2293-60-9Relevant articles and documents
A general method for the formation of zinc enolate equivalents from iodoacetates by diisopropylzinc-iodine exchange reaction: Preparation of β-Hydroxy esters
Sato,Takizawa,Soai
, p. 2825 - 2826 (2000)
Diisopropylzinc is found to be a highly efficient reagent for the formation of zinc enolate equivalents from various iodoacetates via iodine-Zinc exchange reaction at room temperature, affording β-Hydroxy esters in high yields by the reaction with aldehydes and ketones.
Synthesis method of beta-tertiary alcohol ester compound
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Paragraph 0051-0080, (2020/06/30)
The invention belongs to the technical field of medicine and organic chemical synthesis, and discloses a synthesis method of a beta-tertiary alcohol ester compound. A ketone compound and an iodo-acetate compound are used as raw materials; manganese powder
Method for preparing β - hydroxyl carbonyl compound (by machine translation)
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Paragraph 0071-0075, (2019/10/01)
The present invention relates to a process for preparing β - hydroxycarbonyl compounds, which mainly provides a process for the reaction, using inexpensive commercial iron powder-mediated α -halocarbonyl compounds with aldehydes/ketones, to provide the corresponding β - hydroxycarbonyl compound . the present invention relates to a method. The process is good, has wide functional group tolerance and good compatibility. (by machine translation)