As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:7686-77-3
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryTIANFUCHEM-- 7686-77-3--Phenyl vinyl sulfone in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business relat
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryProduct name:3-Cyclopentene-1-carboxylic acid CAS No:7686-77-3 Appearance:Colorless to pale yellow liquid Content:98% Appearance:Colorless to pale yellow liquid Storage:Preserve in well-closed
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inquiry3-Cyclopentene-1-carboxylic acid CAS:7686-77-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality o
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiry1, High quality with competitive price: We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcels can be sent out within 24 hours after payment. Tracking number is available. 2) Secur
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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Min.Order:100 Gram
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiry3-Cyclopentene-1-carboxylic acid Basic information Product Name: 3-Cyclopentene-1-carboxylic acid Synonyms: CYCLOPENT-3-ENE-1-CARBOXYLIC ACID;CYCLOPENT-3-ENECARBOXYLIC ACID;3-CYCLOPENTENE-1-CARBOXYLIC ACID;3-CYCLOPENTENECARBOXYLIC ACID;TIMTEC-
Cas:7686-77-3
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:7686-77-3
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Shanghai Finebiotech Co.,Ltd.was established in 2020, which providing professional chemical services. As a customer-oriented company, we have distinguished ourself from others in providing worldwide customers with cost-effective and efficient service
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiry3-Cyclopentenecarboxylic AcidAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Dimethyl 3-cyclopentene-1,1-dicarboxylate
3-cyclopentene-1-carboxylic acid
Conditions | Yield |
---|---|
at 185 - 195℃; for 1h; | 100% |
at 180℃; for 1h; Neat (no solvent); | 93% |
at 170 - 175℃; for 2h; | 89% |
Conditions | Yield |
---|---|
With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride In dichloromethane at 40℃; for 1h; Schlenk technique; | 98% |
methyl cyclopent-3-ene-1-carboxylate
3-cyclopentene-1-carboxylic acid
Conditions | Yield |
---|---|
With water; lithium hydroxide In tetrahydrofuran at 25℃; for 15h; | 90% |
Dimethyl 3-cyclopentene-1,1-dicarboxylate
3-cyclopentene-1-carboxylic acid
Conditions | Yield |
---|---|
Stage #1: Dimethyl 3-cyclopentene-1,1-dicarboxylate With water; potassium hydroxide In ethanol at 45℃; for 14h; Inert atmosphere; Stage #2: at 180℃; for 1h; Inert atmosphere; | 73% |
Multi-step reaction with 2 steps 1: 45percent KOH / aq. ethanol / 15 h / Heating 2: 100 percent / 1 h / 185 - 195 °C View Scheme | |
Multi-step reaction with 2 steps 1: water; potassium hydroxide / ethanol / 1 h / Reflux 2: 1 h / 180 °C / Neat (no solvent) View Scheme |
methyl cyclopent-3-ene-1-carboxylate
acetonitrile
A
3-cyclopentene-1-carboxylic acid
B
3-(cyclopent-3-en-1-yl)-3-oxopropanenitrile
Conditions | Yield |
---|---|
With potassium tert-butylate; isopropyl alcohol In 2-methyltetrahydrofuran at 20℃; for 2h; Inert atmosphere; | A n/a B 29% |
(+/-)-cyclopent-2-enecarboxylic acid
methyl iodide
A
3-cyclopentene-1-carboxylic acid
cis-3-methylcyclopentanecarboxylic acid
acide methyl-2 cyclopentanecarboxylique-1 cis
Conditions | Yield |
---|---|
With pyridine; bis(1,5-cyclooctadiene)nickel (0); sulfuric acid 1) THF, room temperature, 24 h, 2) THF, room temperature, 24 h; Yield given. Multistep reaction; | A 10% B n/a C 4% |
carbon dioxide
cyclopent-3-enyl bromide
3-cyclopentene-1-carboxylic acid
Conditions | Yield |
---|---|
(i) Mg, Et2O, (ii) /BRN= 1900390/; Multistep reaction; | |
With magnesium 1.) ether, RT, 5 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
Heating; | |
Multi-step reaction with 3 steps 1: 94 percent / 480 °C 2: KOH / H2O; ethanol / 6 h / Heating 3: 180 °C View Scheme |
Conditions | Yield |
---|---|
With sodium hydroxide |
3-cyclopentene-1-carboxylic acid
Conditions | Yield |
---|---|
With barium dihydroxide; water; silver(l) oxide | |
With sodium hydroxide at 350℃; |
Cyclopent-3-ene-1,1-dicarboxylic acid diethyl ester
3-cyclopentene-1-carboxylic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: KOH / H2O; ethanol / 6 h / Heating 2: 180 °C View Scheme |
cyclopent-3-enol
3-cyclopentene-1-carboxylic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (i) TsCl, Py, (ii) /BRN= 3587243/ 2: aq. NaOH View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: water; potassium hydroxide / ethanol / 4 h / Reflux 2: neat (no solvent) / 3 h / 140 °C / Microwave irradiation 3: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 1 h / 40 °C / Schlenk technique View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: neat (no solvent) / 3 h / 140 °C / Microwave irradiation 2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 1 h / 40 °C / Schlenk technique View Scheme |
3-cyclopentene-1-carboxylic acid
methyl iodide
1-Methylcyclopent-3-ene-1-carboxylic acid
Conditions | Yield |
---|---|
Stage #1: 3-cyclopentene-1-carboxylic acid With lithium diisopropyl amide In tetrahydrofuran; n-heptane; ethylbenzene at -30 - 25℃; for 15h; Stage #2: methyl iodide In tetrahydrofuran; n-heptane; ethylbenzene at -30 - 25℃; for 2h; | 100% |
Stage #1: 3-cyclopentene-1-carboxylic acid With lithium diisopropyl amide In tetrahydrofuran; hexane at -78 - 20℃; for 12h; Inert atmosphere; Stage #2: methyl iodide In tetrahydrofuran; hexane at -40 - 20℃; for 18h; Inert atmosphere; | 87% |
Stage #1: 3-cyclopentene-1-carboxylic acid With tert.-butyl lithium In tetrahydrofuran at -78℃; for 1.5h; Inert atmosphere; Stage #2: methyl iodide In tetrahydrofuran at -78℃; | 70% |
methanol
3-cyclopentene-1-carboxylic acid
methyl cyclopent-3-ene-1-carboxylate
Conditions | Yield |
---|---|
Stage #1: 3-cyclopentene-1-carboxylic acid With 1,1'-carbonyldiimidazole In dichloromethane at 0 - 20℃; for 4h; Stage #2: methanol In dichloromethane | 99% |
With oxalyl dichloride In dichloromethane; N,N-dimethyl-formamide | 85% |
With sulfuric acid at 0 - 80℃; for 6h; | 80% |
Conditions | Yield |
---|---|
With palladium diacetate; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In dichloromethane at 25℃; for 12h; Schlenk technique; Inert atmosphere; | 99% |
With palladium diacetate; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In dichloromethane at 25℃; for 12h; Sealed tube; Inert atmosphere; chemoselective reaction; | 99% |
3-cyclopentene-1-carboxylic acid
4-(hydroxymethyl)cyclopentene
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 23℃; for 0.5h; | 98% |
With lithium aluminium tetrahydride In diethyl ether for 6h; Heating; | 97% |
With lithium aluminium tetrahydride In tetrahydrofuran at 66℃; for 6h; Reduction; | 95% |
3-cyclopentene-1-carboxylic acid
(3S*,4S*)-3,4-dibromocyclopentanecarboxylic acid
Conditions | Yield |
---|---|
With Oxalyl bromide; dimethyl sulfoxide In dichloromethane at -10 - 20℃; Inert atmosphere; stereoselective reaction; | 96% |
With hydrogen bromide; dimethyl sulfoxide In chloroform; water at 65℃; for 12h; | 61% |
With bromine In cyclohexane |
3-cyclopentene-1-carboxylic acid
N,O-dimethylhydroxylamine*hydrochloride
cyclopent-3-enecarboxylic acid methoxy-methyl-amide
Conditions | Yield |
---|---|
Stage #1: 3-cyclopentene-1-carboxylic acid With 1,1'-carbonyldiimidazole In dichloromethane for 0.75h; Stage #2: N,O-dimethylhydroxylamine*hydrochloride In dichloromethane | 96% |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; Inert atmosphere; | 71% |
Stage #1: 3-cyclopentene-1-carboxylic acid With 1,1'-carbonyldiimidazole In dichloromethane at 0℃; for 0.5h; Inert atmosphere; Sealed tube; Stage #2: N,O-dimethylhydroxylamine*hydrochloride In dichloromethane at 0 - 20℃; Inert atmosphere; Sealed tube; |
3-cyclopentene-1-carboxylic acid
methyl iodide
methyl cyclopent-3-ene-1-carboxylate
Conditions | Yield |
---|---|
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 20℃; for 16h; | 96% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 16h; | 96% |
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 20℃; for 16h; | 96% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 16h; Schlenk technique; Inert atmosphere; | 87% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 16h; | 86% |
Conditions | Yield |
---|---|
With glucose-diphenylaminium tosylate-derived carbon solid acid (GDTCSA) In n-heptane at 80℃; for 5h; | 96% |
3-cyclopentene-1-carboxylic acid
(1RS,4SR,6RS)-6-bromo-2-oxabicyclo<2.2.1>heptan-3-one
Conditions | Yield |
---|---|
With trimethylsilyl bromide; N-ethyl-N,N-diisopropylamine In 1,4-dioxane; dimethyl sulfoxide for 12h; Heating; | 95% |
With trimethylsilyl bromide; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine In chloroform for 12h; Heating; | 40% |
With trimethylsilyl bromide; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine In chloroform for 12h; Heating; | 40% |
3-cyclopentene-1-carboxylic acid
benzyl bromide
benzyl cyclopent‐3‐ene‐1‐carboxylate
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 60℃; for 2h; | 95% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; | 94% |
With tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate In dichloromethane; water at 20℃; for 16h; | 70% |
3-cyclopentene-1-carboxylic acid
BnBr
benzyl cyclopent‐3‐ene‐1‐carboxylate
Conditions | Yield |
---|---|
With potassium carbonate In [(2)H6]acetone; ethyl acetate; Petroleum ether | 95% |
3-cyclopentene-1-carboxylic acid
(E)-(5-bromopent-3-en-1-yl)benzene
Conditions | Yield |
---|---|
Stage #1: 3-cyclopentene-1-carboxylic acid With lithium diisopropyl amide In tetrahydrofuran; hexane at -78 - 20℃; Inert atmosphere; Stage #2: (E)-(5-bromopent-3-en-1-yl)benzene In tetrahydrofuran; hexane at -40 - 20℃; Inert atmosphere; | 92% |
3-cyclopentene-1-carboxylic acid
1-methyl-1-phenylethyl 2,2,2-trichloroacetimidoate
2-phenylpropan-2-yl cyclopent-3-enecarboxylate
Conditions | Yield |
---|---|
In dichloromethane; cyclohexane at 20℃; for 16h; | 90% |
ethanol
3-cyclopentene-1-carboxylic acid
ethyl 3-cyclopentene-1-carboxylate
Conditions | Yield |
---|---|
With thionyl chloride at 5 - 20℃; for 1.5h; | 89.42% |
With thionyl chloride at 5 - 20℃; for 0.5h; | 84% |
With thionyl chloride at -10℃; for 4h; Inert atmosphere; Schlenk technique; Reflux; | 80% |
With thionyl chloride at 0 - 20℃; | 54% |
With thionyl chloride at 10 - 35℃; |
Conditions | Yield |
---|---|
Stage #1: 3-cyclopentene-1-carboxylic acid With lithium diisopropyl amide In tetrahydrofuran; hexane at -78 - 20℃; Inert atmosphere; Stage #2: 2-methyl-3-bromo-1-propene In tetrahydrofuran; hexane at -40 - 20℃; Inert atmosphere; | 89% |
3-cyclopentene-1-carboxylic acid
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; | 89% |
Conditions | Yield |
---|---|
Stage #1: 3-cyclopentene-1-carboxylic acid With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -10 - 20℃; for 2h; Inert atmosphere; Stage #2: 1-iodo-3-chloro-propane In tetrahydrofuran at -10 - 0℃; for 0.5h; Inert atmosphere; | 89% |
Stage #1: 3-cyclopentene-1-carboxylic acid With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -20 - 20℃; Stage #2: 1-iodo-3-chloro-propane In tetrahydrofuran; hexane at -20 - 20℃; |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; Inert atmosphere; | 88% |
3-cyclopentene-1-carboxylic acid
aniline
3-cyclopentenecarboxylic acid phenyl amide
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere; | 87% |
Stage #1: 3-cyclopentene-1-carboxylic acid With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 1h; Stage #2: aniline With dmap In dichloromethane at 20℃; for 16h; |
3-cyclopentene-1-carboxylic acid
Conditions | Yield |
---|---|
With dmap; diisopropyl-carbodiimide In DClO4 for 12h; Inert atmosphere; | 86% |
With dmap; diisopropyl-carbodiimide In dichloromethane for 1h; | 60% |
With dmap; diisopropyl-carbodiimide In dichloromethane at 20℃; | 46% |
Conditions | Yield |
---|---|
With thionyl chloride Heating; | 85% |
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 0 - 20℃; for 5h; Chlorination; | 80% |
With thionyl chloride |
3-cyclopentene-1-carboxylic acid
Conditions | Yield |
---|---|
With oxalyl dichloride; 1,1'-sulfinylbisbenzene In dichloromethane at -78 - 20℃; for 1h; Inert atmosphere; | 85% |
3-cyclopentene-1-carboxylic acid
isobutene
tert-butyl cyclopent-3-ene-1-carboxylate
Conditions | Yield |
---|---|
With sulfuric acid In diethyl ether for 96h; Ambient temperature; | 84% |
With sulfuric acid In diethyl ether at -78 - 20℃; for 96h; Sealed tube; | 16.98 g |
Conditions | Yield |
---|---|
Stage #1: 3-cyclopentene-1-carboxylic acid With 4-methyl-morpholine In tetrahydrofuran at 0℃; for 0.166667h; Stage #2: With isobutyl chloroformate In tetrahydrofuran for 0.25h; Stage #3: N,N-dimethylethylenediamine In tetrahydrofuran for 2h; | 84% |
3-cyclopentene-1-carboxylic acid
tert-butyl alcohol
tert-butyl cyclopent-3-ene-1-carboxylate
Conditions | Yield |
---|---|
Stage #1: 3-cyclopentene-1-carboxylic acid With oxalyl dichloride In dichloromethane; N,N-dimethyl-formamide at 5 - 20℃; Stage #2: tert-butyl alcohol With triethylamine In dichloromethane at 5 - 20℃; | 83% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; Inert atmosphere; | 83% |
Conditions | Yield |
---|---|
With thionyl chloride at 0℃; for 5h; Inert atmosphere; Reflux; | 82% |
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