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Cas:930-55-2
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
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Cas:930-55-2
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Min.Order:1 Kilogram
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Type:Trading Company
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Cas:930-55-2
Min.Order:1 Gram
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Type:Lab/Research institutions
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Cas:930-55-2
Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Cas:930-55-2
Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Cas:930-55-2
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
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FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the N-NITROSOPYRROLIDINE, CAS:930-55-2 with the most competitive price and the best quali
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Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen
CFTC?PharmaChem?is?a?service?based?company?in?China,?a?pharmachem?division?of?Changzhou?Foreign?Trade?Corp.,supplying?raw?materials,?intermediates,?APIs?and?fine?chemicals?for?the?pharmaceutical?and?specialty?chemical?industries?worldwide. Applicatio
Conditions | Yield |
---|---|
With sulfuric acid; silica gel; sodium nitrite In dichloromethane at 20℃; for 0.166667h; | 98% |
With cross-linked polyvinylpyrrolidone*N2O4; dinitrogen tetraoxide In dichloromethane at 20℃; | 98% |
With toluene-4-sulfonic acid; sodium nitrite In dichloromethane at 20℃; for 0.0833333h; chemoselective reaction; | 97% |
C6H12NO(1+)*CH3O4S(1-)
A
pyrrolidine
B
1-pyrrolidinecarboxaldehyde
C
N-nitrosopyrrolidine
Conditions | Yield |
---|---|
With sodium nitrite In water | A n/a B 70% C n/a |
pyrrolidine
bromonitromethane
A
N-nitrosopyrrolidine
B
formaldehyd
Conditions | Yield |
---|---|
In acetonitrile at 70℃; for 168h; | A 62% B n/a |
Conditions | Yield |
---|---|
With sodium nitroprusside at 20℃; Cyclization; | A 50% B n/a |
Conditions | Yield |
---|---|
With trifluoroamine oxide at -15℃; for 1.5h; | A 20% B 30% |
Conditions | Yield |
---|---|
With dinitrogen tetraoxide In tetrachloromethane 40 - 50 deg C, 20 deg C, 15 min; | 30% |
With nitric acid; acetic anhydride 1.) 50 deg C, 30 min, 2.) room temp., 16 h; | 13% |
O2-chloromethyl 1-(pyrrolidin-1-yl)diazen-1-ium-1,2-diolate
1-hydroxy-[3-(2-hydroxyethyl)-3-methyl]-1-triazene 2-oxide sodium salt
A
N-nitrosopyrrolidine
B
N-(2-hydroxyethyl)-N-methyl-N-nitrosamine
Conditions | Yield |
---|---|
With sodium carbonate In acetonitrile at 0 - 20℃; for 7h; | A 30% B 20% |
Benzyl-[1-pyrrolidin-1-yl-meth-(E)-ylidene]-amine
acetic acid
A
1-pyrrolidinecarboxaldehyde
B
N-nitrosopyrrolidine
C
Benzyl acetate
D
benzyl formate
E
benzyl nitrite
F
benzyl alcohol
Conditions | Yield |
---|---|
With cis-nitrous acid at 37℃; Product distribution; further products; time course; | A 1.4% B 23% C 13% D 6.5% E 4% F 6% |
With cis-nitrous acid at 37℃; Product distribution; Mechanism; further products; time course; | A 1.4% B 23% C 13% D 6.5% E 4% F 6% |
piperylin
N-nitrosopyrrolidine
Conditions | Yield |
---|---|
With perchloric acid; sodium nitrite In water at 100℃; for 2h; Product distribution; other reaction conditions; | 2.2% |
With perchloric acid; sodium nitrite In water at 100℃; for 2h; | 2.2% |
Conditions | Yield |
---|---|
With sodium perchlorate at 25℃; Rate constant; |
pyrrolidine
n-propyl nitrite
A
N-nitrosopyrrolidine
B
propan-1-ol
Conditions | Yield |
---|---|
With sodium hydroxide In water at 25℃; Rate constant; Thermodynamic data; ΔH(excit.) and ΔS(excit.); var. solvent system and temp.; |
Conditions | Yield |
---|---|
With sodium hydroxide In water at 25℃; Rate constant; |
pyrrolidine
N-methyl-N-nitrosotoluene-p-sulfonamide
A
N-nitrosopyrrolidine
B
N-methyl-p-toluenesulfonylamide
Conditions | Yield |
---|---|
With sodium bis(2-ethylhexyl)-sulfosuccinate In 2,2,4-trimethylpentane at 25℃; Rate constant; also in water; | |
In 1,4-dioxane; water at 25℃; Rate constant; |
Conditions | Yield |
---|---|
With sodium perchlorate at 25℃; Rate constant; |
1-[N-(4-chloro-phenyl)-formimidoyl]-pyrrolidine
A
1-pyrrolidinecarboxaldehyde
B
N-nitrosopyrrolidine
C
N-(4-chlorophenyl)formamide
D
4-chloro-aniline
E
chlorobenzene
Conditions | Yield |
---|---|
With cis-nitrous acid In acetic acid at 37℃; Product distribution; Mechanism; |
pyrrolidine
S-nitroso-N-acetylpenicillamine
A
N-nitrosopyrrolidine
B
1-Amino-1-carboxy-2-methyl-propane-2-thiol anion
Conditions | Yield |
---|---|
With sodium hydroxide; ethylenediaminetetraacetic acid In water at 25℃; pH=11.57; Kinetics; Further Variations:; Reagents; Nitrosation; |
Conditions | Yield |
---|---|
In acetone at 240℃; Rate constant; Thermodynamic data; decomposition in sealed tube; |
Conditions | Yield |
---|---|
With diethylenetriaminopentaacetic acid; peroxynitrite In phosphate buffer at 37℃; for 0.25h; pH=7.4; Product distribution; Further Variations:; pH-values; |
Conditions | Yield |
---|---|
With 4-nitro-benzenesulfonic acid-(methyl-nitroso-amide) In cyclohexane at 25℃; Kinetics; |
acetic acid
A
N-nitrosopyrrolidine
B
N-(acetyl)pyrrolidine
C
Phenyl acetate
D
phenol
Conditions | Yield |
---|---|
With sodium hydroxide; sodium nitrite In water at 25℃; pH=3.7; Kinetics; |
N-nitrosopyrrolidine
10-(bromomethyl)-2,3,6-trimethoxyphenanthrene
1-nitroso-2-[(2,3,6-trimethoxy-10-phenanthryl)methyl]pyrrolidine
Conditions | Yield |
---|---|
Stage #1: N-nitrosopyrrolidine With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 1h; Inert atmosphere; Stage #2: 10-(bromomethyl)-2,3,6-trimethoxyphenanthrene In tetrahydrofuran at -78 - 20℃; Inert atmosphere; | 93% |
N-nitrosopyrrolidine
N-aminopyrrolidine
Conditions | Yield |
---|---|
With carbon dioxide; water; ammonium chloride; zinc at 35℃; under 1500.15 Torr; for 1.5h; Autoclave; Green chemistry; | 92% |
With titanium(III) chloride In water for 1h; Ambient temperature; | 56% |
With lithium aluminium tetrahydride In diethyl ether Reduction; Heating; |
N-nitrosopyrrolidine
10-(bromomethyl)-2,3,5,6-tetramethoxyphenanthrene
1-nitroso-2-[(2,3,5,6-tetramethoxy-10-phenanthryl)methy]pyrrolidine
Conditions | Yield |
---|---|
Stage #1: N-nitrosopyrrolidine With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 1h; Inert atmosphere; Stage #2: 10-(bromomethyl)-2,3,5,6-tetramethoxyphenanthrene In tetrahydrofuran at -78 - 20℃; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
With potassium sulfate; potassium hydrogensulfate; potassium peroxomonosulfate; acetone In phosphate buffer pH=7 - 8.5; | 88% |
With dihydrogen peroxide; trifluoroacetic anhydride In dichloromethane; water at 0℃; Product distribution / selectivity; Reflux; | 80% |
With dihydrogen peroxide | 65% |
N-nitrosopyrrolidine
9-(bromomethyl)-2,3,6,7-tetramethoxyphenanthrene
1-nitroso-2-[(2,3,6,7-tetramethoxy-9-phenanthryl)methyl]pyrrolidine
Conditions | Yield |
---|---|
Stage #1: N-nitrosopyrrolidine With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 1h; Inert atmosphere; Stage #2: 9-(bromomethyl)-2,3,6,7-tetramethoxyphenanthrene In tetrahydrofuran at -78 - 20℃; Inert atmosphere; | 81% |
Conditions | Yield |
---|---|
With isocyanate de chlorosulfonyle In diethyl ether for 10h; Ambient temperature; | 78% |
N-nitrosopyrrolidine
[(5,10,15,20-tetraphenylporphyrinato)Fe(THF)2]ClO4
[(5,10,15,20-tetraphenylporphyrinato)Fe(N-nitrosopyrrolidine)2]ClO4
Conditions | Yield |
---|---|
In toluene byproducts: C4H8O; (N2, Schlenk) to a toluene-soln. of complex was added nitrosoamine-compound, the mixt. was stirred for 45 min; the solvent was reduced in vol., hexane was added, -22°C overnight, crystals were filtered, washed with hexane, dried in vac.; | 72% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 23℃; for 48h; Irradiation; Inert atmosphere; Sealed tube; Overall yield = 72 percent; regioselective reaction; | A 30% B 42% |
N-nitrosopyrrolidine
A
1-benzamidopyrrolidine
B
N-pyrrolidino-dibenzamide
Conditions | Yield |
---|---|
With acetic acid; zinc Behandeln des Reaktionsprodukts mit Benzoylchlorid und wss. Natronlauge.; |
Conditions | Yield |
---|---|
With lithium diisopropyl amide 1.) 45 min, -78 deg C, THF, HMPT, 2.) -78 degC, 4 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With titanium(III) chloride; ammonium acetate In water for 1h; Product distribution; Ambient temperature; variation of reaction conditions ( pH<1, pH=9.4 ); | A 0.1 % Chromat. B 98 % Chromat. |
With hydrogenchloride; zinc In water for 24h; Product distribution; Ambient temperature; | A 3 % Chromat. B 98 % Chromat. |
With potassium hydroxide; aluminium In water for 24h; Product distribution; Ambient temperature; | A 15 % Chromat. B 87 % Chromat. |
N-nitrosopyrrolidine
C4H9N2O(1+)*C4H8N2O*F6P(1-)
Conditions | Yield |
---|---|
With hexafluorophosphoric acid In diethyl ether |
N-nitrosopyrrolidine
Conditions | Yield |
---|---|
at -253.2℃; Irradiation; |
N-nitrosopyrrolidine
Conditions | Yield |
---|---|
In phosphate buffer at 20 - 25℃; pH=7.4; phosphorylation; UV-irradiation; |