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inquirychengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiryOur company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryWe are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryHigh Quality 6-Bromo-4-hydroxy-3-nitroquinoline 853908-50-6 in stock fast delivery good supplierAppearance:Powder Storage:Dry and ventilated Package:according to customers' requirements Application:APIs Transportation:By air(EMS or EUB or FedEx or TN
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryProduct name: 6-Bromo-3-Nitro-4-Quinolinol CAS No.: 853908-50-6 Molecule Formula:C9H5BrN2O3 Molecule Weight:269.05 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryLIDE PHARMACEUTICALS LIMITED is a professional leading manufacturer of chemicals and APIs in China. Our core business line covers APIs, Intermediates, Flavours and fragrances, Specialty chemicals, Dietary additives etc.We are specialized in chemical
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryShanghai Finebiotech Co.,Ltd.was established in 2020, which providing professional chemical services. As a customer-oriented company, we have distinguished ourself from others in providing worldwide customers with cost-effective and efficient service
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inquiryhigh purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
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Min.Order:100 Gram
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inquiryQualityAdvanced technologySupper qualityEffective & safety packageServiceProfessional and timely afte-sale service(replied within 12h)Appearance:see the specification Storage:cool,dry, ventilated Package:1kg/bag, 10kg/drum, 25kg/drum(on requests) App
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inquiry6-bromoquinolin-4-ol
6-bromo-3-nitroquinolin-4-ol
Conditions | Yield |
---|---|
With nitric acid; propionic acid for 2h; | 64.5% |
With nitric acid In propionic acid at 125℃; for 2h; | 50.2% |
With nitric acid In propionic acid at 125℃; for 2h; | 50% |
With nitric acid In propionic acid at 125℃; for 2h; |
(E)-5-bromo-2-((2-nitrovinyl)amino)benzoic acid
6-bromo-3-nitroquinolin-4-ol
Conditions | Yield |
---|---|
With potassium acetate In acetic anhydride at 120℃; for 3h; | 64% |
With potassium acetate In acetic anhydride at 120℃; for 1.5h; | 43% |
With potassium acetate; acetic anhydride at 120℃; for 2h; | 38% |
5-bromo-2-((2-nitroethenyl)amino)benzoic acid
6-bromo-3-nitroquinolin-4-ol
Conditions | Yield |
---|---|
With sodium acetate; acetic anhydride at 120℃; for 2h; | 60% |
With potassium acetate; acetic anhydride at 120℃; for 2h; | 60% |
With potassium acetate; acetic anhydride at 60 - 110℃; for 4h; | 56% |
6-bromo-3-nitroquinolin-4-ol
Conditions | Yield |
---|---|
With sodium acetate; acetic anhydride |
5-bromo-2-((2-nitroethenyl)amino)benzoic acid
acetic anhydride
6-bromo-3-nitroquinolin-4-ol
Conditions | Yield |
---|---|
With potassium acetate at 120℃; for 1.5h; |
5-Bromo-2-aminobenzoic acid
6-bromo-3-nitroquinolin-4-ol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: hydrogenchloride / water / 24 h / 20 °C 2: 24 h / 20 °C 3: acetic anhydride; sodium acetate / 2 h / 120 °C View Scheme | |
Multi-step reaction with 3 steps 1: hydrogenchloride / water / 24 h / 20 °C 2: 24 h / 20 °C 3: acetic anhydride; potassium acetate / 2 h / 120 °C View Scheme | |
Multi-step reaction with 3 steps 1: hydrogenchloride / water / 24 h / 20 °C 2: 24 h / 20 °C 3: potassium acetate; acetic anhydride / 2 h / 120 °C View Scheme |
2-amino-5-bromobenzoic acid hydrochloride
6-bromo-3-nitroquinolin-4-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 24 h / 20 °C 2: acetic anhydride; sodium acetate / 2 h / 120 °C View Scheme | |
Multi-step reaction with 2 steps 1: 24 h / 20 °C 2: acetic anhydride; potassium acetate / 2 h / 120 °C View Scheme | |
Multi-step reaction with 2 steps 1: 24 h / 20 °C 2: potassium acetate; acetic anhydride / 2 h / 120 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: sodium hydroxide / water / 2.17 h / 0 - 20 °C 1.2: 0 °C 1.3: 18 h / 20 °C 2.1: potassium acetate; acetic anhydride / 1.5 h / 120 °C View Scheme |
4-bromo-aniline
6-bromo-3-nitroquinolin-4-ol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: ethanol / 0.17 h / 90 °C 1.2: 0.5 h 2.1: diphenylether / 0.08 h / 220 °C 3.1: nitric acid / propionic acid / 2 h / 125 °C View Scheme | |
Multi-step reaction with 3 steps 1: ethanol / 6 h / 105 °C 2: diphenylether / 0.25 h / 200 °C / Microwave irradiation 3: nitric acid / propionic acid / 2 h / 125 °C View Scheme |
C13H12BrNO4
6-bromo-3-nitroquinolin-4-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diphenylether / 0.08 h / 220 °C 2: nitric acid / propionic acid / 2 h / 125 °C View Scheme |
anthranilic acid
6-bromo-3-nitroquinolin-4-ol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: ammonium bromide; dihydrogen peroxide; acetic acid / 16 h / 10 - 20 °C 2: ethanol / 18 h / 20 °C 3: potassium acetate; acetic anhydride / 2 h / 120 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
Conditions | Yield |
---|---|
With acetic anhydride; potassium carbonate at 90℃; for 1h; |
6-bromo-3-nitroquinolin-4-ol
Conditions | Yield |
---|---|
With potassium carbonate In acetic anhydride at 90℃; for 1h; |
5-(((4-bromophenyl)amino)methylene)-2,2-dimethyl-1,3-dioxane-4,6-dione
6-bromo-3-nitroquinolin-4-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diphenylether / 0.25 h / 200 °C / Microwave irradiation 2: nitric acid / propionic acid / 2 h / 125 °C View Scheme | |
Multi-step reaction with 2 steps 1: 0.17 h / 200 °C / 7757.43 Torr / Microwave irradiation 2: nitric acid / propionic acid / 2 h / 125 °C View Scheme | |
Multi-step reaction with 2 steps 1: diphenylether / 0.25 h / 190 °C 2: nitric acid; propionic acid / 2 h View Scheme |
6-bromo-3-nitroquinolin-4-ol
6-bromo-4-chloro-3-nitroquinoline
Conditions | Yield |
---|---|
With trichlorophosphate for 0.75h; Reflux; | 100% |
With trichlorophosphate at 100℃; for 4h; | 95% |
With trichlorophosphate at 100℃; for 3h; | 95% |
Conditions | Yield |
---|---|
With potassium acetate; bis-triphenylphosphine-palladium(II) chloride In dimethyl sulfoxide at 80℃; Inert atmosphere; | 87% |
methanol
6-bromo-3-nitroquinolin-4-ol
6-methoxy-3-nitroquinolin-4-ol
Conditions | Yield |
---|---|
Stage #1: methanol With sodium at 20℃; for 0.5h; Stage #2: 6-bromo-3-nitroquinolin-4-ol With copper(l) iodide In N,N-dimethyl-formamide at 100℃; for 72h; | 70% |
6-bromo-3-nitroquinolin-4-ol
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; sodium carbonate In N,N-dimethyl-formamide at 140℃; for 16h; | 50% |
With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; sodium carbonate In N,N-dimethyl-formamide at 140℃; for 16h; | 50% |
6-bromo-3-nitroquinolin-4-ol
1-[(6-bromo-3-nitroquinolin-4-yl)amino]-2-methylpropan-2-ol
Conditions | Yield |
---|---|
With trichlorophosphate In N,N-dimethyl-formamide at 100℃; for 0.166667h; |
6-bromo-3-nitroquinolin-4-ol
2-(4-((6-bromo-3-nitroquinolin-4-yl)amino)phenyl)-2-methylpropanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h View Scheme | |
Multi-step reaction with 2 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h View Scheme | |
Multi-step reaction with 2 steps 1: trichlorophosphate / 0.75 h / Reflux 2: acetic acid / 2 h / Reflux View Scheme |
6-bromo-3-nitroquinolin-4-ol
2-[4-(3-amino-6-bromo-quinolin-4-ylamino)-phenyl]-2-methyl-propionitrile
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr View Scheme | |
Multi-step reaction with 3 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-nickel / tetrahydrofuran; methanol / 1 h / 20 °C / 1292.9 Torr View Scheme | |
Multi-step reaction with 3 steps 1: trichlorophosphate / 0.75 h / Reflux 2: acetic acid / 2 h / Reflux 3: hydrogen / Raney Ni / tetrahydrofuran; methanol / 24 h / 20 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C View Scheme | |
Multi-step reaction with 4 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-nickel / tetrahydrofuran; methanol / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice View Scheme | |
Multi-step reaction with 4 steps 1: trichlorophosphate / 0.75 h / Reflux 2: acetic acid / 2 h / Reflux 3: hydrogen / Raney Ni / tetrahydrofuran; methanol / 24 h / 20 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
2-(4-(8-bromo-2-oxo-3-(4-(trifluoromethoxy)phenylsulfonyl)-2,3-dihydro-1H-imidazo[4,5-c]quinolin-1-yl)phenyl)-2-methylpropanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
2-(4-(8-bromo-2-oxo-3-(m-tolylsulfonyl)-2,3-dihydro-1H-imidazo[4,5-c]quinolin-1-yl)phenyl)-2-methylpropanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-nickel / tetrahydrofuran; methanol / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice 5: dichloromethane / 3 h / 20 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
2-(4-(8-bromo-3-(2-methyl-5-nitrophenylsulfonyl)-2-oxo-2,3-dihydro-1H-imidazo[4,5-c]quinolin-1-yl)phenyl)-2-methylpropanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-nickel / tetrahydrofuran; methanol / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice 5: triethylamine / dichloromethane / 3 h / 20 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
2-(4-(8-bromo-3-(3-fluoro-4-methylphenylsulfonyl)-2-oxo-2,3-dihydro-1H-imidazo[4,5-c]quinolin-1-yl)phenyl)-2-methylpropanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-nickel / tetrahydrofuran; methanol / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice 5: triethylamine / dichloromethane / 3 h / 20 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
2-(4-(8-bromo-3-(3,5-dimethylphenylsulfonyl)-2-oxo-2,3-dihydro-1H-imidazo[4,5-c]quinolin-1-yl)phenyl)-2-methylpropanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-nickel / tetrahydrofuran; methanol / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice 5: triethylamine / dichloromethane / 3 h / 20 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
2-(4-(8-bromo-2-oxo-3-(phenylsulfonyl)-2,3-dihydro-1H-imidazo[4,5-c]quinolin-1-yl)phenyl)-2-methylpropanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-nickel / tetrahydrofuran; methanol / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice 5: triethylamine / dichloromethane / 3 h / 20 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
2-(4-(8-bromo-2-oxo-3-tosyl-2,3-dihydro-1H-imidazo[4,5-c]quinolin-1-yl)phenyl)-2-methylpropanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-nickel / tetrahydrofuran; methanol / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice 5: triethylamine / dichloromethane / 3 h / 20 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
2-(4-(8-bromo-2-oxo-3-(thiophen-2-ylsulfonyl)-2,3-dihydro-1H-imidazo[4,5-c]quinolin-1-yl)phenyl)-2-methylpropanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-nickel / tetrahydrofuran; methanol / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice 5: triethylamine / dichloromethane View Scheme |
6-bromo-3-nitroquinolin-4-ol
2-(4-(8-bromo-3-(3-fluorophenylsulfonyl)-2-oxo-2,3-dihydro-1H-imidazo[4,5-c]quinolin-1-yl)phenyl)-2-methylpropanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-nickel / tetrahydrofuran; methanol / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice 5: triethylamine / dichloromethane / 3 h / 20 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
2-(4-(8-bromo-2-oxo-3-(quinolin-8-ylsulfonyl)-2,3-dihydro-1H-imidazo[4,5-c]quinolin-1-yl)phenyl)-2-methylpropanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-nickel / tetrahydrofuran; methanol / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice 5: triethylamine / dichloromethane / 3 h / 20 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
2-(4-(3-(4-acetylphenylsulfonyl)-8-bromo-2-oxo-2,3-dihydro-1H-imidazo[4,5-c]quinolin-1-yl)phenyl)-2-methylpropanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-nickel / tetrahydrofuran; methanol / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice 5: triethylamine / dichloromethane / 3 h / 20 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
2-(4-(8-bromo-2-oxo-3-(3-(trifluoromethyl)phenylsulfonyl)-2,3-dihydro-1H-imidazo[4,5-c]quinolin-1-yl)phenyl)-2-methylpropanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-nickel / tetrahydrofuran; methanol / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice 5: triethylamine / dichloromethane / 3 h / 20 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
2-(4-(8-bromo-3-(3-methoxyphenylsulfonyl)-2-oxo-2,3-dihydro-1H-imidazo[4,5-c]quinolin-1-yl)phenyl)-2-methylpropanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-nickel / tetrahydrofuran; methanol / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice 5: triethylamine / dichloromethane / 3 h / 20 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
2-(4-(8-bromo-3-(3-bromophenylsulfonyl)-2-oxo-2,3-dihydro-1H-imidazo[4,5-c]quinolin-1-yl)phenyl)-2-methylpropanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-nickel / tetrahydrofuran; methanol / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice 5: triethylamine / dichloromethane / 3 h / 20 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
2-(4-(8-bromo-3-(3,5-difluorophenylsulfonyl)-2-oxo-2,3-dihydro-1H-imidazo[4,5-c]quinolin-1-yl)phenyl)-2-methylpropanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-nickel / tetrahydrofuran; methanol / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice 5: triethylamine / dichloromethane / 3 h / 20 °C View Scheme |
6-bromo-3-nitroquinolin-4-ol
2-(4-(8-bromo-3-(2,4-difluorophenylsulfonyl)-2-oxo-2,3-dihydro-1H-imidazo[4,5-c]quinolin-1-yl)phenyl)-2-methylpropanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-Ni / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C 5: triethylamine / dichloromethane / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: trichlorophosphate / 0.75 h / 120 °C 2: acetic acid / 2 h 3: hydrogen / Raney-nickel / tetrahydrofuran; methanol / 1 h / 20 °C / 1292.9 Torr 4: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice 5: triethylamine / dichloromethane / 3 h / 20 °C View Scheme |
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