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Negotiable |
TRIMEB methyl cyclodextrin cyclodextrin
Test
Method | Result | |
Appearance | Visual | white to slight yellow powder |
Identification 1 | HPLC (EP 2.2.29) | tR of the major peak corresponds to that of the reference |
Identification 2 | NMR (EP 2.2.33) | conform to theoretical structure |
Appearance of 10% aqueous solution | Visual (EP 2.2.1-2) | clear and colorless |
Residual BCD content | TLC (EP 2.2.27) | max. 0.25% |
Residual methyl iodide content | GC (EP 2.2.28) | max. 0.1% |
Methanol content | GC (EP 2.2.28) | max. 0.3% |
Residual solvents: THF |
GC (EP 2.2.28) |
max. 720 ppm |
Assay | HPLC (EP 2.2.29) | min. 97.0% |
Conductivity (25 °C, 1% solution in water) |
Conductometry (EP 2.2.38) | < 100 μS/cm |
Light absorbing impurities (1%) |
UV-Vis (EP 2.2.25) |
A230 - A350: max. 0.1 A350 - A720: max. 0.02 |
Loss on drying | EP 2.2.32 | max. 5.0% |
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