Add time:07/30/2019 Source:sciencedirect.com
In the present work, three different kinds of In2S3: hierarchical microspheres A, B and C (HMa, HMb and HMc), which were synthesized by a hydrothermal method in the sodium dodecyl sulfate-thiourea (SDS-thiourea) system. XRD, SEM and BET were used to characterize the prepared In2S3 materials. Compared with the other two kinds of In2S3, the as-prepared In2S3 hierarchical microspheres B (In2S3 HMb) exhibit the best cataluminescence response to ammonium sulfide. The response and recovery times of the home-made ammonium sulfide gas sensor with In2S3 hierarchical microspheres B as sensing materials were about 8 s and 24 s, respectively. The linear dependence of the sensitivity on the ammonium sulfide concentration was observed in the range of 4–200 ppm with an excellent selectivity. These results indicated that In2S3 hierarchical microspheres B would be a good candidate for fabricating practical cataluminescence ammonium sulfide sensor.
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