69558-44-7Relevant articles and documents
Synthetic method for cis-1,4-cyclohexanediol
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Paragraph 0048-0052, (2018/03/24)
The invention discloses a synthetic method for cis-1,4-cyclohexanediol, belonging to the field of organic chemical synthesis. According to the method, 4-(alkylacyloxy)cyclohexanone is used as a raw material and is only subjected to reduction and hydrolysis so as to conveniently synthesize cis-1,4-cyclohexanediol. The method can guarantee high selectivity of the reactions, and is high in the yieldof cis-1,4-cyclohexanediol and suitable for large-scale production.
Facile and highly selective monoacylation of symmetric diols adsorbed on silica gel with acetyl chloride
Ogawa, Haruo,Amano, Misa,Chihara, Teiji
, p. 495 - 496 (2007/10/03)
Monoacetylated alcohols of symmetric 1,n-diols are synthesized quantitatively by refluxing a suspension of the diols adsorbed on silica gel with acetylchloride.