M-aminophenol

M-aminophenol

M-aminophenol

Min.Order / FOB Price:Get Latest Price

25 Kilogram

Negotiable

  • Min.Order :25 Kilogram
  • Purity: 99.0%
  • Payment Terms : T/T

Keywords

591-27-5 M-aminophenol

Quick Details

  • Appearance:white crystalline powder
  • Application:M-aminophenol is an important organic raw material and pharmaceutical intermediate, widely used in petrochemical industry, pesticides, medicine, printing and dyeing industries.
  • PackAge:25kg / Kraft Paper Bag ; 25kg/Cardboard Drums
  • ProductionCapacity:3000|Metric Ton|Year
  • Storage:Store in a cool, ventilated warehouse. Keep away from fire and heat. The package is sealed. It should be stored separately from oxidants, acids and food chemicals, and should not be mixed.
  • Transportation:

Details:

Using m-phenylenediamine as the starting reactant, m-aminoacetanilide hydrochloride was synthesized by monoamino salt formation and acetic anhydride monoacetylation, and then m-aminophenol was synthesized by diazotization and hydrolysis of diazonium salt. Process conditions for multi-step reaction: The optimal reaction conditions for the preparation of m-aminoacetanilide hydrochloride are: acetic anhydride: m-phenylenediamine = 1.1:1, 30% hydrochloric acid solution is added dropwise, and the reaction temperature is 40 ° C. Under the conditions, the yield is up to 92.5%; the optimum reaction conditions for the diazotization of m-aminoacetanilide hydrochloride: m-aminoacetanilide hydrochloride: sodium nitrite: sulfuric acid = 1:1.1:3, in 20% sulfuric acid In the medium, the reaction temperature is -10 ° C. Under the conditions, the diazonium salt synthesized by hydrolysis has the highest yield of meta-aminophenol, which is 70.5%, and the total yield of m-phenylenediamine is 65.2%. 99.9% .

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