water at 20℃; for 2h; | 51% |
Yield given. Multistep reaction; |
1-(4-methyl-5-thiazolyl)-1-phenylmethanol
1-Methyl-cyclopropanoic acid
1-methylcyclopropanecarboxylic acid (4-methyl-5-thiazolyl)-phenylmethyl ester
Conditions | Yield |
---|---|
With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane | 85% |
1-Methyl-cyclopropanoic acid
3-(piperidin-4-yl)-3,4-dihydro-1H-pyrano[4,3-c]isoquinolin-6(5H)-one
rac-2-[1-(1-methylcyclopropanecarbonyl)piperidin-4-yl]-1,2,4,10-tetrahydro-3-oxa-10-azaphenanthren-9-one
Conditions | Yield |
---|---|
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 4h; Inert atmosphere; | 85% |
1-Methyl-cyclopropanoic acid
1-t-Butoxycarbonylpiperazine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; O‐(1H‐benzotriazol‐1‐yl)‐N,N,N′,N′‐tetramethyluronium tetrafluoroborate In N,N-dimethyl-formamide at 0 - 20℃; | 85% |
1-Methyl-cyclopropanoic acid
Conditions | Yield |
---|---|
With HATU; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 2.5h; | 83% |
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